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Patent 1212610 Summary

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Claims and Abstract availability

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(12) Patent: (11) CA 1212610
(21) Application Number: 1212610
(54) English Title: METHOD FOR MAKING HOT MELT ADHESIVE BONDED PILE FABRICS
(54) French Title: METHODE DE FABRICATION DE TISSUS AU VELOURS LIE A LA COLLE THERMOFUSIBLE
Status: Term Expired - Post Grant
Bibliographic Data
(51) International Patent Classification (IPC):
  • B32B 7/12 (2006.01)
(72) Inventors :
  • MACHELL, GREVILLE (United States of America)
  • WETHINGTON, CHARLES A. (United States of America)
(73) Owners :
  • MILLIKEN RESEARCH CORPORATION
(71) Applicants :
  • MILLIKEN RESEARCH CORPORATION
(74) Agent: GOWLING WLG (CANADA) LLP
(74) Associate agent:
(45) Issued: 1986-10-14
(22) Filed Date: 1982-09-21
Availability of licence: N/A
Dedicated to the Public: N/A
(25) Language of filing: English

Patent Cooperation Treaty (PCT): No

(30) Application Priority Data:
Application No. Country/Territory Date
304,488 (United States of America) 1981-09-22

Abstracts

English Abstract


Abstract Of The Disclosure
A method for making hot melt adhesive bonded pile fabric
which comprises positioning a pile forming yarn in pile forming
fashion adjacent to one side of a liquid-permeable base layer,
applying a hot melt adhesive heated to at least its softening point
to the base layer on the opposite side of the base layer from the
side adjacent to the pile forming yarn, forcing said hot melt ad-
hesive through the support layer into bond forming contact with
the pile forming yarn, and allowing the adhesive to cool to a
temperature below its softening temperature to thereby bond the
pile forming yarn to the base layer.


Claims

Note: Claims are shown in the official language in which they were submitted.


WHAT IS CLAIMED IS:
1. A method for making hot melt adhesive bonded pile
fabric which comprises positioning a pile forming yarn in pile
forming fashion adjacent to one side of a liquid permeable base
layer, applying a hot melt adhesive heated to at least its soften-
ing point to the base layer on the opposite side of the base layer
from the side adjacent to the pile forming yarn, forcing said hot
melt adhesive through the support layer into bond forming contact
with the pile forming yarn, and allowing the adhesive to cool to
a temperature below its softening temperature to thereby bond the
pile forming yarn to the base layer.
2. A method for making a hot melt adhesive bonded pile
fabric which comprises: positioning two continuous, liquid-per-
meable base layers in a passage where they lie in substantial
parallel relationship to one another at a predetermined distance
from one another; driving at least one continuous pile forming
yarn by folder blades alternatively against the opposing surfaces
of said base layers when they are at or near the entrace to the
above mentioned passage in such a way as to position the pile
forming yarn relative to the base layers and to fold it zig-zag;
thereafter applying to the back of said base layers a hot melt
adhesive; forcing said hot melt adhesive through said base layers
so that said hot melt adhesive contacts said pile forming yarns;
and cooling said hot melt adhesive to a temperature below its
softening point to thereby bond said pile forming yarn to said
base layers.
3. The method according to Claim 2 which comprises the
further step of separating said base layers from one another
to form two continuous hot melt adhesive bonded products.
-17-

4. A method for making a hot melt adhesive bonded pile fabric which
comprises: positioning two continuous, liquid-permeable base layers in a
passage where they lie in substantial parallel relationship to one another
at a predetermined distance from one another; driving at least one
continuous pile forming yarn by folder blades alternatively against the
opposing surfaces of said base layers when they are at or near the entrance
to the above mentioned passage in such a way as to position the pile
forming yarn relative to the base layers and to fold it zig-zag without
tufting said pile-forming yarns through said base layers, thereafter
applying to the back of said base layers a hot melt adhesive; forcing said
hot melt adhesive through said base layers so that said hot melt adhesive
contacts said pile forming yarn; cooling said hot melt adhesive to a
temperature below its softening point to thereby bond said pile forming
yarn to said base layers; and cutting said pile forming yarns to form two
continuous hot melt adhesive bonded products.
18

Description

Note: Descriptions are shown in the official language in which they were submitted.


