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Patent 2440169 Summary

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(12) Patent Application: (11) CA 2440169
(54) English Title: COOLING PLATE
(54) French Title: PLAQUE DE REFROIDISSEMENT
Status: Deemed Abandoned and Beyond the Period of Reinstatement - Pending Response to Notice of Disregarded Communication
Bibliographic Data
(51) International Patent Classification (IPC):
  • C21B 7/10 (2006.01)
  • F27B 1/24 (2006.01)
  • F27D 1/12 (2006.01)
  • F27D 9/00 (2006.01)
(72) Inventors :
  • KORBIK, ELMAR (Germany)
  • HEINRICH, PETER (Germany)
  • BIRNBACH, DETLEF (Germany)
(73) Owners :
  • SMS DEMAG AKTIENGESELLSCHAFT
(71) Applicants :
  • SMS DEMAG AKTIENGESELLSCHAFT (Germany)
(74) Agent: RICHES, MCKENZIE & HERBERT LLP
(74) Associate agent:
(45) Issued:
(86) PCT Filing Date: 2002-03-21
(87) Open to Public Inspection: 2002-10-03
Examination requested: 2006-09-26
Availability of licence: N/A
Dedicated to the Public: N/A
(25) Language of filing: English

Patent Cooperation Treaty (PCT): Yes
(86) PCT Filing Number: PCT/EP2002/003186
(87) International Publication Number: WO 2002077296
(85) National Entry: 2003-09-09

(30) Application Priority Data:
Application No. Country/Territory Date
101 14 720.1 (Germany) 2001-03-23

Abstracts

English Abstract


The invention relates to a cooling plate (1, 101) for a shaft furnace provided
with a refractory lining. Said shaft furnace comprises a first laminated
cooling plate element (2, 102) which is oriented towards the inside of the
furnace (Oi), a second laminated rear cooling plate element (3, 103) which is
welded to the first element, a cooling channel (7, 107) arranged between the
first and second cooling plate elements, and tube sections (8, 9) to the
cooling agent inlet or the cooling agent outlet. The aim of the invention is
to improve the production, flow and cooling properties. To this end, the first
cooling plate element (2, 102) is embodied in the form of a bloom having a
plane front side (14) facing the inside of the furnace (O1), and the cross-
sectional surface of the cooling channel is larger than in the central region
(20; 120), in relation to the longitudinal extension of the cross-section in
the end regions (18, 19; 118, 119). The invention also relates to a cooling
plate system (33).


French Abstract

L'invention concerne une plaque de refroidissement (1, 101) pour fours à cuve munis d'une garniture intérieure réfractaire, comprenant un premier élément laminé de plaque de refroidissement (2, 102) dirigé vers l'intérieur du four (O¿I?) et un second élément de plaque de refroidissement laminé, disposé à l'arrière (3, 103), lesquels sont soudés entre eux, ainsi qu'un canal de refroidissement (7, 107) se trouvant entre le premier et le second élément de plaque, et des sections de tube (8, 9) pour l'entrée, ou la sortie, du fluide de refroidissement, et a pour but d'améliorer les propriétés de finition, d'écoulement et de refroidissement. A cet effet, l'invention est caractérisée en ce que le premier élément de plaque de refroidissement (2, 102) est réalisé sous forme d'un bloom comportant une face avant plane (14) dirigée vers l'intérieur du four (O¿I?), et en ce que la surface transversale du canal de refroidissement est, par rapport à l'extension longitudinale de la section transversale dans les zones d'extrémité (18, 19 ; 118, 119), plus grande que dans la zone médiane (20 ; 120). L'invention concerne en outre un système à plaques de refroidissement (33).

Claims

Note: Claims are shown in the official language in which they were submitted.


