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Patent 1158905 Summary

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(12) Patent: (11) CA 1158905
(21) Application Number: 374857
(54) English Title: METHOD AND APPARATUS FOR THE TREATMENT OF A CELLULOSE- CONTAINING MATERIAL
(54) French Title: METHODE ET INSTALLATION DE TRAITEMENT DE MATIERES A TENEUR DE CELLULOSE
Status: Expired
Bibliographic Data
(52) Canadian Patent Classification (CPC):
  • 92/54
(51) International Patent Classification (IPC):
  • D21B 1/00 (2006.01)
  • D21B 1/30 (2006.01)
  • D21B 1/34 (2006.01)
  • D21D 1/36 (2006.01)
(72) Inventors :
  • SOROKIN, VASILY I. (USSR)
  • ZAROGATSKY, LEONID P. (USSR)
(73) Owners :
  • VSESOJUZNOE NAUCHNO-PROIZVODSTVENNOE OBIEDINENIE TSELLJULOZNO-BUMAZHNOIP ROMYSHLENNOSTI (Not Available)
(71) Applicants :
(74) Agent: SWABEY OGILVY RENAULT
(74) Associate agent:
(45) Issued: 1983-12-20
(22) Filed Date: 1981-04-07
Availability of licence: N/A
(25) Language of filing: English

Patent Cooperation Treaty (PCT): No

(30) Application Priority Data:
Application No. Country/Territory Date
2963339 USSR 1980-07-23
2911021 USSR 1980-04-19
2908425 USSR 1980-04-08

Abstracts

English Abstract


- 34 -
METHOD AND APPARATUS FOR THE TREATMENT OF A

CELLULOSE-CONTAINING MATERIAL

A b s t r a c t

Disclosed is a method for the treatment of a cellulose-
-containing material basically comprising the steps of con-
tinuously charging the material together with the solution
of reagents into a working chamber and repeatedly machani-
cally compacting the same by means of the cooperation bet-
ween an inner and an outer working bodies, the outer working
body enclosing the inner working body and defining in combi-
nation therewith the aforesaid working chamber. The step of
repeatedly mechanically compacting the material is effected
by imparting to one of the working bodies wobbling and roll-
ing over the other working body through a layer of the mate-
rial treated, the aforesaid wobbling and rolling being pro-
duced by the rotation of a mass unbalanced with respect to
the axis of rotation and coupled ratably to one of the work-
ing bodies.
Also disclosed is an apparatus for practising the above
method, which comprises a housing, a rotor made in the form
of a body of rotation arranged inside the housing and defin-
ing in combination therewith a working chamber, a means for
charging the cellulose-containing material together with
the solution of reagents into the aforesaid working chamber,
a drive shaft and its driving gear. Mounted on the drive
shaft are unbalanced masses, 9 while the shaft itself is rotata-
bly coupled to the rotor or to the housing, a portion of
the surface of the rotor being designed for repeatedly mecha-
nically compacting the material treated.
Fig. 1.


Claims

Note: Claims are shown in the official language in which they were submitted.


- 32 -

The embodiments of the invention in which an exclusive
property or privilege is claimed are defined as follows:

1. A method for the treatment of a cellulose-containing
material, comprising the steps of:
- continuously charging the cellulose-containing mate-
rial together with a solution of reagents into a working
chamber defined by an inner working body and an outer work-
ing body enclosing the same;
- repeatedly mechanically compacting the cellulose-con-
taining material;
- said step of repeatedly mechanically compacting the
cellulose-containing material being effected by imparting
to one of said working bodies wobbling and rolling over the
other working body through a layer of the cellulose-contain-
ing material treated;
- said wobbling and rolling being produced by rotating
a mass unbalanced with respect to the axis of rotation and ro-
tatably coupled to one of said working bodies.
2. An apparatus for practising the method of claim 1,
comprising:
- a housing;
- a rotor arranged inside said housing;
- said housing and said rotor defining in combination
a working chamber;
- a means for charging the cellulose-containing mate-
rial together with a solution of reagents into said working
chamber;
- a drive shaft with a driving gear;
- unbalanced masses mounted on said drive shaft;

- 33-

- said drive shaft being rotatably coupled to said rotor;
- said rotor being made in the form of a body of rota-
tion, a portion of the surface of which is intended for re-
peatedly mechanically compacting the cellulose-containing
material.
3. An apparatus for practising the method of claim 1,
comprising:
- a housing;
- a rotor arranged inside said housing;
- said rotor and said housing defining in combination
a working chamber;
- a means for charging the cellulose-containing mate-
rial together with a solution of reagents into said working
chamber;
- a drive shaft with a driving gear;
- unbalanced masses mounted of said drive shaft;
- said drive shaft being rotatably coupled to said hous-
ing;
- said rotor being made in the form on a body of rota-
tion a portion of the surface of which is designed for re-
peatedly mechanically compacting the cellulose-containing
material.
4. The apparatus of claim 2, wherein said rotor is
coupled to said housing via a spherical joint, said drive
shaft with said unbalanced masses is mounted on bearings
inside said rotor the outer lateral surface of said rotor
being designed for repeatedly mechanically compacting the
cellulose-containing material.

5. The apparatus of claim 3 wherein said drive shaft
with said unbalanced masses is mounted on bearing in a
casing, said casing is rigidly coupled to said housing,
said rotor is made in the form of a hollow cylinder and
arranged inside said housing so as to be freely rotatably and
radially movable, the outer lateral surface of said rotor
being designed for repeatedly mechanically compacting the
cellulose-containing material.
6. The apparatus of claim 2 wherein said rotor is made
in the form of a hollow semisphere having its edges bent
outwardly, said means for charging the cellulose-containing
material together with a solution of reagents into said
working chamber is rigidly coupled to said rotor, said hous-
ing is provided with a bottom and a stop member for said
rotor, said drive shaft is made hollow and mounted in bear-
ings on said means for charging the cellulose-containing ma-
terial together with a solution of reagents into said work-
ing chamber, said outwardly bent edges of said hollow semi-
sphere being designed for repeatedly mechanically compacting
the cellulose-containing material.



34

Description

Note: Descriptions are shown in the official language in which they were submitted.


a~90~
~E~HOD AND ~PPARA~US FOR T~E TREA~E~T
0~ A CE~LULOSE-CO~AI~ING MA~ERI~
~ he present inve~tion r~latas in ge~eral to the produc-
tion of *ibrous intermediate products for the manufaature of
paper a~d car~board, or produots of chemical pulp processing.
Mor0 sp0cifically, it relates to methods and appara-tus for
the treatment of a cellulo~e-containi~g material.
~ he present inve~tion can be utilized to the utmo~t
advantage i~ the pulp and paper industry~
~ he propo~ed method and apparatus can be utilized fox
accompli~hiDg a number of important productio~ operation~ i~
the manufacture of pulp a~d paper~ this being do~e by far
more e~ficiently than with the know~ methods and apparatu~O
Such operation~ invol~e th~ impr~gnation of commi~uted ~ege-
table raw material, such as wood chips, with a solution of
cooking reagents, tha cooking o~ impregnated stock in the
productio~ of pulp, the ~eparation of chemically o~ thermo-
.:. chemically treated vegetable raw material into ~iber bund-
les or individual ~ibers and th~ g~i~ding o~ ~iber in the
manufacture o~ paper and cardboard.
~ urthermore, the proposed method and apparatus ~re suit-
able fox application L~ other industrles proces ing Yegetab-
le raw materials, for example, i~ the hydrolysi~ industry
for achiavi~g the improved impregnatio~ o~ a mat~rial with a
solution o~ acid prior to its hydrolysis.
Known i~ the prior art are ~umero~s methods for the
treatment o~ cellulose-c~tai~ing mat~rials, i~volving a


