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Patent 1184765 Summary

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Claims and Abstract availability

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(12) Patent: (11) CA 1184765
(21) Application Number: 424634
(54) English Title: PROCESS FOR MAKING FUEL PELLETS FROM ORGANIC FIBROUS MATERIAL
(54) French Title: METHODE DE FACONNAGE DE BRIQUETTES COMBUSTIBLES A PARTIR DE MATIERE ORGANIQUE FIBREUSE
Status: Expired
Bibliographic Data
(52) Canadian Patent Classification (CPC):
  • 44/34
(51) International Patent Classification (IPC):
  • C10L 5/44 (2006.01)
  • C10F 5/00 (2006.01)
(72) Inventors :
  • RUYTER, HERMAN P. (Netherlands (Kingdom of the))
  • VAN RAAM, LEOPOLD (Netherlands (Kingdom of the))
(73) Owners :
  • SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. (Netherlands (Kingdom of the))
(71) Applicants :
(74) Agent: NORTON ROSE FULBRIGHT CANADA LLP/S.E.N.C.R.L., S.R.L.
(74) Associate agent:
(45) Issued: 1985-04-02
(22) Filed Date: 1983-03-28
Availability of licence: Yes
(25) Language of filing: English

Patent Cooperation Treaty (PCT): No

(30) Application Priority Data:
Application No. Country/Territory Date
8211782 United Kingdom 1982-04-23

Abstracts

English Abstract




A B S T R A C T

A PROCESS FOR MAKING FUEL PELLETS FROM
ORGANIC FIBROUS MATERIAL

A process for producing fuel pellets from organic fibrous
material, in particular pineapple plant waste, which comprises
bruising the material to a maximum particle size of 5 x the
diameter of the holes of the die in the below-mentioned pel-
letizer, whereafter the material is dried to 20-10%w of water on
total material, optionally at least a part of the material is
chopped, and then pelletized in a die pelletizer at a pellet
temperature of 70-135°C.


Claims

Note: Claims are shown in the official language in which they were submitted.


The embodiments of the invention in which an exclusive
property or privilege is claimed are defined as follows:

1. A process for producing fuel pellets from
organic fibrous material, which comprises bruising the
material to a maximum particle size of 5 x the diameter
of the holes of the die in a pelletizer, whereafter
the material is dried to 20-10%w of water on total.
material, and then pelletized in the die pelletizer
at a pellet temperature of 70-135°C.


2. A process according to claim l, wherein at
least part of the dried material is chopped prior to
the pelletizing.


3. A process according to claim l, wherein the
organic fibrous material is mechanically dewatered
to 70-40%w of water on total material at the same
time bruising the material to said maximum particle
size.


4. A process according to claim 2, wherein the
organic fibrous material is mechanically dewatered
to 70-40%w of water on total material at the same
time bruising the material to said maximum particle
size.

- 6 -

5. A process according to claim l, wherein the
organic fibrous material is mechanically dewatered
to 60 to 40%w of water based on total material,
while bruising to said maximum particle size.


6. A process according to claim 2, wherein the
organic fibrous material is mechanically dewatered
to 60 to 40%w of water based on total material,
while bruising to said maximum particle size.


7. A process according to claim l, 2 or 3,
wherein the pelletizing is carried out at a pellet
temperature of 70-120°C.


8. A process according to claim 4, 5 or 6,
wherein the pelletizing is carried out at a pellet
temperature of 70-120°C.


9. A process according to claim l, 3 or 4,
wherein the organic fibrous material is pineapple
plant waste.


10. A process according to claim l, 2 or 3,
wherein the organic fibrous material is maize waste.


11. A process according to claim l, 2 or 3,
wherein the pelletizing is carried out in the pre-

sence of water or steam.

- 7 -

12. A process according to claim 1, 2 or 3,
wherein the pelletizing is carried out to form
pellets having a diameter of 10-20 mm and a length of
20-60 mm.


13. A process according to claim 4, 5 or 6,
wherein the pelletizing is carried out to form
pellets having a diameter of 10-20 mm and a length
of 20-60 mm.