CLAIMS
1. Cooling plate (1, 101) for refractory-lined shaft
furnaces,
-- with a first cooling plate element (2, 102) facing the
inside (O i) of the furnace and a second, rear cooling plate
element (3, 103), which are welded together,
-- with a cooling channel (7, 107) formed between the first
and the second elements of the cooling plate, and
-- with pipe sections (8, 9) connected to the coolant inlet
and coolant outlet,
characterized by the fact that the first cooling plate
element (2, 102) is designed as a bloom with a plane front side
(14) facing the inside (O i) of the furnace, and that the cross-
sectional area of the cooling channel is larger in the end
regions (18, 19; 118, 119) than in the center region (20; 120),
as viewed along the longitudinal extent of the cross-section.
2. Cooling plate in accordance with Claim 1, characterized
by the fact that the end regions (18, 19; 118, 119) bulge out on
one or both sides.
3. Cooling plate in accordance with Claim 1 or Claim 2,
characterized by the fact that, on its side facing the furnace
16

interior (O i), the cooling channel cross section is formed by the
first cooling plate element (2) with at least two recesses (16,
17) that run along its rear side (5).
4. Cooling plate in accordance with any of Claims 1 to 3,
characterized by the fact that the cooling channel cross section
is formed on its rear side by a second cooling plate element
(103) that has an at least double trough-like shape with bulges
that project towards the furnace wall.
5. Cooling plate in accordance with Claim 3, characterized
by the fact that the cooling channel cross section is formed on
the rear side by a more or less plane second cooling plate
element (3).
6. Cooling plate in accordance with Claim 4 or Claim 5,
characterized by the fact that the edge region (324, 325) of the
second cooling plate element (103) is formed thicker than its
center region.
7. Cooling plate in accordance with any of Claims 1 to 6,
characterized by the fact that the second cooling plate element
(3, 103) is welded by its longitudinal edges to the rear side (5)
of the first cooling plate element (2, 102).
17

8. Cooling plate in accordance with Claim 7, characterized
by the fact that the second cooling plate element (3) is welded
to the rear side of the first cooling plate element (2) at some
distance from the edges (2a, b) of the first cooling plate
element, and that at least one slit (31) is produced in the edges
regions (2a, b) of the first cooling plate element (2)
perpendicularly to the longitudinal axis of the cooling plate.
9. Cooling plate in accordance with any of Claims 3 to 8,
characterized by the fact that the pipe sections (8, 9) for the
coolant intake and discharge extend through bores in the second
cooling plate element (3) at the rear of the cooling plate, and
that, at the level of these pipe sections (8, 9), the first
cooling plate element (2) is hollowed out, and the depth of the
hollow (39) was intended] decreases in ramp-like fashion towards
the cooling channel recesses (16, 17).
10. Cooling plate in accordance with any of Claims 1 to 9,
characterized by the fact that the cooling plate (1, 101) has at
least two suspension points (34, 38) for mounting the cooling
plate on the furnace wall (10) of the shaft furnace, such that a
first suspension point (34) is designed as a fixed connection in
the upper part of the cooling plate, and a second suspension
18

point (38) is designed as a loose connection in the lower part of
the cooling plate.
11. Cooling plate in accordance with Claim 10,
characterized by the fact that the first suspension point (34)
comprises a screw connection as the fixed connection, and that
the second suspension point (38) comprises a hung connection as
the loose connection.
12. System (33) for cooling refractory-lined shaft
furnaces, which comprises a large number of cooling plates (1,
101) of the types specified in Claims 1 to 11, which are made of
rolled copper or a rolled copper alloy and are installed side by
side or in an overlapping fashion.
19

Description

Note: Descriptions are shown in the official language in which they were submitted.


CA 02440169 2003-09-09
COOLING PLATE
The invention concerns a cooling plate far refractory-lined
shaft furnaces, especially blast furnaces, with a first rolled
cooling plate element facing the inside of the furnace and a
second rolled cooling plate element facing to the rear, which are
welded together, with a cooling channel formed between the first
and the second elements of the cooling plate, and with pipe
sections connected to the coolant inlet and coolant outlet. Both
the first and second cooling plate elements consist of copper or
a low-alloy copper. In addition, the invention concerns a
cooling system.
A cooling plate of this general type is described in German
Patent Application 100 00 987.5, which discloses a cooling plate
for refractory-lined shaft furnaces with cooling channels into
which coolant can be admitted, in which (cooling plate) at least
the front side facing the inside of the furnace consists of a
bloom that contains grooves for receiving refractory material and
is preferably made of copper or a low-alloy copper; in which two
__ _ __ ___. _~__