3~



:

- ~ 158~
~ 2 --
mecha~ical impact on the material i~ the process o* treat-
ment. ~his mechanical impact o~ -the cellulose-containing
material treated is effected wi-th a view to i~t~n~ify the
impregnation o~` the oomminubed ve~etabl~ raw ma-terial wi~h
a solution o~ cooki~g rea6snts or for the gri~din~ o~ fibro-
us materials in th~ production o~ paper and ca~dboard there-
from.
For example, known is a m~thod of treatment (see ~RG
Patent ~o. 2,818~320, U.S. Pa-tent No~ 3575791, UOS~S~
ventor's Certificate ~o, 506671) rasidi~g in the si~gle-
-step compactio~ of wood chip~ with the subseque~t submer-
sio~ thereof i~to a s~lution of reage~ts. ~or the implemen-
tatlon o~ this method us~ is made o~ a conical screw extrud-
ar by means o~ which th~ chips are compacted and o~truded
into ~essels containi~g the solution of reage~ts. ~he above
method of treatment and the apparatus, emplo~ed pximarily
~or the impreg~ation of wood chips with th~ solutio~ o~
cooking reagents, ~xhibit-the ~ollow~g disadvantagesr
. The singl~ step compressio~o~ the chips i~ ths sore~
extruder ~orces to arrange seq~e~tially a ~ew ~crew e~brud-

ers Sfrom three to:$ive) so as to ob~ai~ ~he uni~ormi~y o~impregnation, which makes the meth~d u~necessari~y ~omplex
and cos~ly and call~ for co~siderabla operati~g area~.
~ e number o~ chips compression cycles lLmite~ by t~e
~umber of screw e~truders ¢ompel~ to inc-xease ex~essivel~
th-e force of compression, which results i~ tha sig~ificant
deformatio~ and destructio~ o~ the c~ip~ a~ well as in the
d.amage o~ the pulp fibers.

,, Xl~
~ 3 --
The cansiderable compression ~orces applied~ the rigid
coupling betw~en the housin~ a~d th~ screw, and -the repeated
effectuation of compaction laad to the substantial expendi-
ture of electric powar~
Unoriant~d position o* ths chips in the screw extruder
in relation -to the compressing sur~ces also results in the
damage of the pulp ~ibers and i~ the impaired quality of a
finished product.
So~.o~the ~or~going disadvantage~ o~ the ab~ve method
and apparatus ha~e be~n obviated in a method and apparatus
for the treatment of a cellulose-¢ontaining material disclos-
ea i~ ~ranch Pat~nt No. 2,276,420. ~his method en~isages tha
single-~tep passage of chips together with a solution of
reagents between two pre~ i~g rollers rota~ing in opposite
directions at egual speed~. As compaxed to the above-consid-
ered mathod~ this method a~d apparatus ensure an oriented
po~ition of the chips in the process o~ treatme~t~ due to
which the chips are subjected to the compression b~ the ~ol-
lers in the optimum direGtion acros~ the ~ibers.
However~ in conseç~uence o~` th2 single-step compactiQn
o~ the chips, the ~orce o~ compression betw~en ~he rollers
for the unifo~mity of impregnatio~ should be so great that
the chips are i~evitabl~ c~ushed, which res~lt~ i~ the se
vere damage of the pulp- ~iber~ a~d, th~refor~, the paper
a~d cardboard produGed therefrom exhibit a l~w degree o~
mechanical ~tre~th.
~ he disadva~tages i~here~t in ~he abo~e-considered me-
thods and apparatus for the treatmQ~t o~ cellulose contain-


~ ~58~

ing materials have been ellminated to a con~iderable exten~in a methcd a~d apparatus ~or the treatment of fibrous ma-
terials discloæed in U.S.S.R~ InYentor's Certificate
~o. ~12808, which is used mai~ly for the impregnation or
grindi~g of ~ibrous wood materials. This method, identified
as prototypal, features the repeated mechanical compaction
of the material, such as wood ¢hips, supplied into the ap-
paratu~ togeth~r with a solutio~ of reagents. ~he method is
carried out in the apparatus compri~i~g a housing, a rotor
arra~ged insid~ the housing, a means ~or chargi~ the mate-
rîal treate-d a~d the solubio~ o~ reags~ts into a worki~g
chamber9 a drive shaft ana its driving gear. ~he dri~e sha~t
is ri~idly coupled to the rotor, while the rotor supports
compressing rollers mou~ted in carriers in a ~`ew rows. ~he
l~teral sur~ace o~ compr~ssing rollers aLd the i~ner sur~a-
ce of the housi~g serve ~or the repeated mechanical co~pac-
tion o~ the material treated.
Although such a treatme~t method is v~ry clo~e to the
optimum o~e, yet the method it el~ and the app OE atus for the
imple~entation ~hexeof have been found to di~pla~ a number
o~ disadvanta~es impairi~g the efficie~cy o~ treatme~t as
well as the quality o~ ~the product obtained.
Go~sidering that the diameter o~ the rolleræ is smallor
by a~ order of magnitude than the i~er diameter of the hous-
ing, the compxession of the material~ ~uch as wood chips,
takes place ununiformly over ~heir e~tire area~ particularly
at ths starting mome~t of co~act between the chips and ~ha
roller. Moreovsr, i~ o~e admits that the roller rollæ o~er

5~5
-- 5 --
the housing and the chips without slipping~ then it should
rotate around its axis with an an~ular speed which is al~o
~reater by an order of magnitude than the rotational speed
of the rotor and it~ value ~hould reach about ten thou~and
revolution~ p~r minute, thi~ bein~ un~easible for the desc-
ribed apparatus. Hence~ the roller will be unavoidably ~iv-
e~ to slippi~ with respect to the s~r~ace o~ th~ housing
a~d o~ the ~hips, thus resulting i~ -their abrasion. A cer-
tain amount of the chips treated findi~g their way into the
free space betw~en the adjacen-t roller~ is forc~d i~to rota-
tion by the rotor and upon i~teractio~ with the chips rema-
ini~g motionl0~s with respect to the housing undergoes ab-
rasion and destxuction. Additional destruction of the chips
is caused by the action o~ the carriers coupling the roll-
ers to the rotor.
~ hus, the above m~thod a~d apparatus ~or the treatme~t
o~ cellulose-containing materials su~er ~rom the following
disadvantages:
- the u~uni~oxmity o~ distribution o~ the compressin~-
~orce over the antire area of the wood ~chips leadi~g to
the ob~6ctio~able eo~ce~tratio~ of force at the poi~ts o~
eo~tact bstwee~ the c~ip~ and the roll~r and to the destruc-
tion o~ tha pulp fibers;
- the slipping of th~ rollers o~ the sux~ace o~ the
chip~ leadi~g to ~heir abrasio~;
- the de~tructio~ and abrasion o~ the chips pe~etrat
ing into tho ~pace betwee~ the ad3acent rollers a~d forced
i~o rotatio~ by -the rotor upon th~ir i~taractio~ with ~ha
~otionless chip3:

~ 1~8~
-- 6 --
- the destruction o~ the chips by the ¢arriers coupling
~he rollers to the rotor.
~ 11 this, as veri~ied by ts~ting, lead~ to that ths
mechani¢al treatment o~ the cellulose-co~t~ining material
i~ accompanied by the destru¢tion o~ a~ average o~ 27% of
the material treated.
Furthermore, it ~hould be noted that the apparatus in-
tended for tha împlementatio~ of the method de~cribed ~erein-
above has a~ inade~uate output. ~his stems from the ~act
that the total sur~ace o~ the compre~sing rollers participat-
i~ in the mechani¢al compactio~ o~ the material treated i3
considerably smaller than the i~ner surface of the housing
of the apparatust which also cooperates in the m~chanical
compaction o~ the materialc
It i~ an obaect of the prese~t inventio~ to improve the
quality of tho cellulose-co~taining material obtai~ed after
the treatment.
A further obje~t o~ the present invention is to step
up tha output of the appa~atus for the treatm~nt e~ a cellu- -
lo~e-contai~i~g material.
With these a~d other objects in view there is provided
a ~ethod for the treatment o~ a cellule~e-centaining mater-
ial~ ¢omprisl~g the stepæ of oontinuou~ly char~ing the s~me
together wit~ a solutio~ o~ ~aage~tæ i~o ~ workL~g chamber
a~d repeatedly ~echanically compaGti~g it by mea~s o~ the
cooperation b~tween a~ in~er a~d a~ outer workin8 bodi~s

1~89
-- 7 --
caused. to move in relation to each o-ther~ the outer working
body enclo~ing the inner working body and defining in combi-
nation therewith the a~oresaid working chamber, wherein,
according to the invention, t~le repeated mechanical compac-
-tion o~ the material is e~`fected by imparting wobbling mo-
tion to one ol` the wo.rking bodies and by rolJ.ing it over the
o-ther working body through a layer o~ the material treated~
said wobbling mo-tion and rolling being caused by the rotation
o~ a ma>ss being unbalanced with respect -to -the axi~ o~ rotation
and rota~a~ly coupled to one of -the working bodies.
Due to such a design during the wobbling and rolling
of' one o~` the working bodies over the other the material
treated is subjected to the repeated coll~pac-tion across the
f'ibers in the solution o~ reagents wi-thout the occurrence o~
mechanical impacts causing its abrasion or cuttingO ~his
improves -the q~ality of the cellulose-containing material
obtained a~ter the treatmen-t.
With these and other objects in view,-there is al~o provi-
ded an apparatus ~or the implernenta-tion of -the above method
comprising a housing,a rotor arranged i~side the housing and
constl-tuting in combination therewith a working chamber, a
means for charging the material together with a solu-tion o~
reagents into the working chamber, a drive sha~t and. i-ts
driving gear, wherein, according to the invention, the ro-
tor is made in the f'orm o~' a body of' rotation~ a portion of'
the surf'ace o~ which is intended ~or the repeated mechanical
compaction o~ -the material treated, while -the drive sha~t



~ .,

1 ~890~ -
-- 8 --
has unbalanced masse~ mou~ted thereupon and the shaft itsel~
i8 rot~abl~cou~ to the rotor or to the housing.
Due to ~uch a desig~ the rotation of -the dri~e shaft
provided with the unbala~ced mas~es creates a centri~ugal
force which cause~ the housing or th~ rotor coupled to the
drive sha~t via bearings to execute wobbling, as ~ result
of which the working ~urfaces o~ the housing a~d o~ the ro-
tor are brought in contact and rolled without slipping over
the layer of the material -treated in the worki~g chamber.
Hence, the material is arra~ged i~ parallel with the worki~g
surfaces and subjacted to the repeated mecha~ical compac-tion
across t~e ~ibers in the solutio~ o~ reagents wi~hout the
occu~cy o~ mecha~ical impaots bri~gi~g about the abrasion
or cutti3g of the pulp fiber~, which improves the ~uality ~f
the treated cellulose-co~taining material.
~ urthermore, due bo such a desig~ all o~ the material
bein~ inside the working chamber of the apparatus is subje-
cted to the repeated meaha~ical compaction, which increases
i~s output~ `
It is expedie~t that tho dri~e sha~t bogether with the
u~bal~ced mas~es ba mounted~ o~ baari~ side the rot~r
which in turn ba ~oupled to ~e ~ousi~g ~ia a spherical
joi~t" the lateral surfac0 of tha rotor beî~g intended ~or
the repeated mecharlical impact on the ma~erial treatad,
D~e to sllch a desig~l the e~ire struGtu:ee of tha appa-
ratu~; is made ~ompact. ~oreo~er, the arra~g~ment OI th~
balanced ma~sss i~side the ro~or precludsæ the a~pearaIlce
OI bendir~ mome~ts which might have o¢c~red had the ImbalarL-


1 1~8905
9 _
ced mass~s been arranged outside ths rotor and the dri~e~haft coupled to the rotor.
It is also expedient that the drive shaft together with
the unbalanced masses be mounted on bearings in a ca~ing
rigidly ooupled to ~he hou~ing, while the rotor be made in
the ~orm of a hollow cylinder a~d arranged inside the hous-
ing so as to be freel~ rot~.abl~. ~ mova~la radially, the la-
teral outer surface of the rotor being intended for the re-
peated mechanical impac~ on the material treatad.
Such a de~ign sîmplifies the ~tructure o~ the apparatus
and i~proves its operational re~iability since the rotor i~
this case i9 quite simple in design and has not ~y mec~ani-
cal coupli~gs with t~e housing, the relia~llit~ of which
with the presence o~ alter~ati~g loads is reduc~d~ ~urther-
more, tha free arrangement o~ th~ rotor i~ide the housing
en~ure~ that the compres~in~ ~orce acti~ on the matexi~l
treated is consta~ along the len~th of ~he rotor.
It is expedient that the rotor be made in the ~orm o~ a
hollow semisphere having its edges be~t outwardly~ a~d b~
ri~idly coupled to the means ~or charging the tr~ated mater-
ial toget~er with the solutio~ of reage~t~ into the worki~
chamber, ~a housing be providsd w~th a bottom and a stop
member ~or the rotor, ~hile the dri~e sha~t be mad~ hollow
and mounted on bearings on the a~oresaid mea~s for c~argi~
the material trea~ed, the be~t edge3 o~ tha semisphere bei~g
inte~ded for the repeat~d mechanical compaction o~ t~e mate-
rial treated.