~212610
~ I
APPARATUS FOR MAKING HOT MEI,T
ADHES IVE BONDED P I LE FABRI CS
The present invention relates to pile fabrics. More par- ¦
ticularly the present invention relates to a method of manufactur-
ing hot melt adhesive bonded pile fabrics.
Pile fabrics such as carpeting may be manufactured in
several ways such as by weaving, tufting, needling or bonding.
In each method the pile must be secured to a base or support
layer in one way or another. The present invention is particular-
ly concerned in one aspect with a method of manufacture wherein
the pile is bonded by means of a hot melt adhesive to a base
layer. Such fabrics will herein be referred to variously as hot
melt adhesive bonded pile fabrics, or hot melt adhesive bonded
carpets.
A number of t~chniques are knQwn for the manufacture of
bonded ~ile fabrics which involve the coating of a preformed base
layer with a layer of an adhesive and thereafter pressing pile-
forming lengths of a yarn into the adhesive to adhere pile-
forming lengths to the base laver.
The ~rior commercial techniaues for making bonded fabrics
have relied very extensively on the use of PVC plastisol formu-
lations because of the processing disadvantages thought to be
associated with the use of other adhesive formulations such as
hot melt systems. According to such techni~ues a ~olvvinyl
chloride plastisol was applied to the base layer prior to position-
ing the pile-forming yarn relative to the base layer. Then the
ile yarn may be posi-ioned into contact wit the base layer and

the plas-tisol may then be fused or cured, t~pically by hea-tiny.
When attempts were made to substitute other adhesives, such as
hot melt adhesives for the PVC plastisol in -this process diffi-
culties were encountered. Thus, for instance, with regard to hot
melt adhesives, it has generally been thought that the apparatus
employed for positioning the yarn may become coated with the ad-
hesive requiring fre~uent shut downs of the apparatus for cleaning
which is, of course, commercially unattractive~
Thus, while PVC plastisol has been the bonding agent of
choice in the preparation of pile fabrics it is ~uite expensive,
and it may tend to give off noxious gases when the product is sub-
jected to combustion conditions~ Also, while polyvinyl chloride
(PVC) plastisol compositions generally may provide good "tuft
lock" characteristics, that is its use results in a firm bond of
the pile forming yarn to the base layer, PVC plastisols generallv
may not penetrate to the desired extent into the yarn bundles to
effect complete adhesion of all pile yarn ibers of the pile yarn
bundle to the pile fabric structure which may result in "fuzzing"
of the end product, especially in carpeting end uses.
Another disadvantage typically associated with the prior
art techni~ues for making non-tufted pile fabrics, that is fabrics
where the pile yarn is not tufted through the backinq but simply
adhered to the backing, is that the adhesive is normally applied
to -the base layer on the side of the base layer ~acing the pile
yarns, and the base layer is normally of a construction such that
the adhesive will not flow through it but will substantially remair
on that surface with perhaps some penetration into the base layer.
Then, if it is desired to apply a backing layer, e.g., a hard back,
o the back side ot the pile fabrlc as may be desired in the

making of carpet tiles the backing layer must be either adhered
directly to the backing layer or an additional ~rocess step of
applying adhesive to the back side of the suppor~ layer may be
necessary. In either event, there is created mlmerous distinct
layers in the finished product, namely pile layer, adhesive layerS
base layer, another adhesive layer and a hard back layer. Such
constructions may inherently have processing disadvantages and be
costly to construct. These layers may also be subject to undesired
separation during use.
The method of the present invention provides bonded pile fabrics
wherein the bonding of the pile-fon~ng yarn to the base
ayer may be accomplished by means of a hot melt adhesive which is
a rela~ively inexpensive and hence commercially attractive ad-
hesive system, which maY advantageously flow into the individual
yarn ~undles to effect more complete adhesion of all the ~ibers of
the pile farming yarn to the pile fabric product. In acoordance with
the method herein the hot melt a~lesive is applied to the base
layer conveniently and in a manner which does not interefere with
the machinery employed for positioning the pile yarn. This step
in the method may accomplish an additional function, namely that
of bonding the individual pile-forming yarns to themselves typi
cally at or near the portion of the yarns nearest the base layer,
thereby providing improved performance characteristics to the pile
fabric product. In addition according to the invention, the ad-
hesive may be applied to the base layer, which is a li~uid-permeabl
layer, from the back of the base layer and it snay be forced throuyh
¦he base laye o tha~ a ne step adhesive la r application may