CA 02440169 2003-09-09
r .
trough-shaped rolled sections, each with the trough facing to the
outside, are welded together; in which bores for receiving the
ends of pipe connection fittings, which are welded in, are
produced in the rolled section or supplementary section on the
rear side; and in which the free ends of the rolled sections are
sealed by caps.
The bending of the first cooling plate element or shield and
the production of grooves in the bent shield is difficult from
the standpoint of manufacturing engineering. Moreover, the more
or less "lens-shaped " cross section of the cooling channel
resulting from the trough-like shape of the two cooling plate
elements has been found to be unfavorable from the standpoint of
fluid mechanics. While the amount of heat flowing from the
lateral fins of the shield towards the cooling water channel is
the greatest, it is precisely in the corners of the "lens " that
the flow rate of the cooling water is the lowest. The low flow
rate leads to a low heat-transfer coefficient oc from the inner
surface of the cooling channel to the cooling water. In
addition, the volume of water flowing past there may experience
an unacceptably high degree of heating.
Therefore, the objective of the invention is to develop a
2
_ _ __ _ ___ T

CA 02440169 2003-09-09
cooling plate of the general type described above with improved
characteristics from the standpoint of manufacturing engineering,
fluid mechanics and cooling engineering.
This objective is achieved by a cooling plate with the
features of Claim 1 and by a system with the features of Claim
12. Advantageous modifications are described in the dependent
claims.
In accordance with the essential concept of the invention,
the first cooling plate element or the shield of the cooling
plate or stavelet is no longer designed as an arched structure,
but rather is designed as a bloom with a plane front side facing
the inside of the furnace, i.e., with a plane hot side, and the
cross-sectional area of the cooling channel formed between the
first and second cooling plate elements is larger in the end
regions than in the center region, as viewed along the
longitudinal extent of the cross-sectional area. The end regions
of the cooling channel cross section are the regions near the
joint lines ox weld seam of the two cooling plate elements. The
end regions may have any desired shape, as long as they have a
larger cross-sectional area than the center region. The effect
of the cross-sectional shape in accordance with the invention is
3

CA 02440169 2003-09-09
that the greatest volume of the cooling water no longer flows in
the center region, but rather in the thermally stressed end
regions of the cooling channel, which results in greater flow
rates and thus more favorable values of the heat-transfer
coefficient. In this regard, the cross section in the center
region should be designed in proportion to the cross section in
the end regions in such a way that the smaller amounts of heat
that develop there can be efficiently eliminated.
All together, a cooling plate with improved flow
characteristics of the cooling water and thus improved cooling
characteristics is created in this way. The temperature on the
hot side, i.e., the side facing the inside of the furnace,
becomes more uniform. Furthermore, a significant advantage is
gained with respect to manufacturing engineering, because the
first cooling plate element now has a plane design and no longer
needs to be curved. In addition, it is much easier to produce
grooves in a plane cooling plate than in a curved cooling plate,
e.g., by milling or roll forming.
In accordance with an especially preferred embodiment, the
end regions of the cooling channel cross section bulge out on one
or both sides. Taking the center region into consideration as
4

CA 02440169 2003-09-09
well, this results in a cooling channel cross section that is
shaped something like a bone or like a half-bone cut along its
longitudinal axis. This shape results in an especially good
ratio of the flow rate of the cooling water to the heat loads
that arise.
To obtain a cooling channel with this type of bone-like
shape, various design combinations are proposed. For a cross
section that is shaped more or less like a half-bone, either a
first cooling plate element with recesses produced in its rear
side facing the water is used, or a second cooling plate element
with a double trough-like shape that bulges out towards the wall
of the furnace is used. A first cooling plate element of this
type is combined with a more or less plane second cooling plate
element; a trough-shaped second cooling plate element is combined
with a first cooling plate element with a plane rear side facing
the water. To obtain a bone-shaped cross section, a first
cooling plate element with recesses is combined with a
corresponding second cooling plate element with recesses or with
a double trough-shaped second cooling plate element.
The recesses, which preferably run parallel to the
longitudinal axis of the cooling plate, are produced by roll
_ __ -!_ _ __~_.. _ _ _