1 15890~
-- 10 --
Due to such a desig~, to ~he shapa of the ro~or and
th~ provision of th~ bottom in the housi~g, the treatment of
the cellulos~-containing material is e~fected with its comp-
lete submexsion in the ~olution of reagent~, which ha~ a fa-
vorable e~ect on the quality o~ the treated cellulose-con-
taining material.
~ he objects as well as the ad~antages of the present
invention will become more appare~t from a con~ideration of
speci~ic embodime~ts thereo~ gi~e~ hereinbelow by way o~
example~ with re~erence being made to the accompanying draw-
ings, i~ whi¢h~
~ ig 1 illustrates schema~ically in longitudinal ~ec-
tion the proposad apparatus ~or the impleme~tation of the
mathod for the trea-tment o~ a cellulose-containing material,
according to the inv~ntion;
~ ig. 2 illustrates another e~bodiment o~ the proposed
apparatus; a~d
Fig, 3 illustratas sti}l another embodLme~t of the pro-
posea apparatus.
~ he proposed method is oarried out as ~ollows~
A callulo~e-containi~g material, such as wood chips,
is ~uppliod together with the ~olu~ion o~ reage~t~ i~to a
-
worki~g chamber reprsse~ting a~ annular ~pace betwQen a~
inner working bod~ and a~ outer working body embracing the
material. One of the working bodi~s i5 caused to wobbl~ and
to roll over the other worki~g bod~ through the layer of
the material treated i~ide the working chQmber. ~he wobbl-
ing nd rolling of on~ o~ the working bodi~s over t~e other

i~ en~ured by the rotation of a mass being unbalanced with
respect to the axis of rota-tion a~d~a-ta~y coupled to one
of the working bodies. ~he rolling of one worki~g body over
the other ~s a¢complished at that without slipping, as a re-
sult of which duri~g tha repeated mechanical compaction of
the material treated are e~oluded the forces causing its
abra~ion a~d destruction o~ the pulp fiber~O Due to the co~-
tinuous wobbling and rolling of one working bodg over the
other~ the woo~ chip~ e~tering the working chamber are ar-
ran~ed in parall~l with the surfaces of ~he working bodies
and subjacted to the mechaniaal compaction acros~ the fibars,
which is the optimum condition ~or obtaining the treated pro-
duct of superior quality. I~ the treatment process during
the time spe~t by the material treated inside the working
chamber in the aYerage from 5-to 30 second~ it is subjected
to ths compactio~ a few hundrod times. In order to a~sure
this, tha unbalanced mas~ inducing -the wobbling a~d rolling
of one working body over the other i~ causad to rotate at a
speed o~ about 10 to 50 revolutions per seeo~d.
The force of compression i5 chosen depe~di~g on the
purpose o~ treatment withi~ th~ range from a minimum value
not causing the commi~-tio~ o~ the material to a value ~u~-
~icie~t fo~ grindi~g the material. In each speGi~ic casa ac-
couat i~ take~ o~ ths purpo~e o~ treatm~t a~d of the phyæi-
cal and mscha~ical propsrtie~ of t}le material u~der treat-
me~t7 ~or example, the type o~ waod or other ~e~etable raw
material a~d the nature 9~ a precedi~g treatm~t. The
adjustment of -the compre~sio~ ~orce i~ ~imple and can be

89~
- 12 -
made by varying the speed o~ rotation of the unbala~ced
mass and its sccs~tricity.
The residence time of the material undar treatment in-
side the working chamber depends essentially on the ratio
of the material supplied ~or treatment and the solution o~
reagent~, ~he ratio, commonly ¢hosen from 1 to 3 to 1 to 20,
is u~ed for controlling the re~idence tlme o~ the material
treated in~ide the working chamber.
~ he treated material being under the ac-tlon o~ gravity
~d carr~ed by the solutio~ of reage~t~ entari~g simultane-
ou3ly moves inside the working c~ambar a~ the treatment pro-
cee~s and becom~s discharged there~rom~
~ he method for the treatmen~ o~ a cellulose-containing
mat0rial practiced according to the present i~ve~tion and
compri~ing t~e repeated me¢ha~ical compactio~ o~ t~o mate-
rial i~ the solution o~ reagents allows to increase the e~-
~icie~ey o~ the following operation~ in the ma~ufacture o~
pulp ~nd paper~
- the impregnatio~ o~ wood chips with the solution o~
cooking reage~s;
- the separation o~ tha vegeta~le ra~ material ~ub~e-
cted to chemical or thermochemica} processing in~o fiber
bundles or individual ~ibers;
- the gri~di~g of the fibro~s material ~or the produc-

.




tio~ of paper.
~ he results of the treatme~t of cellulose-co~aining
materials ar~ determined b~ the object pur~ued and al30 de-
pend on the type o~ a star~i~g material (for exampley the




:

1 1~89~5
_ 13 --
~ype o$ wood), the na*ure o~ a preceding treatment gi~en to
the material proc~ssed, and on the ¢onditions o~ carrying
out the treatment accordi~g to thi~ method.
~ he rep~ated meahanical compaction o~ the wood chips in
the solution of reagents accomplished according to the pres-
e~t invent-ion leads to remo~al of the air and moisture from
wood capillaxies at the mome~t oY the compaction of the
chips, and to absorption of the solution of cooki~g reagents
by the capillaries released at the mome~t o~ a pressure re-
lief. D~e to such a treatment ~hexe is achieved the impreg-
~ation of the wood chlps with the solutio~ o~ cooki~æ reag-
ent~.
As compared to other known methods for the impregnation
of wood chips with -the use of mechanical treatment, the pro-
posed method owing to the repeated cycleæ of compactio~ and
pre~sure relief enables to increase the uniformity and ¢om-
plete~ess o~ the impreg~ation of th0 chips and to reduce
the compressio~ ~orce applied thereto.
It is preferable that the for~e o~ compressio~ during
th~ procedure of impregnation should not e~ce0d the lLmit
of elasticity of the material breatsd, but sometimes i~ the
impregDation o~ a particularly hard-te~turad material (~or
e~mple, birch chips) it is advisable to go somewhat beyo~d
the limit of elasticity o as to ensure ~ull impregnationO
The ar~angement o~ chips i~ parallel to th~ compressiDg
surfaces~ while treati~g them according to the proposed ma
-thod, results ~ot only in that the compressio~ o~ the chips
is alwa~s ef~ected across the ~ibsrs, rather ~han alo~g ~hem,
the latter being the mo3t hazardous direction from the Yi8W-


1 1589~5
- 14 -
point of pulp fibers safety, but also in that -t~is takes
place in the absence of forces causing the abrasion or cutt-
ing of the fibers. All thiæ permits to intensi~-g significan-
tly the impregnatio~ of the chips with the solution of cook-
i~g reagents as well as to improve its uniformity without
damaging the pulp fibers.
Durin~ the treatment process ac¢ompanied by -the numero-
us repati~io~ of compressio~ and pxessule relie~ ¢ycles, the
chips may become partially destroyed~.In this case, however,
the deætr~ction com~s about wnder the action of compression
forces dirscted across the fibe~s, these forces being o~ the
~lighta~ danger from tha ~ie~poi~t of fiber safety. Some
partial destruc~ion o~ the wood chips obser~ed ln experimen-
tal testing of the proposed method was attended b~ the for-
mation o~ longitudinal crack~ in the chips followed by their
di~isi~n into separate "matches" without shortening of the
material and ~ithout the ~ormatio~ of a considerable amount
o~ sawdust.
Owing to that t~e trsatment of pulp materials according
to the proposed method is ~ot accompanied by the destructio~
~ the material there iæ achisved an i~oreas~ in the q~ality
o~ the obtained pulp ai well as saving i~ the electric power
required ~or ~ulfilli~g the treatmsnt process.
~ he applicatio~ of the proposed method for the treat-
ment of a c~llulose-conkai~i~g m~terial makes it possible
not only to e~sure its e~peditious ~nd uniform i~pregnation
with the ~olution o~ chemical~, but al~o ke speed up ¢onsi-
de~ably the succeediD$ proces~ o~ extracti~g pulp from the