12~26~
both provide a mea~s for bonding the pile yarn to the base layer
and also provide a means by which a backing layer may be integrally
affixed to the base layer. The resulting product may be less com-
plicated and costly to manufacture and may have fewer separate and
distinct layers in the final product where undesired separation
may occur.
The pile fabrics made by the present invention are hot melt
!¦adhesive bonded fabrics which are comprised of a li~uid-permeable
¦Ibase layer, a pile forming yarn adjacent to but not tufted through
I the base layer, in pile for~ing, preferably folded, fashion; the
pile forming yarn having been bonded to ~he base layer by means of
a hot melt adhesive applied to the back of said base layer and
forced through said base layer into contact with said pile forming
l yarn. Pile forming configurations may include the so-called
I-tuft configuration, e.g. r a non-folded configuration, U-tuft
configurations, and loop pile configurations, among others. Wi~h
regard to the phrase "folded, ~ile forminy fashion," which refers
to a preferred embodiment, it should be understood that what is
intended is a configuration of the pile yarns where the yarns are
~rovided with at least one fold at the portion of the yarn generall~
most nearly adjacent to the base layer, e.g., a cut pile con-
figuration. Another "folded" configuration which is contemplated
lis a loo~ pile configuration where the pile yarns remain uncut in
¦the form of substantially continuous folded yarns in the final
product. A variety of pile configurations both nonfolded and
folded are illustrated in the attached drawing. According to the
most preferred embodiment the pile yarns are cut to form a folded,
cut pile product.
According to the method of the present in-
3D ~ention a pile forming yarn is positioned in pila forming fashion

Ij 12~ 0
adjacent to one side of a liquid-permeable base layer. Thereafter~
a hot melt adhesive, heated to at least its softening point is
applied to the base layer on the opposite side of the base layer
from the side adjacent to the pile forming yarn. According to the
next step of the method a hot melt adhesive may be forced, either
simultaneously with its application or in a separate step, through
the base layer into bond forming contact with the pile forming
yarn, and the adhesive is then allowed to cool, either passively
or by active cooling to a temperature helow its softening tempera-
ture to thereby bond the pile forming yarn to the base layer. The
apparatus includes a means for applyiny the adhesive and forcing
it through the base layer~ It is to be understood that the
~; apparatus is not limited to means for applying only a hot melt
adhesive but may include other bonding compositions commonly used
in the making of bonded fabrics such as, for instance, polyvinyl
~ chloride plastisol formula~ions, etc.
i ~ccording to a preferred embodiment of the present inventior
a method is provided wherein two continuous, liquid- !
permeable base layers are positioned in a passage where they lie
in substantial parallel rela~ionship to one another at a prede-
termined distance from one another; at least one continuous pile
forming yarn is driven by folder blades alternatively against the
opposing surfaces of said base layers when they are at or near the
entrance to the above mentioned passage in such a way as to
~5 position the pile forming yarn relative to the base layers and to
old it zig-zag; thereafter applying to the back of said base
layers a hot melt adhesive; ~orcing said hot melt adhesive through
said base layers so that said hot melt adhesive contacts said
pile forming yarn; and cooling said hot melt adhesive to a tempera-
ture ~elow its softening point to thereby bond said pile forming

