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Patent 1134669 Summary

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Claims and Abstract availability

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(12) Patent: (11) CA 1134669
(21) Application Number: 1134669
(54) English Title: DEHYDRATED EDIBLE PRODUCTS
(54) French Title: PRODUITS COMESTIBLES DESHYDRATES
Status: Term Expired - Post Grant
Bibliographic Data
(51) International Patent Classification (IPC):
  • A23L 3/00 (2006.01)
  • A23L 13/50 (2016.01)
  • A23L 21/12 (2016.01)
  • A23L 27/00 (2016.01)
  • A23L 29/231 (2016.01)
  • A23L 29/256 (2016.01)
(72) Inventors :
  • CHALLEN, IAN A. (United Kingdom)
  • EAST, SANDRA (United Kingdom)
  • SANDERSON, GEORGE R. (United Kingdom)
(73) Owners :
  • UNILEVER LIMITED
(71) Applicants :
  • UNILEVER LIMITED (United Kingdom)
(74) Agent: SMART & BIGGAR LP
(74) Associate agent:
(45) Issued: 1982-11-02
(22) Filed Date: 1979-09-07
Availability of licence: N/A
Dedicated to the Public: N/A
(25) Language of filing: English

Patent Cooperation Treaty (PCT): No

(30) Application Priority Data:
Application No. Country/Territory Date
36121/78 (United Kingdom) 1978-09-08

Abstracts

English Abstract


ABSTRACT OF THE DISCLOSURE:
Readily rehydratable dehydrated edible products are
obtained by drying compositions comprising finely divided
foodstuff dispersed in edible gel substantially free of
??ration and having a gel strength corresponding to
yield stress of 200 grams of a cylinder of gel having
12 mm diameter and 12 mm height compressed at 5 cm/minute
between pressure plates; the gels are produced for example
by mixing solid calcium sulphate particles rapidly
throughout gellable aqueous alginate or low-methoxy
pectate sols and then allowing solid calcium sulphate to
dissolve and the mixtures to gel under shear-free
conditions.


Claims

Note: Claims are shown in the official language in which they were submitted.


-12-
THE EMBODIMENTS OF THE INVENTION IN WHICH AN EXCLUSIVE
PROPERTY OR PRIVILEGE IS CLAIMED ARE DEFINED AS FOLLOWS:
1. A dehydrated edible product which has been obtained
by a method comprising drying a composition which comprises
a finely divided foodstuff dispersed in a calcium-ion-
containing edible gel selected from alginate and low-
methoxy pectate gels which has not been subjected to
aeration and which has a gel strength corresponding to
a yield stress of at least 200 grams when a cylinder of
the gel 12 mm in diameter and 12 mm high is subjected to
compression between plates moving together with a speed of
5 cm/minute.
2. A dehydrated edible product according to claim 1,
wherein the gel has been produced by a method comprising
mixing solid calcium sulphate particles rapidly throughout
a gellable aqueous alginate or low-methoxy-pectate sol and
then under shear-free conditions allowing solid calcium
sulphate to dissolve and the mixture to gel.
3. A dehydrated edible product according to claim 1,
wherein the gel has been produced by a method comprising
rapidly making a mixture comprising an alginate or low-
methoxy-pectate sol, a source of calcium ions that in the
absence of an agent capable of releasing calcium ions
provides insufficient calcium ions to gel the sol, fruit
pulp or puree and an agent capable of releasing calcium
ions, and allowing the mixture so made to gel under sub-
stantially shear-free conditions.
4. A dehydrated edible product according to claim 1,
wherein the gel strength corresponds to a yield stress of
at least 350 grams under the defined conditions.
5. A dehydrated edible product according to claim 1
which gives substantial rehydration in 60-120 seconds of
immersion in hot water.

-13-
6. A dehydrated edible product according to claim 1 which
has been air-dried at from 60°C to 80°C.
7. A dehydrated edible product according to claim 1
which has a moisture content in the range 4-12% by weight.
8. A dehydrated edible product according to claim 1 which
further comprises a texture modifying agent selected from
caseinates, albumen, gelatin, starch derivatives, cellu-
lose derivatives, carrageenans, and xanthans.
9. A rehydrated edible product formed by rehydrating a
dehydrated edible product according to claim 1 in hot
water for up to 20 minutes.
10. In a process of producing a dehydrated edible product by
drying a calcium-ion-containing edible gel selected from
alginate and low-methoxy pectate gels, the improvement
which comprises making an edible gel with a finely divided
foodstuff dispersed therein, free of subjection to aeration
and with a gel strength corresponding to a yield stress
of at least 200 grams when a cylinder of the gel 12 mm in
diameter and 12 mm high is subjected to compression between
plates moving together with a speed of 5 cm/minute, and
drying said gel to form a rehydratable dehydrated product.