~ 15~9~

vegetable raw matsrial, i.e. the cooki~g o~ -~he pulp. ~he
i~tensi~ication of the cooking procedure is sacured due to
the mechanical a~d chemical activation of the starting mate-
tial with respsct to the cooking rea~e~ts. The repeated com-
paction o~ the cellulose~co~taini~ material to~ether with
ths s~lution of chemicals, a~ provided b~ ths propo~ed meth-
od, aGtivates the macromolecules o~ the components in the
vegetable raw ma~erial, resulting in a sub~tantial increase
in their chemical interactio~ with the cooking chemicals.
~he combined impact o~ rapeatedly applied compression ~orce~
coupled wibh the che~ical action o~ the cooking chemicals
leads to that li~nin con-tained in the Yegetable material
becomes oblitsrat~d and dissolved much ~aster than in the
cooking of the material ~ot subjected to th6 mechanical tre-
atment as de~cribed hereinabove. Such a combi~ed impact on
the ~egetable raw material not only accelerates the dissolu-
tio~ o$ ligni~, but also conduces to a reductio~ in the con-
~umptio~ o~ chemicals required for the cookingO O~ing to
this, the applicatio~ o~ the proposed method i~ the manufa-
~cture of pulp allow~ to decrease th~ dura-tion o~ the process
to cut down the con~umption of chemical~ a~d power ~or the
cooki~g and to e~hance the chemical purity of ths pulp obta-

i~edO
A~ wa~ already m~ntioned hareinabove~ the repeated me-
chanical compaction o~ the cellulose-containing material
eYfected according to the prop4sed method ma;y be accompanied
by the separation of the material tr~ated into ~iber bu~dles
or i~dividual fiber~ The desired degxee o~ disi~tegration




.

.

~ 05
- 16 -
o~ the material i8 a-ttained by choosing -the force and frequ-
enc~ o~ the compression applied to the ma-terial or ~y relax-
ing fiber-to-fiber bonds in the cellulose-containi~g mater i
al by means of pretreati~g it with reagents causing the in-
tercellular matter to be~ome partially dissolved or plastif-
ied and tha ~iber-~lber bonds to weaken. ~he separation o~
cel~ulose~con-taining materials into fibers is widely used in
the manufactura of semichemical pulp~ hi~h-yield pulp9 chemi-
-me¢hanical or thermo-chemi-mechanical pulp, as well as in
vari~us stag~-by-stage mathods, e~isti~g or being daveloped~
for producing pulp wit~ the i~tarmediate gri~ding o~ ~he pulp
between the stages of the process~
In bhe overwhelming majority of existing methods for
producing fibrous pulp, the separation of ~egetable materi-
als into ~ib~rs is accompanied b~ grindi~g in cyli~drical,
conical or disk mills of di~ferent designs~ The gr~ding of
the material on a disk mill ~akes placa upon its pa~sage
between two di~ks, one of which is rotati~g a~d the other is
motionless or rotati~g in the opposite directio~ the sur~a-
ce Qf these disks bei~g provided with k~ivss and ~rooves.
I~ the grindin~ process wi~ the use OI k~ife mills the
material sapa:rated is subjected ta the variegat~d actio~ o~
~he grinding tackle, i.e. to the percu~iorl o~ the knives,
~hearing, cuttix~, t~lvisti~g a~d abrasion~ As a result of
this action-o~ the gri~di~ di~ d urlder the ef~ect OI
deIormations occ~g at that" the fibers unde~go damage and
rupture. ~he un~a~orable action o~ the ~ibers is e~anced in
coDseque~ce o~ that the material (chips~grou~d pa~etrates

1 1 5~
_ 17 --
into the space between the grin~i~g disks i~ th~ form of
separate indep~ndent bodies arranged loosely i~ dif~arent
posi~ions and in an unoriented ~ashion with re~pect to the
kniv9s of the ~rinding disks. r~he sharp edges of the knives,
the rigidity of the ~tructure u~ed and the hi~h unit pressu-
re applied to the working surfaces conduca to cutting of the
fibers. ~he use of the fibrous pulp thus obtained in the ma-
nufacture o~' papex and cardboard leads to a considerabla re-
ductio~ o~ the mechanical strength of a finished product.
~esides, thH undesirabla damage of the ~ibers al~o causes
the increased consumption of power raquired for this opera-
tion~ ~he unproducti~e expe~ditures of power in t~e treat-
ment o~ the material o~ the disk mill al~o arise due to im-
mense energy losses for o~ercoming the hydraulic resistance
upon the rotation of the knifa disks and also for the trans-
portation o~ ths material treated.
The struct~re of the kni~e mills in use su~fers from
~nothex es~ential disadva~tage residi~g in the vulnerability
to the penetration o~ axtra~aouæ solid inclusions. The metal
or ceramics findi~g its way into the mill in~lict great da-
mags to the kni~es and may re~der tha mill inoperative. ~he
subseque~ sharpening of the kni~es takes considerable time
resulting i~ the downtim~ of the e~uipment.
~ he optimwm conditions of treating ~egetable material~
accordi~g to the proposed met~o~ can be establi~hed in each
~pecif ic case b~ choo~ing the shape of ths bod~ o~ rotatio~,
by decreasing or increasing the force of cru~hing tbrou~h
the exte~t of the unbalanced mass, the speed o~ its rotation

90.S
- 18 -
or the residence time of the material in the treating zone.
By varyi~g the above conditions or b~ repeating a simi-
lar treatment there can be achieved not only the separation
of the material trea~ed into individual ~ibers, but also en-
sur~d its further grinding to the desired degree o~ fineness.
r~he proposed treatment method can also be employed for
grinding pulp and other ~ibrous intermediate products in the
production of paper therefrom.
~ he treatment of the matsrial according to the proposed
method does not i~volve ths unproductive e~penditures o~ po-
wer associated with the rotation of th~ grinding disks ar-
ranged in pro~imit~to each other and provided with knivas.
~he tra~sportation of the material treated is accomplished
under the ~orce o~ graYity and does not require an~ power
consumption. ~hese adva~tages enable to cut down the con-
sumption of power ~or the treatment.
Ths proposed method for the produc-tion o~ ~ibrous in-
termediate products precludes the harm~ul con~e~ue~ces for
the equipme~t attended by the penetration of e~tranaous- so-
lid objects into the apparatus since in -t~i~ case there is
no rigid coupling between the elements acting o~ the mate-
rial bei~g ~ro~d.
~ he method under consideratio~ will be ~urthex illust- -
rated hereinbelow by its speci~ic embodiments.
xa~e 1
- 2 kg of aspen chip~ were conti~uousl~ charged into the
apparatus and a 14% solu~ion o~ sodium hydroxida in the
weight ratio of 1 to lO was supplied. ~he d~ration o~ the