1 ~o ~ ~
yarn to said base layers. This step in the method may accomplish
an additional function, namely that of bonding the individual pile
forming yarns to themselves ty~ically at or near the portion of
the yarns nearest the base layer, thereby providing improved per- ¦
formance characteristics to the pile fabric product. Thereafter,
the base layers may be separated from one another to form two
continuous, hot melt adhesive bonded products. Typically such
separation may be accomplished by means of a stationary or moving
knife blade positioned between the base lavers which cuts the pile
yarns along the entire width of the joined base layers to provide
the hot melt adhesive bonded products.
The yarn used in forming the pile mav be made of any type
of fiber known to be useful for fusion bonded fabrics such as
carpets, for example nylon, acrylics, polyester, wool, cotton and
rayon.
The hot melt adhesive compositions which may be emplo~ed
according to the present invention include a wide range of hot
melt adhesives which have been available for many ~ears. Typicall~
such compositions mav have a melt viscositv of less than about
200,000 cps, preferably less than about 100,000 cps a~ 30~F.
Examples include, for instance, blends of ethylene/vinyl ester co-
polymer, petroleum wax and a thermoplastic resin as disclosed in
U. S. Patent Number 3,551,2310 Other
suitable blends which ~ay be used include ethylene/vinyl ester
copolymer, low molecular weight, low density polyethylene, micro-
crystalline wax, aliphatic thermoplastic hydrocarbon resin, di-
cyclopentadiene alkylation polymer, antioxidant and filler as
disclosed in U. S. Patent Number 3,684,600.
Other suitable hot melt adhesives of the ethylene/
vinyl ester tvpe which may be used are disclosed in U. S. Patent

, ,`
- :~L2~
~ ,
¦Numbers 3,583,936, 3,676,280, 3,684,600, 3,745,054, 3,723,371,
3,911,185, 3,914,489 and 4,012,547.
Other hot melt adhesive formulations which may be employed include
those of the atactic polypropylene type. In general such com-
positions may contain a predominant amoun~, e.g., from about 10
parts to about 100 parts or more, preferably from about 60 parts
to 100 parts, by weight atactic polypropylene; from 0 to about 70
parts of another compatible thermoplastic material such as hvdro-
carbon resins, waxes, polyethylene, especially linear, low density
polyethylene; isotactic polypropylene, polyisobutylene and poly-
butene~l. Fillers in widely varying amounts may be added to such
compositions as will be readily apparent to those skilled in the
art.
Other compatible thermoplastic materials which may be em-
ployed in the adhesive formulation include ethylene/ethyl acrylate
polyacetals, polyes~ers, polystyrene, polyacrylonitrile, polyacry-
lic ester, polymethacrylic ester, polyvinyl chloride, polyvinyli-
dene chloride, polyvinyl acetate, polyvinyl acetal, polyvinyl
ether, polytetrafluoroethylene, polyamide, coumarone/indene resins~
natural resins, hydrocarbon resin, bitumen and others.
The amount of hot melt adhesive applied may vary widely,
based upon the particular pile yarn employed, base layer and pro-
perties desired in the pile fabric product. In general the amount
employed may be from about 2 to about 200 ounces, preferably about
4 to about 80 ounces per square yard. Tuft binds for carpet yarns
that may be achieved according to the invention may be from about
2 to about 20 pounds.
Suitable liquid-permeable base layers which may be employed
n the product and process of the nvention include woven fabrics,

i
nitted $abrics, non-woven scrims, felted materials, or even
flexible, foraminous materials.
Where it is desired to provide the ho~ melt adhesive
bonded pile fabrics as floor covering
products, especially carpet tile~, it may be desirable to apply
any of a wide variety of suitable, resilient backing layers to
the fabric. Such carpet tiles are also considered to be within
the scope of the present invention. The backing layer may be
formed, for example, from a suitable thermoplastic ~aterial such
as blends containing ethylene/vinyl acetate copolymers, atactic
polypropvlene, bi~umen, hydrocarbon resins, waxes, synthetic and
natural rubbers.
The backing may be bonded to the base layer by means of the
same adhesive applied to the base layer to bond the pile fibers.
Thus, the resulting product may have fewer separate layers subject
to separation than known carpet tiles. This is, rather than
having pile layer, adhesive layer, base layer, another adhesive
la~er and backing layer, the pr~sent car~et tile may typically
have a pile layer, a single, integral, hot melt adhesive layer int
~a which the base layex may be disposed or suspended, and a back~ng
layer bonded to the comnosite by means of the hot melt adhesive.
ThP backing layer may be provided with at least one stiffening and
stabilizing membrane, such as woven or nonwoven glass fibers.
After the backing has been applied the consolidated material may
then be severed by suitable cutting means into a carpet tile bv
an~ of a variety of techniques which are well-known to those
skilled in the art.

