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Patent 2082836 Summary

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(12) Patent: (11) CA 2082836
(54) English Title: PROCESS AND DEVICE TO AVOID CONTAMINATION OF TAPPING STEEL BY FLUSH SLAG WITH A TILTABLE CONVERTER
(54) French Title: METHODE ET DISPOSITIF PERMETTANT DE PIQUER L'ACIER SANS LE CONTAMINER AVEC DU LAITIER DE VIDANGE
Status: Deemed expired
Bibliographic Data
(51) International Patent Classification (IPC):
  • C21C 5/46 (2006.01)
  • F27D 3/15 (2006.01)
(72) Inventors :
  • STILKERIEG, BERTHOLD (Canada)
  • BREIER, FRIEDHELM (Canada)
(73) Owners :
  • CONE-PLAST ENGINEERING INC. (Canada)
(71) Applicants :
  • STILKERIEG, BERTHOLD (Canada)
  • BREIER, FRIEDHELM (Canada)
(74) Agent: MOFFAT & CO.
(74) Associate agent:
(45) Issued: 2000-07-18
(22) Filed Date: 1992-11-13
(41) Open to Public Inspection: 1993-10-08
Examination requested: 1992-11-13
Availability of licence: N/A
(25) Language of filing: English

Patent Cooperation Treaty (PCT): No

(30) Application Priority Data:
Application No. Country/Territory Date
P 42 11 593.0 Germany 1992-04-07

Abstracts

English Abstract




This invention concerns a process for the reliable
avoidance of slag contamination of the converter tapping
steel by flush slag. In accordance with the invention a
plastic, workable stopper made of fire-proof material
containing silicic and oxidic components as well as
suitable binding agents is used for this purpose. The
stopper is introduced so far into the tapping channel with
the help of a setting device that its front surface,
terminated with a funnel-shaped compression plate, almost
aligns flushly with the interior side of the converter,
and it fills in the diameter of the tapping channel as a
result of being compressed, creating such a plane treat the
flush slag occurring during tipping of the converter is
reliably directed past the tapping channel. Stopper
systems used up to now had the disadvantage that age-dependent
enlargements of the tapping channel had a detrimental
effect on the functioning of the stopper. The new plastic
stopper adapts to a large range of tapping channel
diameters in accordance with the process used.


Claims

Note: Claims are shown in the official language in which they were submitted.




THE EMBODIMENTS OF THE INVENTION IN WHICH AN EXCLUSIVE PROPERTY
OR PRIVILEGE IS CLAIMED ARE DEFINED AS FOLLOWS:
1. Device for sealing the taphole of a tiltable converter
with a sealing plug (8) which is made of a heat-resistant
material, a faceplate (2) directed towards the inside of the
converter (9) which melts on contact with liquid steel and a
jigging device by which the sealing plug (8) can be inserted
into the taphole (10) and can be moulded therein against its
wall, whereby the sealing plug (8) comprises a cylindrical,
plastic core (1) covered by a faceplate (2) and a base plate
(4) which are connected with the jigging device displaceably
towards one another, characterised in that the faceplate (2)
is designed passing into a funnel channel (5) which penetrates
the sealing plug or core (1) and is designed to receive a
drawing claw (6) acting on the faceplate.
2. Device according to claim 1, characterised in that the
cylindrical core (1) is made of a fire-retardant with a grain
size of below 3mm, binding agents, liquefiers and plasticizers.
3. Device according to claim 2, characterised in that the
cylindrical core (1) comprises as a fire retardant mixture of
20 to 40 wt % aluminosilicate
20 to 40 wt % bonding clay
and



0 to 30 wt % water
to 20 wt % oil
0.5 to 3 wt % plasticizer
0.1 to 2 wt % liquefier
0.1 to 2 wt % temporary binding agent
0.1 to 5 wt % permanent binding agent
and has a density of 0.8 - 0.9 kg/dm3.
4. Device according to claim 3, characterised in that the
permanent binding agents are silicates, the temporary binding
agents - cellulose-material, the plasticizers - polyelectrolyte
alcohols and the liquefiers fatty acids.
5. Device according to claim 1, characterised in that the
faceplate (2) is funnel-shaped and convex towards the smaller
opening and the smaller opening is designed to exit into the
funnel channel (5).
6. Device according to claim 5, characterised in that the
funnel channel (5) is designed passing over the baseplate (4)
and into the jigging device.
7. Device according to claim 1, characterised in that the
funnel channel (5) with a taphole diameter of 20 cm has a
diameter of 25 to 38 mm.