- alss~o~
- 19 -
continuous charging o~ the chips and the solution amounted
to 2 min. ~he rotation frequency o:E the drive shaft was
1480 rev/min. ~he approximate residence time of the chips in
the working chamber was 15 ~ec and the requlsite average num-
ber of chips oompression cyclos was 370. Su~sequ~nt to the
treatm~nt according to the method, tha impregnated chips
were separated on a screen from ths ~reely dripping solution
~nd a portion thereof was placed i~ an autocla~e and heated
at a temperature of 160 to 165C for 1 hour and a half. ~he
cookad pulp was washed with water~ sorted and air-dried~
The yield and ~uality indexes were determined~
Yield from wood~ % . . . . . . ~ . 50.5
~ignin co~tent, % . . . . . . . . 1.3
Breaking length, m . ~ ~ . . . 0 9170
Folding resistance, nwmber ~
double folds . . ~ . ~ . . . . . 2320
E~ample 2
~ he treatment o~ 2 kg of birch chips was effe~ted as
described i~ Exampla 1 ~imulta~eousl~ ~uppl~ng into tha
apparatus a 16% solution of sodium hydroxide i~ the weight
ratio of 1 to 10. ~he duratio~ of the conti~uous char~ing
o~ the chips and the æol~tio~ was 1 mi~ 40 se~. ~he rotation
~rsq~ency o~ the drive sha~t was 2850 reY/min. ~he appro~lm-
ate residence time o~ the ehips i~ the apparatus wa~ }1 sec
and the requisite avexaga numbar o~ chips compressio~ cycles
was 5500 Subsequent to the treatment according to the method,
the impregnat~d chips wsre separated on a scree~ from ~he
e~ce~s of the solution and a portio~ thereof was subjected

`"` 1~5~
20 -
to cooking in the autocla~e at a temperature of 160 to
165C ~or 1 hnur and a half.
Pulp ~ield, % . . . . . . . . . . . . 48.3
~igni~ co~tent, ~0 . . . ~ . . . 0.8
Breaking length, m . O . . . . . O . 9430
Folding resistance~number of
double ~olds . . . . . . . . . . . 2840
Exam~le ~
Bi~ch chips were preheated with a 2% solution o~ qodium
hydroxide *Qr 1 hour and a hal~ at a temperature of 100C,
wherea~ter the pulp waæ subjected to the repeated mechanical
compactio~ according to the method, substa~tially as describ-
ed in ~xamples 1 and 2. The rotatio~ ~requency o~ the dri~e
shaft ~as ~100 rev/mi~. ~he treatment was repeated 6 times
with in-termediate washing after the ~irst passage, and ~ith
~he extraction of the pulp after tha second3 fourth a~d
sixth pasqage through the apparatus. ~he extracted samples
o~ the pulp were washed and the beating degree a~d mechanic-
al strength i~de~es were determined.
Wood residue yield a~tar ¢hemical
treatment 7 ~ o 9
Indexes ob~ai~ed a~ter the second pass-
ing of the pulp t~rough the apparatu~:
beatin~ degre0 . ~ . . . 23
breaking le~gth, m . . ~ 350
foldi~g~resista~ce, ~umber o~
double folds . . 0 9 . O . . . . 18
bursti~g strength, kg/cm2 ~ . . . 1.5

` ~5~5
~ 21 ~
Inde~as obtained after the fourth pass-
i~g of the pulp through the apparatus:
baating degree . . . . . . . ~ . . . 35
breaking length, m ~ 0 . . ~ . . 0 . 5860
foldin$ resistance, ~umber o~
double ~olds . . r ~ 104
bursting stre~gth, kg/cm2 . . . . . 2.2
Indexes obtained a~ter the sixth ~a~s-
i~g o~ ~he mass through the apparatus:
beating degree . . . . . . . . . . . 60
breaking l~gth~ m ~ . . O . . ~ . . 7020
foldi~g resistance~ number o~
double fold~ . . . . 0 . . . . . . 27~
bursting strangth, kg/cm2 . . . . 2.9
Example 4
Birch chips were pretreated with a 2~o solu~ion o~ sod-
ium oarbonate ~or 1 hour and a half at a tempe~ature o~
100C, wharea~ter tha pulp was subj~ctad to tha repsated
mechanical compaction accordin~ to the method, æubstantial
ly as describad 1~ Example ~.~ he ro~a~i~n ~reque~c~ o~ the
dri~e ~ha~t is 2100 rev/mi~. ~hs pulp was passed through
the apparatuB thr~a:times with i~t~rmediat3 washing~a~tsr
the ~ir~t pa~sLng.
Wood residue yield after chemical
tr~atment~ % ~ . O ~ . 92~1
Beating d~gree . . ~ 0 ~ 30
Braaking le~gth9 m . . . . . . . . . 5550
Foldi~g resistance, n~mber of
double ~old~ ~ ~ . . 0 . . . . . 0 . 73

- 22 -
~earing rssistance . . . . . O . . . . 60
Bursting stre~gth; kg/¢m2 . ~ . . . . 2.2
~3~a~
Aspen chip~ wexe prcaonditioned in a 5% solution of am-
mo~ia ~or 12 hours at room temperat~re, whereafter it was
subjected to the repeated mechanical compaction according to
the method, substantially as de~oribed in Exampl~ 3. ~he
rotatio~ freque~cy o~ the driva sha~-t was 2100 rev/mi~.
Wood residue yiald after chemical
t~eatmen~, % ~ . . . . . . . . , . 0 96.2
Degree of grin~ing~ . . . . . . . . ~ 60
Breaking length, m ~ O . . . . . ~ ~ 6400
~olding resistance~ number of
double folds . ~ . . . . . . . . . ~ 1~2
~aaring resistance~ . . . . . . . ~ 42
Bur3ting stre~gth, k~cm2 . . . ~ . . 2.6
~xa~le 6
~ aqueous suspension o~ unbleached sul~ate pulp was
prepared from pi~e i~ 10% co~centration and pa~s~d through
tbLe apparatus Ior the repeated mecha~ical co~pactio~ accQrd-
i~g to the pr~posed msthod. ~h~ rotatie~ ~requency of the
drire s~aft was 2100 rev/mi~. ~he i~de~ss o~ the mass obtai-
ned after the sixth passi~g through the apparatus ~ere as
~ollow~.
Beating degree . . . . . . . . . ~ . . 48
Breaki~g length, m . . . . . ~ . ~ . . . 9150
~olding resistance, ~umber of
double fold~ . . . . 2890

9~
- 2~ -
Example 7
Bleached pulp cooked in nit.rate was subjected to the
treatme~t according to the proposed me-thod, substantially
as described in Example 6. The indexes of ~he mass obtain~d
a~ter the sixth pas~i~g throu~h the app~ratus wer~ a~ fol-
lows.
Bea-ting dagree ........................ 58
Breaking length, m . . . ~ . . . . . . ~ . 6880
FoldiD~ resistancs, ~umber of
double folds . . . . . . . . . . . . . . 47~
~ he appara-tus for practising the proposed method compr-
ises a housing 1 /Fig. 1/ mounted on a foundation 2 by means
o~ flexible shock absorbers 3. Arranged insids the housing 1
is a rotor 4, which in combination with the housing 1 defin-
as a working chamber 5. ~he housing 1 is provided with a me-
~8 6 for charging the cellulo~e-containing material -togeth-
er with the solution of reagents into the working chamber 5.
~he apparatus also comprises a drive sha~t 7 with unbala~c-
ed masse~ 8 moL~tad thereon so that the eccentricity of
their mass i~ adjustable~ The drive shaft 7 is coupled via
a flexible coupling 9 to a drivin~ gear lO. ~he rotor 4 is
mada i~ the ~orm o~ a bod~ of rotatio~, the o~ter lateral
sur~ace 11 o~ which is i~tsnded for ropflatedly mecha~ic~lly
compacting ~he material u~der trea~e~t~ th~ ~aterial treat-
ment baing dispo~ed between tha ~utor lateral sur~ace 11 o~
the rotor 4 and the inner surfa~ 12~ o~ the housing 1.
According to on~ of the embodiments of tha apparatus,
the rotor 4 is coupled via a hoIlow rod 13 and a spherical