14. A process according to claim 1, 2 or 3,
wherein the bruising is carried out in a roll
crusher.


15. A process according to claim 4, 5 or 6,
wherein the bruising is carried out in a roll
crusher.


16. Fuel pellets produced by the process of
claim 1.


17. Fuel pellets according to claim 16, which
are at least partially carbonized.


18. Fuel pellets according to claim 16, having
a diameter of 10-20 mm and a length of 20-60 mm.

- 8 -


19. Fuel pellets according to claim 17, having
a diameter of 10-20 mm and a length of 20-60 mm.


20. Fuel pellets according to claim 18 or 19,
wherein the organic fibrous material is pineapple
plant waste or maize waste.

- 9 -

Description

Note: Descriptions are shown in the official language in which they were submitted.




A PROCESS FOR M~KING FUEL PELLETS F~OM
ORGP~IIC FIBROUS ~ATFIRLAL

This invention relates to a process for making fuel pellets
frcm organic fibrous material and to fuel pellets thus obtained~
Such processes are already kncwn. Philippines patent 11922
for instance describes a process wherein the moisture content of
ccmminuted fibrous material, such as sawdust, is adjusted to
16-28%w and the material is pelletized at a temperature of
163-177C.
According to the process of the present invention a much
lower pelleti2ing te~erature can be applied.
Moreover it has been found that by bruising the fibrous
material in a crusher, preferably a roll crusher, the cuticles
of the material, if this is of the very wet type such as leaves,
are damaged which results in a reduction of the dryiny time of
80-85% compared with only cutting the material, such as leaves
into pieces.
Furthermore, this bruisiny results in considerable fibril-
lation, which has a favourable influence on the coherence forces
of the p~llets due to entanglement of the fibres.
Thus the present invention relates to a process for pro-
ducing fuel pellets from organic fibrous material, which ccm-
prises bruising the material to a maximum particle size of 5 x
the diameter of the holes of the die in ~he below-mentioned pel-
letizer, whereafter the material is dried to 20-10%w of water on
total material, optionally at least a pc~rt of the material is
chopped, and then pelletized in a die-pelletizer at a pellet
temperature of 70-135C, preferably 70-120C, more preferably
70-100C. ~le pellets may be Eurther dried in the field .
~.


'765

-- 2
If the organic fibrous material is of the very wet type,
such as pine-apple plant waste containing more than 70 %w of
water, the material is mechanically dewatered to 70 40 %w, pre-
ferably 60-40 %W, of water on total material at the same ti~
bruising the ~aterial -to said maximum particle size. This
mechanical dewatering is not necessary if the material has a
moisture content up to 70 -OW, e.g. 30-60 %w, such as certain
types of wood waste, e.g. mixtures of sawdust, bark fibres and
bark chips.
Preferably the bruising is carried out in such a way that
the particle size of the material shows some variation. The
s~aller particles then fill the voids between the larger par-
ticles, resulting in a lower pelletizing energy and a still
better entanglement of the fibres.
If desirable, water or steam may be used during the
pelletizing to facilitate the pellet-formation, e.g. 3-5 %w of
water or steam.
Suitable diameters of the holes of the die pelletizer are
in the range of from 5-30 mm.
The pellets preferably have a diameter of 10-20 mm, and
more preferably 13-18 mm, and an average length of e.g.
20-60 mm. Preferably the pelletizing is carried out in such a
way that some variation in the length is obtained, resulting in
a higher bulk density and therefor lcwer transport costs.
According to the invention the material may be mlxed with
other fine materials! e.g. coal or charcoal p~wder before
pelletizing and then pelletized. Also the material may be mlxed
with certain chemicals to prevent soot formation when burning
the pellets, or with hydrophobic ccmpounds to decrease n~isture
absorption of the pellets.
Furthermore the pellets may be treated with hot oil to
carbonize the outer skin thus decreasing the moisture sensivity,
making storage in wet surroudings possible.
m e present pellets may be used directly as industrial