8. Process for operating a converter and for the even and
slag-free removal of the liquid steel, whereby a sealing plug
made of plastic is inserted into the taphole connecting the
inner wall and outer wall up to the height of the inner wall
of the converter in the taphole and is then moulded by means
of a jigging device from its side averted from the inner wall
and also from its side facing the inner wall until it fits
tightly against the hole wall, the sealing plug is positioned
by means of the jigging device in the transition zone in
relation to the converter inner chamber opening a funnel
channel passing therethrough by squeezing, whereby the plastic
material of the plug is made of
20 to 40 wt % insulating aluminosilicate
20 to 40 wt % binding clay
0 to 30 wt % water
to 20 wt % mineral oil
0.1 to 3 wt % plasticizer, e.g., polyelectrolyte
alcohols
0.1 to 2 wt % liquefier, e.g., fatty acid
0.1 to 2 wt % temporary binding agent, e.g.,
cellulose and
0.1 to 5 wt % permanent binding agent, e.g.,
silicates
is mixed to form a fire-retardant with a density of 0.8 to 0.9
kg/dm3, formed into a cylindrical body and is then penetrated
by the funnel channel of a funnel-shaped squeezer plate, fitted
onto the jigging device, inserted into the taphole and secured.

Description

Note: Descriptions are shown in the official language in which they were submitted.





2Q82836
Process and Device to Avoid Contamination
of Ta~ping Steel by Flush Slag with
a Tiltable Converter
Description
This invention concerns a process and a device to
avoid, or rather prevent, contamination of tapping steel
by flush slag with tiltable converters.
Tiltable converters have a discharge opening located
at a suitable spot in the converter wall above the bath
level through which liquid steel is transferred into the
tap ladle. In order to empty the converter, it is tipped
into such a position that the steel flows through the
discharge opening into the ladle. Since specifically
lighter slag of various viscosities is always found on the
molten metal, it first passes into the tap hole during the
tilting process and thus varying quantities of flush slag
end up in the tap ladle. The presence of oxygen-rich slag,
frequently enriched with phosphorous or sulphur, is dis-
advantageous for numerous subsequent metallurgical pro-
cesses. This results in the demand that converter steel be
transferred to the tap ladle as free of slag as possible.
This is preferably achieved by plugging the tap opening of
the converter temporarily.




2482836
2
In this regard, a number of systems are known which
are supposed to open the tapping channel only when the
slag has passed the tapping channel during the tipping
process. In particular, slide systems are known as closing
mechanisms; but they cannot prevent flush slag entering
the tapping channel. In addition, up to now stoppers made
of various materials or combinations of materials have
been placed outside in the tap opening or driven into it.
Combinations of fibrous materials with solid bodies,
plastic clay materials, wooden stoppers, and also pitch
stoppers are used for the external placement and, for the
internal placement, combinations of sheet metals coated
with fireproof materials and sheet metal claws which are
supposed to dig into the tapping channel as described in
DE 39 38 687 C2.
The technically required conical or funnel-like shape
of the tapping channel and the progressive wear of the
fire-proof material in this area results in the premature
breakdown of the stopper protection against flush slag
contaminants, so that the behaviour of the stoppers cannot
be controlled and, therefore, they are a negative factor.
Consequently, fairly large quantities of flush slag are
frequently transferred into the ladle.
The problem of this invention is to present a flush
slag stopper and a process which reliably prevents large
quantities of converter flush slag from being transferred
into the ladle.