'~ :

~ 1~8~5
- 24 ~
bearing 14 to the housing 1. The drive shaft 7 with the un-
balanced mass~s 8 is mo~nted on bsarings 15 inside the rot-
or 4. ~hus, in this specific embodiment of the apparatus
the drive sha~t 7 with the unbalanced masses 8 is coupled
ta the rotor 4 and due to it~ mou~ting in -the bearings 15
is capable of ~ree rotation with respect thereto~
Accordi~g to a~oth~r embodiment of the apparatus, it
al~o comprise~ the housing 1 /~ig. 2/ mounted on the founda-
tio~ 2 by means of the flexible shock absorbers 3 and incor-
poratin~ therei~side the rotor 49 the aforesaid rotor 4 and
housing 1 de~ining in combi~ation -the working chamber 5,
~ho housing 1 is provided with the means 6 for charging -the
material treated together with the ~olutio~ o~ reagents i~-
to the working chamber 5. ~he apparatus al~o compri~es the
drive shaft 7 with the ~nbalanced masses 8 mou~ted th~raon,
the aforesaid drive shaft 7 being coupled ~ia a flsxible
couplin~ 9 to a driving ~ear 10.
~ partic~lar ~eatur~ of this embodime~t of the appara-
tus resides in that the drive shaft 7 with ths u~bala~ed
masseæ 8 is mounted o~ baarings 15 within a casing 16 rig- :
idly coupled via ribs 17 to the housing 1. Thus, in this
speci~ic embodimant o~ the apparatus the drive sha~t 7 with
the u~bal~nced masses 8 is coupled to the housing 1 and~due
to its mountinæ in the baaring~ 15 i8 capable of ~ree rota-
tion with r~pact th~reto. The r~tor 4 i~ mad~ i~ the form
o~ a hollow cylinder ~hich is freely mounted inside th~
housing 1 a~d supported by th~ ribs 17. Dua to this, the
rotor 4 is capa~le of free rotation and radial moveme~

1 ~5~9
-- 25 _
sid~ the housing 1~ the outer lateral surface 11 of ~he ro-
tor 4 and tha i~ner sur~ace 12 o~ tha housing 1, as in the
embodiment considered hereinabove, being intended for repe-
atedly mechanically compacting the material treated.
Aocording to still another embodiment of the apparatus
and similaxly to its other embodiment~, it also comprises
the housing 1 ~Fig. 3/ mounted on the foundation 2 b~ means
o~ the flexiblo shock absorbers 3. Arranged inside thq hous-
i~g 1 iæ the rotor 4~ the a~orasaid rotor 4 defining i~ com-
bi~ation with the housin~ 1 a workin~ chambor 5. The appara~
tus also compriseæ the drive sha~t 7 with the u~balanced maæ-
s~s 8 mou~ted thereon, the a~ore~aid drive shaft 7 being co-
upl9d to the driving gear 10.
A particular ~eature o~ this em~odiment o~ the appara-
tu~ xesides in that the rotor 4 is made i~ the ~arm of a
hollow semispher~ having its edges 18 be~t out~ardly. The
housing 1 is provided with a bottom 19. ~ou~ted on a cover
20 of the housi~g 1 is a stop member 21 for the rotor 4 hav-
i~g a concave spherical surface. The driv~ shaft 7 with the
unbalanced masse~ 8 is mada hollo~ a~d mounted i~ bearings
15 on the mea~3 6 ~or charging the material trea-ted which~
i~ turn9 is ri~idly coupled t~ the rotor 4. ~hus, in this
specific em~odiment of the apparatu~ the drive shaft 7 with
the unbala~ced masse~ 8 is coupled to the rotor 4 a~d due to
its mou~ti~g i~ the bearings 15 i~ capable of froe rotation
with respect thereto. ~he outwardly bent edges 18 of the se-
misphere serve for repeatedly mechanic~lly compacting the
material u~der treatment whichis dispos~d betwsen the outwar-


a 1589~5
_ 26 -
dly be~t edges 18 of the semisphere and the inner sur~ace 12
of the bottom 19 of the housing 1.
~ he apparatus operates as followsO ~he torsional moment
~rom -tha drivi~ gear 10 /Fig. 1/ via -the flexible coupling
9 and the drive sha~t 7 is -transmitted to the unbalanced
masses 8, who~e rotation produces centrifugal ~orce tra~s-
mitted via the beari~s 15 to the rotor 4, which starts to
deviate from the lo~gitudinal axis of the housing 1 a~d to
per~orm circular oscillating motio~s arou~d the center of
the spherical joint 1~ coupling the rotor 4 to the housin~ 1.
In other words, the rotor 4 is caused to perform wobbli~g
motions. I~ this process the oute~ lateral surface 11 of the
rotor 4 comes in contact w~th the i~ner sur~ace 12 o~ the
housing 1 and the rotor 4 is caused to roll over this surfa-
ce rotating according to the law of pla~tary rotation tow-
ard the side oppo~ite the direetion o~ rotatio~ of its axis
and of the drive sha~t 7 with th~ unbalanced masses 8.
The material to be treated is charged together wi-th the
solutio~ of reagents via the mean~ 6 into th~ working ~hamb-
er 5 of the apparatus, wherein it is arranged in a uniform
layer between the outer lateral surface 11 o~ the rotox 4
and the i~ner suxface 12 o~ ~he housing 1
Due to the annul~r shape o~ the worki~g chambex 5 a~
well as to the wobb-ling motion a~d rolling o~ the rotor 47
the material treated, for example~ wood chip~, is arra~ged
in parallel with the sur~ace 11 o~ the rotor 4 and with the
surface 12 o~ the housing 1~ a~ a re~ult o~ which the ~orc~s
of compres~ion are directed across the ~ibexs and the chips
ara subjected solely to the repeated mechanical compaction.

