Language selection

Search

Patent 1041451 Summary

Third-party information liability

Some of the information on this Web page has been provided by external sources. The Government of Canada is not responsible for the accuracy, reliability or currency of the information supplied by external sources. Users wishing to rely upon this information should consult directly with the source of the information. Content provided by external sources is not subject to official languages, privacy and accessibility requirements.

Claims and Abstract availability

Any discrepancies in the text and image of the Claims and Abstract are due to differing posting times. Text of the Claims and Abstract are posted:

  • At the time the application is open to public inspection;
  • At the time of issue of the patent (grant).
(12) Patent: (11) CA 1041451
(21) Application Number: 1041451
(54) English Title: SYSTEM FOR HANDLING THE UNDERFLOW FROM A PRIMARY SEPARATION VESSEL IN THE TAR SAND HOT WATER PROCESS
(54) French Title: SYSTEME DE MANUTENTION DE LA DECHARGE D'UNE CUVE DE SEPARATION PRIMAIRE DANS LE TRAITEMENT DES SABLES BITUMINEUX A L'EAU CHAUDE
Status: Term Expired - Post Grant Beyond Limit
Bibliographic Data
(51) International Patent Classification (IPC):
  • C10G 1/04 (2006.01)
(72) Inventors :
  • MCQUITTY, STANLEY (Canada)
(73) Owners :
  • IMPERIAL OIL LIMITED
  • CANADA-CITIES SERVICE
  • GULF OIL CANADA LIMITED
(71) Applicants :
  • IMPERIAL OIL LIMITED (Canada)
  • CANADA-CITIES SERVICE (Canada)
  • GULF OIL CANADA LIMITED (Canada)
(74) Agent:
(74) Associate agent:
(45) Issued: 1978-10-31
(22) Filed Date: 1975-03-03
Availability of licence: N/A
Dedicated to the Public: N/A
(25) Language of filing: English

Patent Cooperation Treaty (PCT): No

(30) Application Priority Data: None

Abstracts

English Abstract


"SYSTEM FOR HANDLING THE UNDERFLOW
FROM A PRIMARY SEPARATION VESSEL
IN THE TAR SAND HOT WATER PROCESS"
ABSTRACT OF THE DISCLOSURE
For operating control and safety, a close-
coupled pump is direct connected to the underflow of the
primary separation vessel (PSV). The desired discharge density
of the PSV is 70 - 80% solids in order to minimize bitumen
losses. For a good pumping system, the pump discharge density
should be less than 65% solids to avoid settling out of the
solids in the downstream conduit. Therefore it is necessary
to dilute the PSV underflow before it reaches the pump.
Secondary flotation tailings, a dilute stream containing a
high proportion of fine solids, is used for this purpose.
The solids content of the PSV underflow is monitored by one of
two alternative systems - a torque recorder on the PSV rake
shaft or a density gauge on the PSV underflow conduit. The
former is used when the PSV is being fed low fines tar sand -
the latter when it is treating high fines tar sand. The
density of the stream at the pump discharge is monitored to
control the amount of secondary flotation tailings added.
By the use of the controlled-speed, close-coupled pump, a
closed system for controlling underflow density is provided.
By using secondary tailings as the diluent, water requirements
for the process are reduced and a pumpable mixture is provided
from which the solids do not readily settle out.


Claims

Note: Claims are shown in the official language in which they were submitted.


The embodiments of the invention in which an
exclusive property or privilege is claimed are defined as
follows:
1. In the hot water process for recovering
bitumen from tar sand wherein aqueous, tar sand slurry is fed
to a primary separation vessel having a sand rake and tailings
outlet and conduit to produce a primary bitumen froth stream,
a relatively dry primary tailings stream comprising coarse
solids, and an aqueous middlings stream being processed in a
secondary recovery flotation cell to produce a secondary bitumen
froth stream and a relatively fluid secondary tailings stream
comprising water containing fine solids,
the improvement comprising the steps of:
pumping at least part of the secondary tailings
stream with a variable speed pump through a conduit which
joins the primary separation vessel outlet conduit and
combining said stream with the primary tailings stream,
said combined secondary tailings stream being supplied at
a rate sufficient to produce a stream of combined tailings
which is pumpable; and then
pumping the combined tailings stream through
a conduit with a variable-speed close-coupled pump to deliver
it to a tailings distribution system, the speed of said
close-coupled pump being controlled to maintain the density
of the primary tailings stream close to a pre-determined value.
2. The process as set forth in claim 1
wherein:
the combined secondary tailings stream is
supplied at a rate sufficient to produce a stream of combined
tailings containing a maximum of 65% by weight solids.
3. The process as set forth in claim 2
comprising:
- 8 -