CA 02440169 2003-09-09
forming or by milling. The trough-shaped second cooling plate
element, which is designed thinner than the first cooling plate
element, is produced by roll forming or bending.
Both the first and the second cooling plate element are made
of copper or a copper alloy.
In accordance with a preferred embodiment, the trough-shaped
second cooling plate element has variable material thickness
across its width. It is formed thicker at its edges than in its
center region. This has the advantage that, in the region of
greater heat flow, i.e., in the edge region, more copper material
is available for the conduction of heat. Due to the reinforced
edge regions, the weld for joining the two elements with each
other can also be made more massive. This contributes to the
mechanical stability of the cooling plate and thus to further
improvement of the cooling characteristics of the system.
A second cooling plate element can be welded with the edges
of the first cooling plate element; in accordance with a
preferred embodiment, it is welded to the rear side of the first
cooling plate element as a supplementary section with its
longitudinal edges bent towards the rear side of the first
cooling plate element. To prevent waviness of the edges of the
6
_ ___- _. T ._ _ _.

CA 02440169 2003-09-09
first cooling plate element due to a nonuniform temperature
distribution, it is proposed that slits be produced at regular
intervals in the edge regions of the first cooling plate element
perpendicularly to the longitudinal axis of the cooling plate.
In a preferred embodiment, the free ends of the two joined
cooling plate elements are sealed with caps, and the pipe
sections for the coolant intake and discharge extend through
bores in the second cooling plate element on the rear side. To
reduce pressure losses on the water side in the vicinity of the
coolant inlet and outlet, the first cooling plate element, which
is provided with cooling channel recesses, is hollowed out at the
level of the pipe sections, e.g., by milling out the copper. A
ramp-like transition from the inlet and outlet regions that have
been enlarged in this way to the cooling channel recesses is
produced by gradually reducing the depth of the hollow in the
direction of the cooling channel recesses. The reason for the
smaller pressure losses is the smoother transition that now
exists from the round pipe section to the cooling channel cross
section of the invention with its larger end regions and smaller
center region.
Aside from a flange-and-bracket connection for mounting the
7

CA 02440169 2003-09-09
cooling plate on the furnace wall of the shaft furnace, it is
proposed that the cooling plate have at least two suspension
points, such that a ffirst suspension point is designed as a fixed
connection in the upper part of the cooling plate, preferably
above the pipe section to the coolant inlet or outlet, and a
second suspension point is designed as a loose connection in the
lower part of the cooling plate, preferably just above the pipe
section to the coolant inlet or outlet. This advantageous
suspension with loose attachment points, which are preferably
designed as hangers, allows the lower part of the cooling plate
to undergo thermal expansion.
Further details and advantages of the invention are evident
from the dependent claims and from the following description, in
which the embodiments of the invention illustrated in the
drawings are explained in greater detail. In this regard,
besides the combinations of features enumerated above, features
on their own or in different combinations are also intrinsic
parts of the invention.
Figure 1 shows a cross section of a cooling plate in
accordance with a first embodiment.
Figure 2 shows a cross section of a cooling plate in
8
_-_ _.r ___

CA 02440169 2003-09-09
accordance with a second embodiment.
Figure 3 shows a preferred design of a second cooling plate
element in accordance with Figure 2.
Figure 4 shows a longitudinal section of a cooling plate
mounted on the wall of a shaft furnace.
Figure 5 shows a partial segment of a longitudinal section
of a preferred design of a first cooling plate element in
accordance with Figure 1.
Figure 6 shows a side view of a cooling plate with a
preferred design of the first cooling plate element.
Figure 7 shows a segment of a cooling system mounted on a
furnace wall.
Figure 8 shows the longitudinal section A-A of a cooling
plate in accordance with Figure 7.
Figure 9 shows an enlarged view of the upper partial segment
shown in Figure 8.
Figure 10 shows enlarged views of the partial segments shown
in Figure 8.
Figure 1 shows a cooling plate 1 or stavelet with a first
cooling plate element 2 facing the inside Oi of the furnace and a
second, rear cooling plate element 3, which are welded together.
9