Description

Note: Descriptions are shown in the official language in which they were submitted.


346fo9
~ .1009
_ H~DR~TED EDIBLE PRODUCTS
The present invention relates to dehydrated edible
products, and in particular to products including pieces
or particles o~ comminuted food, ior example derived irom
pureed meat and vegetables.
Dried ~oods capable o~ reconstitution on the addition
o~ water are well known. Examples include soups, desserts
and snack products. Some of these products, o~ten referred
to as iinstant', are suitable ~or consumption within a ~
short time a~ter reconstitution, e.g. 1-2 minutes, while
others require a longer period of soaking to allow the
constituents o~ the food to rehydrate. Clearly,
specification of the rehydration conditions depends on the
nature of the ingredients comprising the iood. When the
~P '.

11;~4~ i9
- 2 - Q.100
~ood contains pieces o-f dried vegetables or meats,
simmering in boi]ing water -for up to 20 minutes may be
required and con~equently such foods are not acceptable as
instant products.
Instant products comprising dried food pieces such as
dried vegetables and dried meats are commercially available.
These may be obtained by freeze-drying pieces of the
appropriate food. However, pieces obtained by such a
process do not al~iays possess all of the desired
characteristics: e.g. the rehydra-ted product may be
spongy and may be deficient in flavour, colour or texture,
so that it may entirely fail to resemble the original
foodstuff. ~s an example, it has been found that rehydrated
free~e-dried tomato pieces can be undesirably light and
spongy and lac~ing in flavour. In addition, such pieces
are also expensive.
An alternative source of dried edible products is
described in the prior art (Belgian Specification No 836 19~).
These are made by preparing a dispersion of comminuted
foodstuff in an aerated calcium alginate or calciu~ pectate
gel, cutting the gel into pieces and drying the said
pieces. Use of an aerating agent is expensive and may also
in some cases result in an undesirable spongy te~ture in
the rehydrated pieces. ~his approach, therefore, a]so has
disadvantages.
We have surprisingly discovered that unaerated alginate
gels containing comminuted foodstuffs, e.g. purees, after

113~9
3 Q . loog
cut-ting and air dry:ing, c~n be so made as to provide dried
foodstuff pieces which are acceptable for use in instant
produc-ts~
The abili-ty of alginate solutions to form films on
drying is well known. Consequently, it would not be
entirely surprising, and in fact we find, that pieces o~
alginate gel also tend to form films after air drying. In
some cases, depending on the geometry of the gel piece~
prior to drying, a dried ou-ter skin with a hollow interior
is obtained. Such an effec-t can be ob-tained when drying
gelled dice. It has to be noted, moreover, that the dried
materials so obtained have very poor rehydration
characteristics.
In contrast, by including a comminuted foodstu~ in
the gel matrix in accordance with the present invention as
described below, an excellent texture simulating vegetable
or meat pieces can be obtained after rehydration o~ the
air-dried gel piece~. Without being bound by theory, the
presence o~ the comminuted food particles appears to hinder
collapse of the alginate network with the accompanying iilm
formation and provides in the dried products particles of -
.
comminuted food dispersed throughout a dried al~inate matrix.The food particles are thus free to hydrate on the addition
of water but in so doing, are prevented from ~eparating by
the alginate matrix. Discrete rehydrated particulates
result.

~ ~ _ Q.lOO~
According to the invention there is provided a dehydrated
edible product obtained by drying a co~position comprising a finely
divided, e g comminu-ted or pureecl, foodstufP dispersed in an
edible (and preîerably thermostable) gel which has not been subjected
5 to aeration and which has a gel strength corresponding to a value
of at least 200 grams when determined by the method defined below
Since the gel has not been subjected to aeration, it has beIore
drying either no overrun or else a minor amount due to unintentional
incorporation of bubbles not sufIicien-t to render the material a
lO foam, e.g. notmore thanlO/O, preferably5/Oorless, e.g. less than-
1%, for example 0.5%,
Desirablythe product is capable of satisfac-toryrehydration
in 60-120 seconds of immersion in ~ater, e.g. hot water. Of course,
the gels are prepared without addlng aerating or foaming agents as
15 such: any constituents which are added for other reasons and are
capable of promoting aeration are preferably restricted to levels
at which any foam_promoting effects are negligible.
In order to produce a dried product capable of satisfactory
rehydration, the drying is preferably carried out by air-dryin~ or
20 oven-drying~
The gel strength can be measured with a commercial Instron (Trade
Mark) test machinewhich compresses a gel of defined size betweentHo
plates at a defined speed: the stress increases to a peak at the yield
point and the yield stress measures the gel strength. The gels used
25 in this invention have at least 200 grams gel strength for a cylind-
rical gel sample 12mm diameter and 12mm high, compressed at 5cm/minute
Desirably the strengths are even higher, corresponding to 350 or more
and can conveniently reach 600 or 700 or more.
One highly desirable ~ethod of producing gels~hich give
30 satisfactory dehydrated products according to this invention