establishing a measure of the density of the
combined tailings stream and controlling the speed of the
secondary tailings pump relative thereto to maintain the
solids content of the combined stream below about 65% by
weight.
4. In combination:
primary separation vessel means for separating
bitumen from an aqueous aerated tar sand slurry by flotation
to produce and recover a primary bitumen froth stream, a
middlings stream comprising water, fine solids and bitumen,
and a primary tailings stream containing coarse solids,
said vessel means having a tailings outlet at its base
and a middlings outlet between its ends;
secondary recovery vessel means for
separating bitumen from the middlings stream by aeration
and flotation to produce and recover a secondary bitumen
froth stream and a dilute aqueous secondary tailings stream
containing fine solids, said secondary recovery vessel
means having an inlet and a secondary tailings outlet;
means connecting the middlings outlet of
the primary separation vessel with the inlet of the
secondary recovery vessel for the transfer of the middlings
stream therebetween;
- 9 -

first conduit means leading from the primary
tailings outlet for the removal of the primary tailings stream;
second conduit means connecting the secondary
tailings outlet with the first conduit means at a junction
adjacent the primary tailings outlet for delivering at least
part of the secondary tailings stream thereto to be combined
with the primary tailings stream to form a pumpable mixture;
a first variable speed pump cooperating with
the second conduit means to pump secondary tailings therethrough;
third conduit means connected with the outlet
of the first conduit means for conveying the combined tailings
stream to a distribution zone;
variable-speed close-coupled pump means cooperating
with the first conduit means to pump the combined tailings
stream through the third conduit; and
means for controlling the speed of the close-
coupled pump means to maintain the solids content of the
primary tailings close to a pre-determined value.
5. The combination as set forth in claim
comprising:
means for controlling the speed of the first
pump responsive to the solids content of the combined tailings
stream, whereby the rate at which secondary tailings is added
to the primary tailings may be varied to maintain a pumpable
combined tailings stream.
- 10 -

Description

Note: Descriptions are shown in the official language in which they were submitted.


BACKGROUND OF THE INVENTION
This invention relat:es to the hot water process
for extracting bitumen from tar sand. More particularly, it
/
1 30 relates to a system for controlling the density or solids
, j
:~1
''I .
~ ,
.
:,
.-: : ~
1 ~ .::, ;
:~, ;'.
~ : ~
;

5~
content of the primary separation vessel (PSV) underflow and
fluidizing it to render it pumpable and non~plugging.
A large proportion of the world's known
hydrocarbon reserves exists in the form of tar sands. One
large deposit of this material is found along the banks of
the Athabasca River in Alberta. The tar sand exists in the
,. ...
~ form of water-wet grains of sand, sheathed in a film of bitumen.
:~ :. . .
~ In treating the tar sand to recover commercially useful -~
; products, it is first necessary to separate the bitumen from
the water and sand.
, . . .
-~ The method commonly employed to extract the -~
i bitumen from the mined tar sand is known as the hot water
'3,' process. In the first step of this process, tar sand, hot water
and steam are fed into a rotating tumbler and mixed therein.
The hot water is supplied at a temperature of about 180F
and in amounts sufficient to supply a slurry containing about
20 - 25~ by weight water. The residence time within the -
tumbler is typically four minutes and the exit temperature of
the slurry is about 180F. While in the tumbler, the tar sand
disintegrates and the bitumen particles are liberated from the
i sand.
ii . :
¦ The t~bler product is passed through a screen
to remove lumps and rocks and is then flooded with additional
hot water to further disperse the sand and bitumen particles.
A typical flooded, aqueous, aerated slurry will have a
composition of~7% bitumen, 43% water and 50% solids, and its
temperature will be about 160F - 180F.
The ~looded slurry is then continuously fed ' `1-
into a primary separation vessel. This vessel is conventionally
3Q a cylindrical settler having a conical bottom. In the
vessel, most of the large sand particles (i.e. plus 200 mesh),
.: :: ,
~ fall to the bottom and leave through an outlet as a primary ~ ;
: ... .
:

~f~f~
tailings stream. Most of the bit~men particles, rise to
~` the top of the vessel and form primary bitumen ~roth. This
froth overflows the vessel wall into a launder for removal.
A middlings stream, typically comprising about
~- 5 77~ water/ 21% solids and 2% bitumen, is continuously with-
drawn from the intermediate zone of the primary vessel. The
middlings stream is processed in a secondary recovery flotation
-~ cell to produce secondary froth and a secondary tailings
stream.
.. . .. .:
.,i . ~ ~. .
:' 10 SUMMARY OF T~IE INVENTION
It is desirable to operate the primary separation
, vessel so as to keep the underflow or tailings relatively dry.
fi This is done to reduce the loss of bitumen with this stream,
;f since bitumen loss increases as the water content of the
primary tailings stream increases. In practice, the PSV
is operated to try to keep the primary tailings solids content
;f above about 65% by weight, preferably above 7~%. A typical
! primary tailings stream may comprise 30% waterl 69.3% solids
-: ~ ,. :.
I and 0.7~ bitumen. The solids are mainly coarse in nature,
; ..........
as shown in Table I hereinbelow which provides an illus~rative -
particle siæe analysis.
Due to the high coarse sand content, the primary
tailings stream must be diluted to improve its pumpability
and to reduce the possibility o the solids settling out and
~ 25 plugging the conduit carrying it to the tailings distribution - :
i~ ~ system.
f The secondary tailings stream is a good deal
more dilute than the primary tailings stream and carries a
large proportlon of fine clay and silt solids particles in
it. A typical secondary tailings stream comprises 78.4% by ;~
f~
1~; ~ ~ ' ' - ` '
$ ~ - 3 -
1 ' :

weight water, 21.1% solids and 0.5% bitumen. Table 1 shows
an illustrative particle size analysis ~or this stxeam.
TABLE I
Size fraction Primary Secondary
(microns?_ _ tailings tailings -~
.:
~ 5 0 - 5 2.6 11.
- 5 - 10 .2 10.7
10 ~ 20 1.5 10.4
20 - 3Q .8 ~.5
30 - 44 1.4 4.3
_ 44 6.6 ~1~6
44 - 74 3.2 10.5
^:
~ 74 - 147 48.~ 46.0
,~,
~ ~ 147 42.1 1.8
;' ' .
In accordance with one aspect of this invention,
Z the PSV is operated to produce a dry primary tailings stream.
At least part of the secondary tailings stream is combined
therewith between the PSV outlet and the pump to produce a ~ ;
. single pumpable stream. As a result, the fine solids of
the secondary tailings stream help to keep the coarse solids
~i 20 of the primary tailings stream in suspension and process water
is conserved.
It is also desirable to provide a responsive and
safe system for controlling the rate at which the primary
tailings are withdrawn from the PSV. In this connection, a
variable-speed close-coupled pump is direct connected to the
PSV downcomer conduit and pumps the combined tailings through
a line to the tailings distribution system. The speed of
Z~ the pump is controlled to ensure that the solids content of
the PSV tailings is maintained close to the desired level. ~;
In a preferred feature, the speed of the close-
::
- 4 - -

~` coupled pump ~s controlled responsive to the torque on the
PSV rake shaft or to the density of the PSV tailings stream.
In the case where the PSV is operating on low ~ines tar sand
~eed, the torque-sensing system is used. With high fines tar
sand ~eed, the density~sensing system is used.
Broadly stated, the invention comprises an
improvement in the hot water process for recovering bitumen
~rom tar sand wherein aqueous tar sand slurry is fed to a primary
separation vessel having a sand rake and tailings outlet and
conduit to produce a primary bitumen froth stream, a relatively
- dry primary tailings stream comprising coarse solids, and an
:
aqueous middlings stream comprising fine solids and bitumen,
said middlings stream being processed in a secondary recovery
~lotation cell to produce a secondary bitumen froth stream ~ ;
and a relatively Eluid secondary tailings stream comprising
,;. . :.
water containing fine solids. The improvement comprises the ~ ~
steps o~: pumping at least part of the secondary tailings -
stream with a variable speed pump through a conduit which
3 joins the primary separation vessel outlet conduit and combining
said secondary tailings with the primary tailings, said
secondary tailings being supplied at a rate su~ficient to
., .:
I produce a stream o~ combined tailings which is pumpable;
and then pumping the combined tailings stream through a
conduit with a variable-speed close-coupled pump to deliver it ;. h
to a tailings distribution system, the speed o~ said close- -
coupled pump being controllad to maintain the density of the
primary tailings stream close to a pre-determined value.
DESCRIPTION OF T~E DRA~ING
The figure is a schematic ~iew o~ the no~el
~; 30 system.
- . :
:" .
.- :: .. . .
: ~- 5 ~