CA 02440169 2003-09-09
The weld seams 4 are located on the protected, cold side of the
cooling plate or stavelet. Between the rear, water side 5 of the
first cooling plate element 5, which is designed as a rolled
copper bloom, and the water side 6 of the second cooling plate
element 3, a cooling channel 7 is formed, which is supplied with
a coolant, preferably cooling water. Pipe sections 8, 9 for
water intake and discharge are mounted in bores in the second
cooling plate element 3. The cooling plate 1 is mounted on the
furnace wall 10, for example, by means of a flange 11, which is
inserted into a bracket 12 mounted on the furnace wall and
secured by a bolt 13 (see Figure 4). The first cooling plate
element 2 is designed as a massive bloom with a plane -- in the
sense of being noncurved -- front side 14, in which grooves 15
are produced, which run transversely to the longitudinal axis of
the cooling plate 1 and facilitate the application of refractory
ramming mix or injection molding compound after completion of the
mounting.
Two recesses 16, 17 that run parallel to the longitudinal
axis of the cooling plate 1 at some distance from each other are
produced on the rear, water side 5 of the first cooling plate
element 2 or shield. Each of these recesses has a more or less

CA 02440169 2003-09-09
semicircular cross section. The cooling channel 7 is sealed on
the rear side, i.e., towards the furnace wall, with an
approximately plane or slightly outwardly curved second cooling
plate element 3 as a supplementary element. This results in the
formation of a cooling channel 7 with a cross-sectional area,
such that the end regions 18, 19, as viewed along the
longitudinal extent of the cross-sectional area (x-direction),
have a larger cross-sectional area than the center region 20.
Figure 2 shows another preferred embodiment of a cooling
plate 101 with a cooling channel cross section claimed in
accordance with the invention. In this embodiment, the desired
cross section of the channel 107 -- here the cross section
perpendicular to the longitudinal axis of the cooling plate -- is
determined by the shape of the second cooling plate element 103,
which is shaped to form a double trough. The desired cooling
channel cross section with larger end regions 118, 119 relative
to the center region 120 of the cross section is created by the
curvature of the troughs 121, 122 and the formation of a center
region 123, which, in the case shown here, is short, but may also
be longer.
To achieve mechanical stability of a cooling plate 101 of
11

' ~ CA 02440169 2003-09-09
' , , _ , ,
this type, the trough-shaped second cooling plate element 203 or
the copper sheet is reinforced, i.e., made thicker, in its edge
regions 324, 325, as shown in Figure 3. This may be
accomplished, for example, by roll forming.
Figure 4 shows the longitudinal section of a cooling plate 1
in its mounted position on the furnace wall, for example, the
wall of a blast furnace. After the cooling plate has been
secured by the flange-and-bracket principle, the remaining space
between the cooling plate 1 and the furnace wall 10 is filled
with backfill compound 26. The pipe sections 8 and 9 are welded
(27) with the second cooling plate element 3. The free ends of
the cooling channel 7 are sealed by caps 28, 29.
Figure 5 shows another preferred embodiment of the cooling
plate 1 based on the embodiment shown in Figure 1. The massive
first cooling plate element 1 is further hollowed out (hollows
30) in the regions facing the pipe sections 8, 9 for the water
intake and discharge, so that the inlet and outlet regions are
enlarged. This cross-sectional enlargement is gradually adapted
-- in ramp-like fashion -- to the curvature of the cooling
channel recesses 16, 17. This has the positive effect of
reducing the cooling water pressure losses.
12

' CA 02440169 2003-09-09
Due to the fact that the second cooling plate element 3 is
mounted on the rear side of the first cooling plate element 2 in
such a way that the edge regions 2a, b (or fin regions) are not
covered, there is the danger of waviness developing in the first
cooling plate element. This is prevented by producing slits 31
in the edge regions 2a, b transversely to the longitudinal axis
of the cooling plate. These slits extend from the edge 32
approximately as far as the second cooling plate element 3. The
slits allow the edge regions to undergo thermal expansion without
stress when the furnace is charged.
The cooling plates of the invention are combined into a
cooling system. For example, they may be installed immediately
adjacent to one another, and their stability can be supported by
a spring-and-groove principle in the first cooling plate
elements. Alternatively, the edge regions of the first cooling
plate elements can also be installed in overlapping fashion.
Figure 7 shows a segment of this type of cooling system 33,
which comprises several cooling plates 1 or stavelets. Figure 7
also reveals another preferred system for mounting the stavelets
on the furnace wall 10. To this end, each cooling plate 1 or
stavelet has several suspension points 34-39, six each in the
13