9~
- 27 -
~ he operation o~ the apparatus according to the embo-
diment illustrated in Fig. 2 proceeds similarlyO ~he dif~e-
rence being in that the centxifugal force arising upon the
rotation of the drive shaft 7 with the unbalanced masses 8
is transmitt~d via the bearin~ 15 and the ribs 17 to the
housing 1 cau~ing its wobbling motions, In othar words, the
hou~ing 1 starts to deviate from the origi~al positio~ and
to perform cir¢ular oscillating motio~. Upon contact of
the inner surface 12 of the housing 1 with the outer later-
al sur~ce 11 o~ the rotor 4, due -to its inertia, it is ca-
used to roll o~er the inner surface 12 of the housing 1~
The operatio~ of the apparatus according to the embo-
dimant illustrated in Fig. ~ pro~eeds similarly to that of
the embodiment illustrated i~ Fig. 1. ~he difference being
in that the ce~tri~ugal force arising upon the rotation of
t~e hollow dri~e sha~t 7 with the unbalanced masse~ 8 is
tra~mitt~d to the rotor 4 via-the means 6 ~ox chargi~g th~
material to be tr~ated to~ether with the solution of reag-
ents into the working chamber 5, the rotor 4 being caused
to roll by the outwardly bent edges 18 over the sur~ace 12
o~ the bottom 19 o~ the housin$ 1, aæ a result o~ which
upo~ c~ar~in~ of the material together wi~h the solutio~
of reagents into ths working chamber 5 the material is
subjacted to the repeat~d macha~ical compaction~
Owing to that in all of the above-co~sidered embodim-
en~s of the apparatus the drive ~haft 7 with the unbala~c~
ed ma~ses 8 ~reely rotate~ o~ tha bearings 15 with respect
to the rotor 4 (~ig~. 1 a~d 3) or with respect to the hous-


8~
- 28 ~
ing 1 ~Fig. 2), the material upon rollin~ of the rotor 4
wer the surface 12 of -t~e housing 19 .i~ subjected solely
to the repeated mechanical compaction without the occu~ence
of an~ ~orces causin~ abra~ion or cutting of the pulp fibersO
~his is attributable to that rolling of thq rotor 4 i~ cau-
sed not by direct tra~smissio~ o~ the torsion~l moment Yrom
the dr~e shaft 7, but results from contact of the housing
and the rotor upon the wobbling motions of one of them un~
der th~ action of the centrlfugal force of the rotati~g un-
balanced mass~s 8. ~his improves signi~icantl~ the quality
of the tr~ated material.
Due to ~hat all oP ths mat~rial disposed in the working
chamber is subjected to the repea-ted mecha~ical compaction,
the output of the apparatus is thereby l~creased.
The forco o~ compressio~ applied by th~ rotor 4 to tha
.. .
layer of the material under treatme~t is governed b~ the
mass of t~e unbalanced masses 8~ by the ang~ular spesd of
their rotation and the eccexLtricit~sr of the mass of ths u~-
balanced mass~s 8 with respect to the axis of thsi:L ro~a-
tio~ and is detexmined from the formula~
m w2 . R
where: m i~ the ma~ OI the ~balanced ma~ses,
w is ~he a~ular ~peed of rotatio~
R is the eccent:~i¢ity o~ the mas~ OI the unbalanced
massas with respact to the axis of rotatio~O
T~e eutput of the ~pparatus a~d the qualit~ of Ehe ma-
terial treatmant depends on tha choice of ths~s p~amoter~.
Dus consideration is also to be gi~en to tha type and pro-


~ 15~9~5
_ 29 _
perti~s of the material -to be treatad. Th~ for~e of compres-
sion i~ this apparatus is readily adju~ted by Yaryi~g the
ecc~ntricity of th~ mass o~ the unbalanced masses 8 and the
a~ular speed of -their rotatlon.
~ or reasons enwmerated hersi~above tho proposed appa-
ratus can be succ~8s~ully exploited ~or the treatme~t of
cellulo~e-co~taining materials ~ith -t~e view of impregnat-
ing them with the solutio~ of cooki~g reagen~s with a grea-
ter or smaller degre~ o~ fiber-to-fibsr bonds relaxatlon~
for ths separation of chemically or thermoch~mically pretre-
at~d materials into fib~r bundla~ or individual ~ibers, or
~or the beating c~ pulp in the pxoductio~ of paper stock.
~ rom the foregoing spacific embod~ments o~ ~he pressnt
i~ve~tion, ~n0 skill~d in the art can easily ascertai~ the
essential characteristics of this inve~tio~9 and with~ut
departing from thq spirit a~d scope ther~of, ca~ make vari- -
OU9 changes and modifications ~f the inventio~ to adap~ it
to various u~ages a~d condi-ti~n Conseque~tly, such chan~-
es a~d modifications are properly, equitably, and inben~d
to b~, within bhe ~ull range o~ ~qui~alence of the ~ollow-
irlg claims.
The advantages of th~ present Lnve~tion, as compared
to all of the prior art msthod~ and ap~aratu~ for the tre~
atment of a csllulose-containi~ material, reside in the
followings
- the propo~qd method and apparatus improve the quali-
ty o~ the tr~ated material, w~ich, i~ tur~, improve~ the
qualit~ o~ thq pulp, paper and cardboard obtained t~r~-
*rom;

i 15890
- 30 -
- the propo~d method a~d appara~u~ enable to dscrease
the co~umptio~ of vege-table ra~ material and chemical re-
agen~s;
- the proposed method a~d apparatus enable to speed !"
up ~he proces~ of pulp pro~uction;
- the propo~ed method and apparatu~ enable to cut down
the con~umption o~ power;
- the propo~ed method and apparatu~ ~eature an increas-
cd output a~d operational reliabllity~
In support of the hig~ afficie~cy inherent in the pro-
po~ed method ~d apparatus there is ~iven hereinbelow a
comparativ~ tablo pre~nti~g the i~dexes of tha pulp pro-
duct~ obtainsd with the u~e of the prasent method and appa-
ratu~ ~ersus those obtainad i~ accordance with the most wi-
dely spr~ad production practice exi~ti~g currently.
~able

Indexe~ Propo~d method ~ tlng methods
~ype o~ wood aspe~ birch birch a~p~n bir¢h birch
Yield ~rom wood a~-
ter chemical treat-
ment, % 96 90 90 90 86 86
:Bsating degrea 60 30 60 60 30 60
Indexes of mechanic-
al s~rength with pa-
per mass o~ 75 g/m ~
breaking l~gth,m 6400 5800 7020 6300 5600 6800
tear resistanc~ 42 60 - 40 45
bursting strength,
kg/cm 2.6 2~2 2.9 2.2 1.9 2.6




.~

9~5
~able (cont.~
IndexesProposed method ~xi~ting methods
~ype of woodaspen birch birch aspsn birch birch
. .
~olding resi~t-
ance, number of
double folds 132 10~ 273 9 12 80
. . . _ . _
Power consump~lon
~or beating to 16
kwhr/t 5 - 7 200 - 400
_ . . . . . . " , . ., _ , ,

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Administrative Status

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Administrative Status

Title Date
Forecasted Issue Date 1983-12-20
(22) Filed 1981-04-07
(45) Issued 1983-12-20
Expired 2000-12-20

Abandonment History

There is no abandonment history.

Payment History

Fee Type Anniversary Year Due Date Amount Paid Paid Date
Application Fee $0.00 1981-04-07
Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
VSESOJUZNOE NAUCHNO-PROIZVODSTVENNOE OBIEDINENIE TSELLJULOZNO-BUMAZHNOIP ROMYSHLENNOSTI
Past Owners on Record
None
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
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Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
Drawings 1994-03-03 2 81
Claims 1994-03-03 3 118
Abstract 1994-03-03 1 67
Cover Page 1994-03-03 1 24
Description 1994-03-03 31 1,535