1` ~,~,26~.
The resulting carpet tile product is suitable for use as
a floor covering in home and/or commercial use in an office en-
vironmen~ where substantial high stress conditions (e.g., wheeled
traffic) are applied across the tiles. The tiles typically have
a dense pile and may not re~uire adhesives for installation. The
individual modules may be replaced or rotated as necessary or de-
sired. The carpet tiles may also have excellent dimensional sta-
bility with substantially no curling, slipping, bucklin~, stretchi] ~g
or shrinking. In addition -the carpet tiles may have low smoke
emission and low "fuzzing" characteristics.
The invention may be further understood bv reference to the
drawings and accompanying description thereof. It is to be under-
stood, however, that various changes may be made without departing
from the scope or spirit of the invention which is to be limited
only by the scope of the appended claims. Referring now to the
drawings:
Figure 1 is an elevation view oE the apparatus; and
Figures 2 through 4 illustrate various embodiments for
forcin~ the adhesive through the base layer.
~o Figures 5 through 8 illustrate various pile forming con-
figurations which may be employed in the hot melt adhesive bonded
pile fabrics of the present invention. Figures 9 and 10 illustratl ,
conventional tufted pile fabric configurations showing the pile
yarns tufted through a base layer. Figure 11 illustrates a con-
ventional I-tuft bonded fabric configuration showing a relatively
impermeable base layer.
Referring now to Figure 1 r carpet yarn 10 is supplied from
a yarn source (not shown) over and around guide rolls 12 and 14
d dow~ to the vertical guides 16 ~ase layer 17 ls supplied

121:11ilU
from rolls 18 into position between the guides 16. As the yarn
10 enters between the vertical guides 16 the ~olding blades 20 and
22 alternately displace the yarn in a zig-zag fashion into one or
the other of the base layer sheets 17 as the carpet backing is
being drawn downwardly. Pivotally mounted bladelets 24 and 26 may
assist in the folding of the yarn. Folding blades 20 and 22 are
mounted, respectively, to connecting rods 28 and 30. Connecting
rod 28 is pivotally connected to vivot shafts 32 and 34 and con-
necting rod 30 is pivotally connected to pivot shafts 36 and 38
through suitable links (not shown). The shafts 32 and 38 are
oscillated by an oscillating crank arm mechanism (not shown).
It should be noted that the blade 20 is out of phase with
the blade 22 so that when the blade 22 is being pivoted inwardly
as shown in Figure 1 the blade 20 is being pivoted outwardly and
vice versa to provide a zig-zag configuration of the yarn between
the carpet base layers 17 which are liquid~permeable, that is
permeable to the adhesive to be applied.
After the yarn has been positioned in zig-zag configuration
between the carpet base layers 17, hot melt adhesive 80 maintained
in troughs 82is applied to applicator rolls 34 by passing through
gaps 86 between the side walls 88 of the troughs 32 and the appli-
cator rolls 84. The hot melt adhesive may be maintained in the
liquid phase by heating means not shown. The amount of adhesive
applied to the applicator rollx may be adjusted as desired by
moving troughs 82 upwardly or downwardly as indicated. Applicator
rolls 84 are caused to move preferably in the directions indicated
by drive means not shown whereby adhesive is applied to the carpet
base layers 17 and simultaneously forced through the base layers
into contact with yarn 10. The rolls maY also be forced to move
in the opposite direction to the directions indicated if so
,deslred.