' ' CA 02440169 2003-09-09
present case, such that the two upper suspension points 34, 35
are designed as fixed suspension points, and the suspension
points 36-39 located below them are designed as loose attachment
points.
A fixed connection between the cooling plate 1 and the
furnace wall 10 is produced at the fixed points 34, 35 (see
Figure 8 and especially Figure 9) by screwing in a screw 40 from
above. For this purpose, a projection 41 is attached --
preferably by welding -- to the furnace wall 10, and a
corresponding projection 42 is attached on the rear side of the
cooling plate 1 outside the region of the cooling channel. The
projections have aligned bores, through which the screw 40 is
inserted to join the two projections. The loose attachment
points 36-39 have a design comparable to that of a door
suspension, as is shown in detail in Figure 10. For this
purpose, at suitable places on its rear side, the cooling plate
has projections 43, each of which is provided with a bore. Each
of the projections 43 is suspended on a pin 44, which is held by
a projection 45 extending out from the furnace wall. These loose
attachment points 36-39 allow the cooling plate 1 to undergo
thermal expansion in the downward direction. To prevent the
14

' ' CA 02440169 2003-09-09
space required for the expansion on the suspensions or loose
attachment points from being blocked by backfill compound, a
throw-away part 46 made of plastic, preferably Styropor, is
inserted at this site during assembly.
All together, the proposed cooling channel cross section
results in a stavelet with optimum characteristics with respect
to the fluid mechanics and cooling effect. In addition, the
stavelet of the invention has advantages over the previously
known stavelet from the standpoint of manufacturing engineering.
Compared to the previously known Cu staves, large savings of
material and weight are realized with these stavelets due to
their smaller thickness, which, in addition, is accompanied by a
greater useful volume of the furnace region.

Representative Drawing
A single figure which represents the drawing illustrating the invention.
Administrative Status

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Event History

Description Date
Time Limit for Reversal Expired 2008-03-25
Application Not Reinstated by Deadline 2008-03-25
Deemed Abandoned - Failure to Respond to Maintenance Fee Notice 2007-03-21
Letter Sent 2006-10-20
Request for Examination Received 2006-09-26
Request for Examination Requirements Determined Compliant 2006-09-26
All Requirements for Examination Determined Compliant 2006-09-26
Inactive: IPC from MCD 2006-03-12
Inactive: IPC from MCD 2006-03-12
Letter Sent 2003-12-12
Inactive: Single transfer 2003-11-20
Inactive: Cover page published 2003-11-14
Inactive: IPRP received 2003-11-12
Inactive: Courtesy letter - Evidence 2003-11-10
Inactive: Notice - National entry - No RFE 2003-11-07
Application Received - PCT 2003-10-01
National Entry Requirements Determined Compliant 2003-09-09
Application Published (Open to Public Inspection) 2002-10-03

Abandonment History

Abandonment Date Reason Reinstatement Date
2007-03-21

Maintenance Fee

The last payment was received on 2006-02-20

Note : If the full payment has not been received on or before the date indicated, a further fee may be required which may be one of the following

  • the reinstatement fee;
  • the late payment fee; or
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Please refer to the CIPO Patent Fees web page to see all current fee amounts.

Fee History

Fee Type Anniversary Year Due Date Paid Date
MF (application, 2nd anniv.) - standard 02 2004-03-22 2003-09-09
Basic national fee - standard 2003-09-09
Registration of a document 2003-09-09
MF (application, 3rd anniv.) - standard 03 2005-03-21 2005-02-23
MF (application, 4th anniv.) - standard 04 2006-03-21 2006-02-20
Request for examination - standard 2006-09-26
Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
SMS DEMAG AKTIENGESELLSCHAFT
Past Owners on Record
DETLEF BIRNBACH
ELMAR KORBIK
PETER HEINRICH
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
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Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
Description 2003-09-09 15 524
Claims 2003-09-09 4 119
Abstract 2003-09-09 2 87
Drawings 2003-09-09 5 73
Representative drawing 2003-09-09 1 4
Cover Page 2003-11-14 1 40
Notice of National Entry 2003-11-07 1 188
Courtesy - Certificate of registration (related document(s)) 2003-12-12 1 125
Acknowledgement of Request for Examination 2006-10-20 1 176
Courtesy - Abandonment Letter (Maintenance Fee) 2007-05-16 1 176
PCT 2003-09-09 8 318
Correspondence 2003-11-07 1 25
PCT 2003-09-10 4 163
Fees 2006-02-20 1 33