gL5~
~ DESCRIPTION OF PREFERRED EMBPDIMENT
- With re~erence to the Figure, tar sand slurry
is introduced into a primary separation vessel 1 of conven-
`~ tional designO In the vessel,floatàble bitumen in the slurry
` 5 rises to the surface of the vessel contents. Here this bitumen
forms primary froth which is recovered in the launder 2.
A middlings stream is wikhdrawn through an
~; outlet 3 intermediate th~ ends of the vessel by a pump 4
and transferred through -the conduit 5 to a secondary separation
vessel 6. The vessel 6 is a conventional flotation unit,
wherein air is~supplied through an agitation shaft 7 to the
agitator blades 8. The air becomes dispersed in the middlings
;~ in the form of fine bubbles and displaces the bitumen to the
::..
~;~ surface where it forms secondary froth. This froth is recovered
in the launder 9.
,~ . .; Tailings streams are produced from the bottom
outlets 10, 11 of the primary and secondary vessels 1, 6. ~-
As previously stated, it is desirable to maintain the primary
tailings solids content at about 70~ ~ however this is a
~; 20 stream which is difficult to pump and is subject to rapid ;;~
-~ settling out of solids. Therefore a portion of the secondary
~:1
~ tailings, which are relatively dilute, is pumped by a variable-
i speed pump 12 through a conduit 13 which connects with the
downcomer conduit 14 of the primary separation vessel. The
~ 25 secondary tailings mix with the primary tailings to form a
"'! dilute stream. The combined tailings stream is pumped by
the variable-speed close~coupled pump 15 through the conduit
~,' 16 to a tailings distribution 17 for transfer to a settling
pond.
1~30 A nuclear density gauge 18 establishes a
~ measure of the density of the combined tailings stream passing ~
'1 - ~ `
'-.': ' :
.,.~ .:
: . ~
.:, ; . , . .. .... .. " ... : .. . .

through the conduit 16, This continuous reading is trans-
mi-tted to a controller on the secondary tailings pump 12 and
the speed of the pump is varied to maintain the solids content i
of the combined stream below 65% ~y weight, thereby ensuring
pumpability and non-plugging of the conduits.
A second nuclear density guage 19 establishes
a measure of the density of th~ primary tailings stream as
it leaves the outlet 10. This continuous reading can be
transmitted to a controller on the primary tailings pump 15
and the speed of the pump can be varied to maintain the
density of the primary tailings stream close to a pre-determined
value, i.e. that value corresponding to a solids content of
about 70%. This method of monitoring the primary tailings
solids content is particularly useful when high fines tar
sand is being fed to the circuit.
l , .
In the event that low fines tar sand is being
fed to the primary separation vessel, it is preferred to
l establish a measure of the torque on the shaft 20 of the
1 , .. i . ,.. ;. .,
l vessel rake 21. A rake torque recorder 22 can be used for
.
this purpose and its signals transmitted to the controller
j on the primary tailings pump 15. The speed of the pump 15
can thus be varied responsive to these signals to maintain
the density of the primary tailings stream at the desired level.
The invention is characterized by several ~-
advan~ages. The use of a close-coupled pump and closed conduit
system ensures a responsive and safe operation. The use of
the secondary tailings as a fluidizing agent for the primary
tailings reduces the possibility of the contained solids
settling out downstream. In addition, the water requirements ~ ;
of the process are less than would be the case if fresh water
was used, as has been advocated in the prior art. Finally, the
control systems used in conjunction with the pumps are
particularly responsive.

Representative Drawing

Sorry, the representative drawing for patent document number 1041451 was not found.

Administrative Status

2024-08-01:As part of the Next Generation Patents (NGP) transition, the Canadian Patents Database (CPD) now contains a more detailed Event History, which replicates the Event Log of our new back-office solution.

Please note that "Inactive:" events refers to events no longer in use in our new back-office solution.

For a clearer understanding of the status of the application/patent presented on this page, the site Disclaimer , as well as the definitions for Patent , Event History , Maintenance Fee  and Payment History  should be consulted.

Event History

Description Date
Inactive: Expired (old Act Patent) latest possible expiry date 1995-10-31
Grant by Issuance 1978-10-31

Abandonment History

There is no abandonment history.

Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
IMPERIAL OIL LIMITED
CANADA-CITIES SERVICE
GULF OIL CANADA LIMITED
Past Owners on Record
STANLEY MCQUITTY
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
Documents

To view selected files, please enter reCAPTCHA code :



To view images, click a link in the Document Description column (Temporarily unavailable). To download the documents, select one or more checkboxes in the first column and then click the "Download Selected in PDF format (Zip Archive)" or the "Download Selected as Single PDF" button.

List of published and non-published patent-specific documents on the CPD .

If you have any difficulty accessing content, you can call the Client Service Centre at 1-866-997-1936 or send them an e-mail at CIPO Client Service Centre.


Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
Abstract 1994-05-17 1 76
Claims 1994-05-17 3 138
Cover Page 1994-05-17 1 41
Drawings 1994-05-17 1 37
Descriptions 1994-05-17 7 356