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(12) Patent Application: | (11) CA 2636378 |
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(54) English Title: | METHOD FOR THE PRECIPITATION OF NICKEL |
(54) French Title: | PROCEDE DE PRECIPITATION DE NICKEL |
Status: | Deemed Abandoned and Beyond the Period of Reinstatement - Pending Response to Notice of Disregarded Communication |
(51) International Patent Classification (IPC): |
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(72) Inventors : |
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(73) Owners : |
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(71) Applicants : |
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(74) Agent: | EUGENE J. A. GIERCZAKGIERCZAK, EUGENE J. A. |
(74) Associate agent: | |
(45) Issued: | |
(86) PCT Filing Date: | 2007-01-10 |
(87) Open to Public Inspection: | 2007-07-19 |
Examination requested: | 2011-11-15 |
Availability of licence: | N/A |
Dedicated to the Public: | N/A |
(25) Language of filing: | English |
Patent Cooperation Treaty (PCT): | Yes |
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(86) PCT Filing Number: | PCT/AU2007/000013 |
(87) International Publication Number: | AU2007000013 |
(85) National Entry: | 2008-07-07 |
(30) Application Priority Data: | ||||||
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A method (10) for the recovery of nickel and cobalt from leach solutions in
the presence of iron and/or chrome, the method comprising the steps of: i)
adding a reductant (13) to a leach solution containing nickel, cobalt and
iron, such that any iron present as ferric sulphate is reduced to ferrous
sulphate and/or any hexavalent chrome is reduced to trivalent chrome; ii)
neutralising (14) at least a portion of the free acid through addition of a
neutralising agent; iii) further addition of the reducing agent (15) to ensure
all iron present remains in the ferrous form and/or any chrome remains in the
trivalent form; iv) heating the solution prior to mixed sulphide
precipitation; v) adding a mixed sulphide seed (21) and hydrogen sulphide (22)
to effect precipitation (20) of the nickel and cobalt in the form of a mixed
sulphide product (24); and vi) maintaining this mixture in the presence of
hydrogen sulphide (22) for the required residence time to effect complete
precipitation of the mixed sulphide product (24).
L'invention concerne un procédé (10) de récupération de nickel et de cobalt dans des solutions de lixiviation en présence de fer ou de chrome, ledit procédé consistant i) à ajouter un agent (13) de réduction à une solution de lixiviation contenant du nickel, du cobalt et du fer, de manière que toute quantité de fer sous forme de sulfate ferrique soit réduite en sulfate ferreux et/ou toute quantité de chrome hexavalent soit réduite en chrome trivalent; ii) à neutraliser (14) au moins une partie de l'acide libre par ajout d'un agent de neutralisation; ii) à ajouter un agent (15) de réduction afin de garantir que tout le fer présent conserve sa forme ferreuse et/ou le chrome conserve sa forme trivalente; iv) à chauffer la solution avant la précipitation du sulfure mélangé; v) à ajouter un germe (21) de sulfure mélangé et un sulfure d'hydrogène (22) pour réaliser la précipitation (20) du nickel et du cobalt sous la forme d'un produit de sulfure mélangé (24); et (vi) à maintenir ce mélange en présence du sulfure d'hydrogène (22) pendant le temps de séjour nécessaire, afin de permettre la précipitation complète du produit de sulfure mélangé (24).
Note: Claims are shown in the official language in which they were submitted.
Note: Descriptions are shown in the official language in which they were submitted.
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Description | Date |
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Application Not Reinstated by Deadline | 2014-08-20 |
Inactive: Dead - No reply to s.30(2) Rules requisition | 2014-08-20 |
Deemed Abandoned - Failure to Respond to Maintenance Fee Notice | 2014-01-10 |
Inactive: Abandoned - No reply to s.30(2) Rules requisition | 2013-08-20 |
Inactive: S.30(2) Rules - Examiner requisition | 2013-02-20 |
Maintenance Request Received | 2013-01-10 |
Inactive: Correspondence - Transfer | 2012-04-10 |
Letter Sent | 2011-11-29 |
Request for Examination Received | 2011-11-15 |
All Requirements for Examination Determined Compliant | 2011-11-15 |
Request for Examination Requirements Determined Compliant | 2011-11-15 |
Letter Sent | 2009-09-28 |
Inactive: Correspondence - Transfer | 2009-07-02 |
Inactive: Office letter | 2009-05-26 |
Inactive: Single transfer | 2009-04-16 |
Inactive: Cover page published | 2008-10-29 |
Inactive: Declaration of entitlement/transfer - PCT | 2008-10-20 |
Inactive: Notice - National entry - No RFE | 2008-10-18 |
Inactive: First IPC assigned | 2008-08-26 |
Application Received - PCT | 2008-08-25 |
National Entry Requirements Determined Compliant | 2008-07-07 |
Application Published (Open to Public Inspection) | 2007-07-19 |
Abandonment Date | Reason | Reinstatement Date |
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2014-01-10 |
The last payment was received on 2013-01-10
Note : If the full payment has not been received on or before the date indicated, a further fee may be required which may be one of the following
Patent fees are adjusted on the 1st of January every year. The amounts above are the current amounts if received by December 31 of the current year.
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Fee Type | Anniversary Year | Due Date | Paid Date |
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MF (application, 2nd anniv.) - standard | 02 | 2009-01-12 | 2008-07-07 |
Basic national fee - standard | 2008-07-07 | ||
Registration of a document | 2009-07-02 | ||
MF (application, 3rd anniv.) - standard | 03 | 2010-01-11 | 2010-01-11 |
MF (application, 4th anniv.) - standard | 04 | 2011-01-10 | 2011-01-10 |
Request for examination - standard | 2011-11-15 | ||
MF (application, 5th anniv.) - standard | 05 | 2012-01-10 | 2012-01-09 |
MF (application, 6th anniv.) - standard | 06 | 2013-01-10 | 2013-01-10 |
Note: Records showing the ownership history in alphabetical order.
Current Owners on Record |
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MURRIN MURRIN OPERATIONS PTY LTD. |
Past Owners on Record |
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BRUCE JAMES WEDDERBURN |
MICHAEL RODRIGUEZ |