~1~6~0` 1
After the hot melt adhesive has been applied to -the carpet
base layer and forced through it into contact with the car~et yarn,
it may be converted into the solid phase by cooling means 90 to
form a bond between the carpet yarn 10 and the carpet base layers
17. Cooling means 90 may be supplied with air blowers 9~, cooling
coils 94 over which air is forced and thereby cooled prior to
exiting the cooling means through exit ducts 96 into contact with
the carpet base layers to thereby cool the hot melt adhesive causi g
it to revert to the solid phase. The yarn 10 may then be severed,
generally in the middle of the base layers 17 by cutting blade 98
to provide, simultaneously, ~wo sheets of carpet.
Figure 2 is an enlarged view of the hot melt adhesive appli
cator means embodiment 7~ shown in Figure 1. Numbers in Figure 2
corresponding to numbers used in preceding drawings refer to cor-
responding parts of the apparatus. The gaps 86 by means of which
the amount of ho-t melt adhesive to be applied may be adjusted as
desired are more clearly illustrated. Also shown in ~igure 2 are
pre-heating plates 101 which may be provided to pre-heat the base
layers prior to application of hot melt adhesive and to facilitate
~o such application.
Figure 3 illustrates an alternative embodiment wherein the
hot melt adhesive is maintained in a reservoir sided on one side
by base layers 17 and on the other side by doctor blades 104. The
adhesive 80 is allowed to contact the carpet backings and is
forced therethrough by the tips 106 of doctor blades 104.
Figure 4 illustrates yet another embodiment of the inventio
where the hot melt adhesive is maintained in tanks 108. Appli-
cation of the adhesive to the base layers 17 is accomplished by
drawing the adhesive out of the tanks 80 through pumps 110 into

12~
manifolds 112. The adhesive is -then forced from -the openings 114
ln manifolds 112 under sufficient pressure to force the adhesive
through the carpet base layers 17 into contact with carpet yarn
l 10.
¦ Figure 5 illustrates an embodiment oE the present invention
showing an I-tuft configuration of the pile yarns, base layer 17
in the form of a relatively open-weave, adhesive permeable fabric.
Hot melt adhesive 80 is shown as a continuous layer into which the
base layer 17 has become embedded at the base -thereof. A backing
layer 150 made of a thermioplastic material is shown as having been
bonded to the pile fabric by means of the same hot melt adhesive
80 used to bond the pile formirlg varns. Figures 6, 7 and 8
illustrate some folded configurations of the pile forming yarns
which may be preferred. Identifying numbers refer to the same
structural components as in Figure 5. Figure 6 shows a folded,
cut pile configuration. Figure 7 shows a loop pile conEiguration.
Figure 8 shows another folded pile configuration where the folded
portion of the yarn is on the surface giving the appearance of a
loop pile, although the loops are not joined to one another at
their base. This configuration provides in essence a loop pile
product while simultaneously offering the advantages of, for
instance, yarn savings of the so-called I-tuft configuration.
Figure 9 illustrates a conventional cut pile tufted carpet
tile having pile yarn 10 tufted through a conventional, polvpropv-
lene backing 152, adhesive layer 153, and backing layer 154.
Figure 11 differs from Figure 10 only in the illustration of a
loop pile tufted configuration rather than a cut pile configuratior i.
Figure 11 illustrates conventional, multilayered I-tuft bonded
roduct showing the configuration of oile yarns 10, adheslve layer

l~
155, adhesiv impermeable base layer 156 in the Eor~ of tightl~
woven jute, another adhesive layer 157 by means of which backing
layer 15~ may be adhered to the base layer.
The invention may be further understood by reference to
the following examples which are not to be construed as undulv
limiting the invention.
EXA~LE 1
Using a machine similar to that shown in Figure 1, a n~lon
carpet yarn was folded between layers of a woven rayon fabric.
By means of an electrically heated plate mounted on one side only,
directly below the vertical guide 16, the yarn loops in contact
with the fabric at this side only were lightly fused to the fabric.
By omitting the hot-melt adhesive application and the cutting by
the blade, a loop-pile fabric was produced on removal of the other
non-adhering rayon fabric.
A hot-melt adhesive composition was formulated using atactic
polypropylene, hydrocarbon resin and wax, and a molten film of
this adhesive cast on a hot-plate at about 350~F. A portion of
~he loop-pile fabric made as described above was contacted on the
loop-pile face with a piece of non-woven glass scrim. This
asse~bly was then placed with the glass in contact with the hot-
melt adhesive, rolled to force the adhesive through the glass and
into the loop pile yarns, and cooled. Then the glass side of the
sandwich was laminated under heat and pressure to a 60 mils thick
sheet of Keldax~, ~a trademark of DuPont for a filled hot-melt
composition based on a copolymer of ethylene and vinyl acetate).
A blade was then used to cut the yarn sandwich between the rayon
fabric and the glass, thus producing two cut-pile carpets.
-13-