208283fi
3
This problem is solved by using a suitable setting
device to push a highly plastic, fire-resistant material
into the tapping channel from the outside up to the area
of transition to the inside of the converter and com-
pressing it with the help of the setting device and a
compressing plate made of heat-resistant materials
attached to the stopper to such an extent that the diam-
eter of the tapping pipe is completely filled in.
As a result of this working method, the geometric
shape of the tapping channel, especially age-related
tapping channel enlargements, are of secondary importance
to the functioning of the stopper.
In the inventive application, the stopper, which
conforms in its fire-proof composition and plasticity to
the occurring operating conditions, adheres instantaneous-
ly to the tapping channel wall, so that immediately after
placement the stopper sits firmly in the tapping channel
directly in the area of transition to the interior of the
converter. On account of the high interior temperatures in
2o the converter, within a short time the fire-proof material
forms a sintered cap a few centimetres thick on the side
facing the interior of the converter which can bear the
blast pressure and the occurring vibration and shaking. In
particular, the time at which the stopper is placed in the
tapping channel in accordance with the invention in order
to exercise its protective function is of secondary
importance. Even after the flush stopper has been in the
tapping pipe for several hours, the different operating
processes and conditions of a converter have no negative




~~~2~3~
4
effect whatsoever on its full functioning and protective
effect. Due to its placement in the area of transition to
the interior of the converter, the penetration of slag
into the tapping channel during the blast process, which
occurs frequently with newly lined converters, is also
effectively prevented. In addition, the permanent and
temporary binding agents contained in the f ire-proof
material of the flush stopper prevent the rest of the mass
decomposing prematurely.
The cap formed towards the interior side of the con-
verter is stable enough to direct the slag securely past
the tapping channel when the converter is tipped. It col-
lapses only when exposed to the ferrostatic pressure.
Because the material adjacent to the tapping channel wall
is not sintered, it is completely removed within a short
time by the outflowing steel.
The fact that large masses of fire-proof material is a
disadvantage of other stopper systems as mentioned in DE
39 38 687 C2 is not supported by the inventive fire-proof
2o material mentioned. For the inventive process mentioned,
merely a mass of ca. 2 - 3 kg fire-proof material is
required to provide complete protection, even with conical
tapping pipes larger than 20 cm in diameter.
The fire-proof material may be made of raw materials
based on suitable compositions of silicon, aluminium, and
magnesium oxides or silicates. Insulating alumosilicate or
magnesium silicate as well as quartz materials in a grain
size less than 3 mm are preferred.




20~2~36
In a preferred embodiment of the invention, the f ire-
resistant material should have the following composition:
- alumosilicate, insulating 20 - 40~ by weight
- bonding clay 20 - 40~ by weight
- water 0 - 30~ by weight
- mineral oil 5 - 20~ by weight
- plasticizer 0.1 - 0.5~ by weight
- liquifier 0.1 - 0.5~ by weight
- temporary binders/celluloses 0.1 - 0.5~ by weight
- permanent binders/silicates 1 - 2.5~ by weight.
This fire-resistant material has a density by volume
of 0.8 - 0.9 kg/dm3 and, therefore, is considerably lighter
than the materials traditionally used for this purpose.
The compression plate used is made of heat-resistant
material and may have any geometric shape suitable for
this purpose. In a preferred embodiment of the invention,
it is funnel-like in shape and has a funnel channel extend-
ed through the stopper. Among other things, this channel
serves as a guide for the setting tool to compress the
stopper and to centre the exiting stream of molten metal
at the moment of the tapping ~in order to avoid the shower
effect of the flowing steel. The funnel channel can have
various diameters. In the case of the inventive embodiment
used, the diameters are 25 - 38 mm; they may, however,
also be larger or smaller, and the entire funnel channel
may be conical. The cross-section of the funnel channel
may deviate from the circular shape.




2082836
(a)
In one broad aspect, the present invention relates to a