'7~5


fuel, especially in boilers for electric power generation, as
well as for domestic purposes. They can also be used for thermal
gasification or the manuracture of liquid and solid fuels, e.g.
charcoal by carbonizing e.g. by heating in a closed burning
chamber.
The invention will in present Example 1 be elucidated ~or
pineapple plant waste and in Example 2 for maize waste~ The
present process is however also suitable for other cellulosic
wastes, such as described in Philippines patent 13155, in
partlcular those of a similar type.
EX~MPLE 1
Pineapple plant waste, e.g. from plantations, had a bulk
density of 200-300 kg/m3 and a water content of about 78 %w on
total material. The heating value was about 2-3 ~J/kg and the
size below about 500 mmO This material, viz. leaves, ste~ and
stumps, but predominantly leaves (65 %w~ was mechanically de-
watered by squeezing on one or more three-roll-crushers to about
56 ~w of water on total material, while by the bruising action of
the rolls the cuticles of the material, in particular of the
leaves, were damaged to facilitate the release of water. This
bruised material had an average length of about 35 mm, the
majority being shorter than 60 mm.
The resulting cake was loosened in a rotary chopper to
allcw for-effective drying.
The material was thermally dried to about 18 %w water on
total material, with hot air in a rotary cascading drier in
cocurrent flow with the combustion gases. ~ther driers, such as
a grate stoker, could also be used.
The dried material was classified and the fragments larger
3 than 65 mm were adequately chopped in a xotary chopper to a size
below 65 mm. me classified and the chopped material was pel-
letized in a three-roll die extrusion pelletizer at a pressure
of 7 kN/cm~, the holes of the die having a diameter of 13 mm and
a length of 65 mm. During this pelletizing, which WAS carried
out continuously, the friction and campaction in the die caused


, ,, ~'r




the temperature of the die and pellets to rise until a station-
ary condition settled after about 15 minutes at about 80C for
the dle and about 75C for the pellets.
The pellets had a diameter of 13 rnm an a length of 20-
60 mm.
The pellets were then cooled with a forced air flow to room
temperature, while being classified by a vibrating screen, and
transferred to a warehouse for despatch.
The pellets had sufficient strength to be handled by
mechanical conveyors. Their heating value was about 18 MJ/kg,
their water content about 14%w on total rnaterial, their density
1.1 g/cm3 and the bulk density was 675 kg/m3.
The output of the pellet mill was almost 50 kg pellets per
kilowatt hour electrical energy consumed by the pellet mill.
m e fines ex-screening may be recycled. The air ex-pellet
cooler may be used as secondary air in the furnace of the drier.
As fuel for firing this furnace mechanically dewatered
rnaterial, thermally dried material, or the pellets may e.g. be
used. The amount required will amount to about 20%w, of the
pineapple waste inta}ce.
EXAMPLE 2
Maize waste (stalls and leaves) with a water content of
62 %w on total material was squeezed and crushed to a water
content of 48 %w on total material. This product was dried in a
stove to 17 %w water on total material.
The length of the thus obtained straw feed stock before
densificatio~ ~as about 30-50 mm and the bu~c density 135 kg/m3.
Pellets were produced with various diameters, i.e. 8, 10 and 15
I~n. m e length over width ratio of the holes of the pelletizer
3 was chosen between seven and eight in those cases. This resulted
in an average pressure oE 11 kN/cm2 c~nd a material density of
about 1.2 g/cm3. The temperature of the die became in stationary

'7~;S;


operation 85C and that of the pellets 75C. The water content
of the cooled product was 13~w. The output of the pellet mill
was about 30 kg/kWh. The calorific value of the pellets was
19.8 ~/kg.

Representative Drawing

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Administrative Status

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Administrative Status

Title Date
Forecasted Issue Date 1985-04-02
(22) Filed 1983-03-28
(45) Issued 1985-04-02
Correction of Expired 2002-04-03
Expired 2003-03-28

Abandonment History

There is no abandonment history.

Payment History

Fee Type Anniversary Year Due Date Amount Paid Paid Date
Application Fee $0.00 1983-03-28
Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
Past Owners on Record
None
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
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Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
Drawings 1993-10-31 1 14
Claims 1993-10-31 4 71
Abstract 1993-10-31 1 15
Cover Page 1993-10-31 1 18
Description 1993-10-31 5 188