Single yarns were then pulled from the carpet bonded by
the hot-melt adhesive to the glass. The average force required
was found to be 4.6 pounds.
EXAMPLE 2
Used a machine similar to that of Figure 1 with a heater
plate as described in Example 1. There was a rayon fabric on the
same side as the heater plate, an open leno-woven glass scrim
fabric on the non-heated side, and a nylon carpet yarn folded into
the aap. The glass side of the sandwich was contacted with a
heated applicator (identified as Number 84 in Figure 1), above
which was mounted a trough 88 containinq the following formulated
hot-melt adhesive at about 300F:
Elvax~ 350 (DuPont ~thylene/vinyl 30 parts
acetate copolymer
melt index - 19)
5hellmax*400 (Shell micro crystalline 45 parts
wax, melting Point 177F)
Piccopale*100 (Hercules hydrocarbon 25 parts
resin, softening
point: 212F)
By varying the speed of the application roll relative to the yarn
sandwich, and the gap between the trough and the applicator roll,
various levels of adhesive were applied to the yarn loops through
the woven glass scrim. After cooling and cutting of the yarns to
make two cut-pile carpets, the tuft bind was measured on the glass
backed carpet portion. Values varied from 4 pounds tuft bind with
15 ounces/sauare yard of adhesive to 6 pounds with 50 ounces/sauar
yard of adhesive.
EXAMPLE 3
A hot-melt adhesive was formulated as follows:
*Trademark

~Z~
- l
Elvax*350 30 parts
U~ 653-04 (U.S. Industries ethYlene/ 10 parts
vinyl acetate copolymer,
melt index: 375)
Shellma~ 500 (Shell micro crystalline 35 parts
wax, melting point 171F)
Piccopale~ 100 25 parts
Using the procedure of Example 2, this adhesive was applied to the
glass side of the yarn sandwich giving tuft bind ranging from 7 to
10 pounds with an adhesive pick-up of 32 to 48 ounces/square yard.
EXAMPLE 4
With the following hot-melt adhesive formulation:
Elvax*260 ~DuPont ethylene/vinyl 35 parts
acetate copolymer
melt index: 6)
Shellma~ 400 40 parts
Piccopale*100 25 parts
and using the procedure of Example 2, obtained a tuft-bind of 5
pounds w.ith as low as 8 ounces/square yard of adhesive. With 36
ounces of adhesive, the tuft-bind was 9 pounds.
EXAMPLE 5
Used the same procedure as for Example 2, except that the
heated applicator roll/trough to apply the hot-melt adhesive was
replaced by a doctor ~lade applicator on the glass side as depicted
in Figure 3. The adhesive was:
Elva~ 660 (DuPont ethylene~vi~yl acetate 20 ~arts
copolymer
melt index: 2.5)
D-82~(Hercules experimental hot~melt 80 parts
adhesive)
With an adhesive pick uv in the range of 5-20 ounces/square yard
following from the relatively high viscosity of this adhesive, the
tuft-bind averaged 4 pounds.
-15-
*Trad~ark

ll 12126~
EXAMPLE 6
¦ Used ~he method of Example 5, but with a lower viscosit~
adhesive prepared thus:
Atactic polypropylene 83 parts
5 . Dowle~ (Dow linear low density 17 parts
polyethylene, melt index: 20)
A 3 pound tuft-bind was obtained with adhesive pick ups in the
¦range l4- ~nwes/~u~rc y-~d.
~Trademark

Representative Drawing

Sorry, the representative drawing for patent document number 1212610 was not found.

Administrative Status

2024-08-01:As part of the Next Generation Patents (NGP) transition, the Canadian Patents Database (CPD) now contains a more detailed Event History, which replicates the Event Log of our new back-office solution.

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Event History

Description Date
Inactive: Expired (old Act Patent) latest possible expiry date 2003-10-14
Grant by Issuance 1986-10-14

Abandonment History

There is no abandonment history.

Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
MILLIKEN RESEARCH CORPORATION
Past Owners on Record
CHARLES A. WETHINGTON
GREVILLE MACHELL
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
Documents

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Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
Cover Page 1993-09-24 1 15
Abstract 1993-09-24 1 19
Drawings 1993-09-24 4 126
Claims 1993-09-24 2 67
Descriptions 1993-09-24 16 657