device for sealing the taphole of a tiltable converter with
a sealing plug (8) which is made of a heat-resistant
5 material, a faceplate (2) directed towards the inside of the
converter (9) which melts on contact with liquid steel and a
jigging device by which the sealing plug (8) can be inserted
into the taphole (10) and can be moulded therein against its
wall, whereby the sealing plug (8) comprises a cylindrical,
plastic core (1) covered by a faceplate (2) and a base plate
(4) which are connected with the jigging device displaceably
towards one another, characterised in that the faceplate (2)
is designed passing into a funnel channel (5) which
penetrates the sealing plug or core (1) and is designed to
receive a drawing claw (6) acting on the faceplate.
In another broad aspect, the present invention relates
to a process for operating a converter and for the even and
slag-free removal of the liquid steel, whereby a sealing
plug made of plastic is inserted into the taphole connecting
the inner wall and outer wall up to the height of the inner
wall of the converter in the taphole and is then moulded by
means of a jigging device from its side averted from the
inner wall and also from its side facing the inner wall
until it fits tightly against the hole wall, the sealing
plug is positioned by means of the jigging device in the
transition zone in relation to the converter inner chamber
opening a funnel channel passing therethrough by squeezing,
whereby the plastic material of the plug is made of
20 to 40 wt % insulating aluminosilicate
20 to 40 wt % binding clay
0 to 30 wt % water
5 to 20 wt % mineral oil
0.1 to 3 wt o plasticizer, e.g., polyelectrolyte
alcohols
A




202836
(b)
0.1 to 2 wt % liquefier, e.g., fatty acid
0.1 to 2 wt % temporary binding agent, e.g.,
cellulose and
5 0.1 to 5 wt % permanent binding agent, e.g.,
silicates
is mixed to form a fire-retardant with a density of 0.8 to
0.9 kg/dm3, formed into a cylindrical body and is then
penetrated by the funnel channel of a funnel-shaped squeezer
plate, fitted onto the jigging device, inserted into the
t....,~.,~., .. "~.~ ~,.,.."~.."a
A:




6
A preferred embodiment of the invention is explained
below, the diagrammatic illustrations being as follows:
Fig. 1 a lateral perspective view of an embodiment through
a slag flush stopper,
Fig 2 a section through an object in accordance with Fig.
1 and positioning in the tapping channel of a converter,
Fig. 3 a section though a configuration following the
insertion and compressing of the object in accordance with
Fig. 1.
to The flush stopper illustrated in Fig. 1 is cylindrical
in shape. The cross-section of the stopper need not be
circular in shape.
The stopper 1 is made of a fire-resistant material and
has a funnel-shaped compression plate 2 on the side
towards the interior of the converter, this plate having
an extended funnel channel 5 which leads through the
stopper 1. In the embodiment illustrated the fire-resis-
tant material of the stopper is composed of the following:
alumosilicate, insulating 35~ by weight


2o bonding clay 35~ by weight


water 20~ by weight


mineral oil 6.5~ by weight


plasticizer 0.2~ by weight


liquifier 0.3~ by weight


temporary binders 0.5~ by weight


permanent binders 2.5~ by weight.






2Q~2~3~
Silicates were used as permanent binders, cellulose
materials as temporary binders, polyelectrolytical alco-
hols and fatty acids as plasticizers and liquifiers. The
specific gravity of the stopper is 0.8 - 0.9 Kg/dm3.
Fig. 2 illustrates how the stopper is inserted into
the tapping channel with the help of the setting device.
The base plate 4 of the setting device, which conforms to
the diameter of the tapping channel, is adjacent to the
opposite side 7 of the compression plate.
A pulling claw 6 is introduced through the funnel
channel 5 to a position above the funnel and holds the
stopper for the time being until it is finally positioned
in the tapping channel. The stopper is introduced so far
into the tapping channel with the help of the setting
device that its compression plate surface almost aligns
flush with the interior side of the converter 9. The lever
system of the setting device is used to draw the pulling
claw 6 to the compression plate 2, producing pressure on
the stopper material 1, which deforms until the diameter
of the tapping hole 10 is completely filled in. Fig. 3
illustrates a compressed stopper 8 in the tapping channel
10. With the help of the setting device the thickness of
the stopper base 12 in Fig. 3 is always adhered to for