113~6~i9
-- 5
is a fast-setting method (e.g. with gelling time below 30 min-
utes, e.g. 6 minutes), e.g. as described in our co-pending
Canadian Patent Application 335,287: the method disclosed com-
prises mixing solid calcium sulphate particles, for example as
an aqueous slurry with a comminuted foodstuff, rapidly through-
out a gellable aqueous alginate or low-methoxy pectate sol, and
then under shear-free conditions allowing solid calcium sul-
phate to dissolve and the mixture to gel.
However, other methods of producing the gels to be dehy-
drated are also usable in the performance of this invention,e.g. that described in our UK Patent Specifications Nos 1 369
198-9. It relates to rapidly making a mixture comprising an
alginate or a low-methoxy pectate sol, a source of calcium ions
(e.g. dicalcium phosphate) that in the absence of an agent cap-
able of releasing calcium ions (e.g. acid) provides insuffi-
cient calcium ions to gel the sol, fruit pulp or puree and an
agent capable of releasing calcium ions, and allowing the mix-
ture so made to gel under substantially shear-free conditions.
Using this invention, dried pieces of vegetables and meats
which possess excellent colour, flavour and texture after re-
constitution for 1-2 minutes in water have been produced.
After formation, the gel may be cut to the desired shape,
e.g. dice, strips, and dried on commercial air-drying .....

il3
- 6 - Q.100
equipment, e.g. an oven or through draugh-t drier. The
preferred temperature range for drying is 60-80C. Use
of lo~er drying tempera-tures result~ in extended drying
times while use of higher temperatures can result in -
unacceptable flavour lo~s and charring. ~lternatively,
drying may be carried out or facilitated with the aid o*
a vacuum and/or a desiccan-t such as P205 or calcium
chloride. For most applica-tions it is desirable to dry the
particulates to a ~inal mois-ture content of ~-12~/,
preferably ~-9~, e.g. 7~0. , Choice of the appropriate drying
condi-tions depends on the -type of gelled comminuted food
to be dried and its intended usage. Such condition~ are
,." . .i
readily determined by simple experiment. It may be desirable
to carry out two-stage drying with intermediate storage for
a period to allow equilibration of the water content of
the partially-dried material.
When the products are used as ingredients in instant
foods, best results are obtained by rehydration for 1-2
minutes in boiling water.
When necessary, rehydra-tion may be improved and the-
texture of the rehydrated particulates suitably modified
by the addition of a texture modifying agent during the
gel preparation step. Such texture modifying agents are
normally pro-teinaceous or carbohydrate in nature, for
example, caseinates, albumen, gelatin, starch derivatives,
cellulose derivatives, carrageenans, xanthan gum etc.
For economic reasons, an inexpensive texture modifying

_ 7 _ Q.lO0~
agent is pre-~erred. Pre-cool;ed or modified starches at a
level of around 0. 5-3% by weight o~ the gelled comminuted
food have been found -to give acceptable results.
The dehydrated products o~ -the invention can be in `-
the form of particles, slices or small blocks or otherconveniently-shaped regular or irregular pieces.
Although the products of the present invention can be
used acceptably in instant products, they maintain their
~tructural integrity and organoleptic quality under more
prolonged and extreme conditions of rehydration, e.g.
boiling in water for 20 minutes, and can, therefore, be
used generally as ingredients in dry food products, e.g.
dry soup mlxes.`
The invention i~ illnstrated by the following
examples, the table given below showing the composition of
the mixtures used therein.
., :
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c~l
I O O O C" ~ O
O C~l t~ O O O~ O
I I I .
~1 0 ~1 ~ O ~ ~
,
~1
a~
o O O O
O C'~ ~ O
~3 I. I . I I I I . .
~ r~ 0 00 O
X C'~ ~
, ~ . ,
a.~ ~ h
,Q X ~ ' '
~d ~ ~ .
~D ~
h h
E~
~ ~ ' ' ' .
- R ~i
,,,,, ,,~ .
~a~ , - v.
- ~0bD ~ a> ^ .
cd ~ . ~ -
V.
* *
~rl ~ h H
~1 ~t:~ h :~ O
a~ I R ~ O
~ ¢ ¢ ~1~ r~
t' ~rO ~s ~,1 Ul t' ~1
~3~j O~ O O ~ ¢
S ~ FLI O O bq O
. ~ ~ I O r~ O
~l o o ~ ~ ~ o s~
¢ U~ x ¢ a E~ *