every tapping channel diameter of a converter, so that it
is guaranteed that the behaviour of the opening is repro-
ducible. Stopper material not required to f ill in the
tapping channel diameter is compressed to the tapping
channel wall with the help of the compression plate as
shown in Fig. 3.




20~~~~~
g
On account of the high radiant heat on the interior
side of the converter, the compression plate melts and
sinters with the f ire-proof material to a solid cap 11,
Fig 3. This cap bears the blast pressure and the resulting
vibration and shaking. The remaining fire-proof insulating
material solidifies to such an extent that it remains
stable in the tapping channel. It does not sinter with the
wall of the tapping channel. The sintered cap is so stable
that it directs the flush slag reliably over the tapping
hole when the converter is tipped and only collapses under
the ferrostatic pressure. The remaining stopper material
is removed within a few seconds by the outflowing steel.
On account of the low material quantities, only a few
foreign substances reach the tapping ladle. The inventive
embodiment and application guarantee a high degree of
reliability in the functioning of the flush stopper, even
where it is exposed to heat for periods longer than two
hours. Where stationary slag measurements were carried out
in tapping ladles of 100 - 250 t capacity, significant
quantities of flush slag could no longer be detected in
200 test relinings.

Representative Drawing
A single figure which represents the drawing illustrating the invention.
Administrative Status

For a clearer understanding of the status of the application/patent presented on this page, the site Disclaimer , as well as the definitions for Patent , Administrative Status , Maintenance Fee  and Payment History  should be consulted.

Administrative Status

Title Date
Forecasted Issue Date 2000-07-18
(22) Filed 1992-11-13
Examination Requested 1992-11-13
(41) Open to Public Inspection 1993-10-08
(45) Issued 2000-07-18
Deemed Expired 2011-11-14

Abandonment History

There is no abandonment history.

Payment History

Fee Type Anniversary Year Due Date Amount Paid Paid Date
Application Fee $0.00 1992-11-13
Registration of a document - section 124 $0.00 1994-01-28
Reinstatement: Failure to Pay Application Maintenance Fees $200.00 1995-02-28
Maintenance Fee - Application - New Act 2 1994-11-14 $50.00 1995-02-28
Maintenance Fee - Application - New Act 3 1995-11-13 $50.00 1995-10-20
Maintenance Fee - Application - New Act 4 1996-11-13 $50.00 1996-11-13
Maintenance Fee - Application - New Act 5 1997-11-13 $75.00 1997-10-29
Maintenance Fee - Application - New Act 6 1998-11-13 $75.00 1998-11-13
Maintenance Fee - Application - New Act 7 1999-11-15 $75.00 1999-11-15
Final Fee $150.00 2000-04-12
Maintenance Fee - Patent - New Act 8 2000-11-14 $75.00 2000-11-14
Maintenance Fee - Patent - New Act 9 2001-11-13 $150.00 2001-11-13
Maintenance Fee - Patent - New Act 10 2002-11-13 $200.00 2002-11-08
Maintenance Fee - Patent - New Act 11 2003-11-13 $200.00 2003-11-13
Maintenance Fee - Patent - New Act 12 2004-11-15 $250.00 2004-11-10
Maintenance Fee - Patent - New Act 13 2005-11-14 $250.00 2005-11-09
Maintenance Fee - Patent - New Act 14 2006-11-14 $250.00 2006-11-09
Maintenance Fee - Patent - New Act 15 2007-11-13 $450.00 2007-11-13
Maintenance Fee - Patent - New Act 16 2008-11-13 $450.00 2008-11-10
Maintenance Fee - Patent - New Act 17 2009-11-13 $450.00 2009-11-13
Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
CONE-PLAST ENGINEERING INC.
Past Owners on Record
BREIER, FRIEDHELM
STILKERIEG, BERTHOLD
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
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Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
Cover Page 2000-06-30 1 44
Representative Drawing 2000-06-30 1 8
Representative Drawing 1998-09-22 1 11
Cover Page 1994-04-30 1 35
Abstract 1994-04-30 1 58
Claims 1994-04-30 2 98
Description 1994-04-30 8 462
Drawings 1994-04-30 3 109
Description 1999-10-27 10 379
Claims 1999-10-27 3 94
Fees 1999-11-15 1 38
Fees 2000-11-14 1 36
Fees 2002-11-08 1 38
Fees 2003-11-13 1 38
Correspondence 2000-04-12 2 62
Fees 2001-11-13 1 39
Fees 1997-10-29 1 38
Fees 1998-11-13 1 42
Fees 2004-11-10 1 36
Fees 2007-11-13 1 64
Fees 2005-11-09 1 35
Office Letter 1993-04-23 1 64
Examiner Requisition 1997-06-10 2 123
Prosecution Correspondence 1997-11-19 6 219
Fees 2008-11-10 1 58
Fees 2006-11-09 1 56
Fees 2009-11-13 1 63
Correspondence 2011-03-15 2 135
Fees 1996-11-13 1 32
Fees 1995-10-20 1 39
Fees 1995-02-28 1 49