.,` 11~6
9 _ Q . loo~
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o o o, ~ o ll
F O .~ o ¦
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~1
C O ~ ~ ¦ ¦ ¦ ¦ ¦
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a~ . .
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- c~ I ~ h
4 ~ ~o C _~ b o~ .
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~ ~ ~ "C5 rl V rl 10 ~4
+, c o ~0~ C 1 ,~ ,y F
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", o y ..

1:1346t~9
- lo - Q.l~og
Example l
~ gel containing ~0% by weigh-t of comminuted tomato
(28-30% solids) was pr~pared by mixing together an
alginate phase and a comminuted food phase, formulated as
shown in the accompanying table, and allowing -the mix to
set under shear free conditions. q'he gel was cut in-to
parallelepipeds with edges varying between 0.~-2.0 cm
which were dried on a commercial through draught drier at
75C for ~ hours. The dried product had an average
mois-ture content of 8.7% and rehydrated.in boiling water
after ca one minute to provide tomato slivers of excellent
taste and pleasant texture.
Example 2
A gel containing ~0/0 by weight of comminuted c~oked
. 15 chicken was prepared as in Example 1 using the formulations
for the alginate phase and the comminuted food phase shown
in the accompanying table The gel was cut into cubes o~
0.8 cm edge which were dried on a through draught drier at
70C for three hours. The dried product had an average
moisture content of 8.1% and on rehydration in boiling
water attained a fibrous texture somewhat akin to cooked
chicken after two minutes.
Example 3
A gel containing 30% by weight of comminuted red
pepper was prepared as in Example 1, u~.ing the formulation
show.n in the accompanying table. The gel was cut into
parallelepipeds (1.5 cm x 0.6 cm x 0 ~ cm) which were

6~9
.looq
dried on a bcnch--scate ilu;dised bcd drier (~'odel FBD/L72*
ex P~L Eng-ineer~ng Ltd) at 70C for 2.5 hours. The result;ng
dried -product of average moistllle content 6.1~o still
retained its strong red colour after nine montll~ storage
and rehydrated in boiling ~ater aftcr ca. one n]inute to
provide ~imulatcd pepper picces with excellent colour,
flavour and texture.
. * Trade Mark
***

Representative Drawing

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Administrative Status

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Event History

Description Date
Inactive: IPC deactivated 2016-03-12
Inactive: IPC deactivated 2016-03-12
Inactive: IPC deactivated 2016-03-12
Inactive: IPC deactivated 2016-03-12
Inactive: IPC deactivated 2016-03-12
Inactive: IPC from PCS 2016-01-09
Inactive: IPC from PCS 2016-01-09
Inactive: IPC from PCS 2016-01-09
Inactive: IPC from PCS 2016-01-09
Inactive: IPC from PCS 2016-01-09
Inactive: IPC expired 2016-01-01
Inactive: IPC expired 2016-01-01
Inactive: IPC expired 2016-01-01
Inactive: IPC expired 2016-01-01
Inactive: IPC expired 2016-01-01
Inactive: IPC from MCD 2006-03-11
Inactive: IPC from MCD 2006-03-11
Inactive: IPC from MCD 2006-03-11
Inactive: IPC from MCD 2006-03-11
Inactive: IPC from MCD 2006-03-11
Inactive: Expired (old Act Patent) latest possible expiry date 1999-11-02
Grant by Issuance 1982-11-02

Abandonment History

There is no abandonment history.

Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
UNILEVER LIMITED
Past Owners on Record
GEORGE R. SANDERSON
IAN A. CHALLEN
SANDRA EAST
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
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Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
Cover Page 1994-02-23 1 9
Abstract 1994-02-23 1 17
Claims 1994-02-23 2 63
Drawings 1994-02-23 1 5
Descriptions 1994-02-23 11 285