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Patent 2298806 Summary

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Claims and Abstract availability

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(12) Patent: (11) CA 2298806
(54) English Title: A GAS CONCENTRATION METER AND INSULATING GLASS ASSEMBLY AND METHOD THEREOF
(54) French Title: ENSEMBLE A INDICATEUR DE CONCENTRATION GAZEUSE ET VERRE ISOLANT ET METHODE APPLICABLE A CET ENSEMBLE
Status: Expired
Bibliographic Data
(51) International Patent Classification (IPC):
  • G01N 27/68 (2006.01)
  • E06B 3/54 (2006.01)
  • E06B 7/16 (2006.01)
  • E06B 7/28 (2006.01)
  • G01N 27/92 (2006.01)
  • E06B 3/677 (2006.01)
(72) Inventors :
  • ALKHOURY, ELIE (Canada)
(73) Owners :
  • CAN-BEST BUILDING SCIENCES CORPORATION (Canada)
(71) Applicants :
  • CAN-BEST BUILDING SCIENCES CORPORATION (Canada)
(74) Agent:
(74) Associate agent:
(45) Issued: 2005-05-17
(22) Filed Date: 2000-02-15
(41) Open to Public Inspection: 2001-08-15
Examination requested: 2002-08-07
Availability of licence: N/A
(25) Language of filing: English

Patent Cooperation Treaty (PCT): No

(30) Application Priority Data: None

Abstracts

English Abstract

The system includes an access assembly for communicating with the gas filled insulating units, flexible electrodes for insertion through the access assembly to the gas and for sensing the concentration of the gas, and a meter for measuring and displaying the concentration of the gas that is sensed through the electrodes.


French Abstract

Le système comprend un ensemble d'accès pour communiquer avec les unités d'isolation remplies de gaz, des électrodes souples pour une insertion à travers l'ensemble d'accès au gaz et pour détecter la concentration du gaz, et un appareil de mesure pour mesurer et afficher la concentration du gaz qui est détecté par les électrodes.

Claims

Note: Claims are shown in the official language in which they were submitted.



CLAIMS
The embodiments of the invention in which an exclusive property or privilege
is claimed are defined as follows:
1. A metering system for measuring the concentration of a gas within a
sealed insulating glass window having two spaced glass panes separated by
an edge spacer, an edge seal and a cavity, from the outside of said window
comprising:
(a) an access port assembly having a connecting tube having one
end within said cavity and a second end outside, a spacer block
and a stopping means, wherein said spacer block is mounted
adjacent said edge seal and said connecting tube is mounted
through said spacer block, said edge seal and said edge spacer,
thereby connecting said cavity to the outside; said stopping
means securing said second end of said connecting tube;
(b) a probing means for insertion through said access port
assembly to said cavity for sensing said gas concentration; and
(c) a measuring means for measuring, calibrating, scaling and
displaying said gas concentration sensed by said probing
means;
wherein said access port assembly allows access into said cavity by said
probing means from the outside, said measuring means attached to said
probing means allowing for the measurement of said gas concentration.
2. A metering system as claimed in claim 1 wherein said connecting tube
is at a 90° angle integrally molded to said spacer block and said
stopping
means is a reusable knock-out cap.
3. A metering system as claimed in claim 1 wherein said probing means
is a pair of flexible electrodes separated from one another by a predetermined




-2-
distance, said predetermined distance dependent on said gas being
measured.
4. A metering system as claimed in claim 3 wherein said pair of flexible
electrodes is a ribbon having exposed tips at a first end and connected to
said
measuring means at a second end by an electrical connector.
5. A metering system as claimed in claim 4 wherein said probing means
may be either permanently installed into said sealed insulating glass window
or removable from said connecting tube.
6. A metering system as claimed in claim 4 wherein said measuring
means is a meter having electronic circuitry to excite, control and monitor
the
excitation level of said flexible electrodes.
7. A metering system as claimed in claim 6 wherein said meter is hand-
held and battery operated.
8. A metering system as claimed in claim 6 wherein said gas being
measured is Argon, Krypton or any combination of inert gas.
9. A method of measuring the concentration of a gas within a sealed
insulating glass window having two spaced glass panes separated by an edge
spacer, an edge seal and cavity, from the outside of said window using a
metering system comprising:
(a) inserting a pair of flexible electrodes separated from one another
by a predetermined distance, said distance dependent on said
gas being measured through an access port assembly having a
connecting tube having one end within said cavity and a second
end outside, a spacer block and a stopping means wherein said
spacer block is mounted adjacent said edge seal and said




-3-
connecting tube is mounted through said spacer block said edge
spacer and edge seal for access by said probing means to said
cavity and said gas; thereby connecting said cavity to the
outside; said stopping means securing said second end of said
connecting tube;
(b) sampling and sensing said concentration of said gas by said
flexible electrodes; and
(c) relaying said concentration of said gas to a measuring means
for measuring calibrating, scaling and displaying said gas
concentration sensed by said flexible electrodes.
10. A method of measuring the concentration of a gas as claimed in claim
9 further comprising charging said flexible electrodes to a level at which the
breakdown voltage produces arcing across said predetermined distance
through said gas.

Description

Note: Descriptions are shown in the official language in which they were submitted.



CA 02298806 2000-02-15
r
A GAS CONCENTRATION METER AND INSULATING GLASS ASSEMBLY
AND METHOD THEREOF
- 5 Field of the Invention
This invention relates in general to a system for measuring a gas sealed
within an insulating glass assembly, and more particularly a gas concentration
meter
and method used for measuring the concentration of a gas within a sealed
cavity or
to window assembly and a means of providing access to the sealed cavity.
Background of the Invention
Due to the high cost of heating and cooling in most building structures, high
15 efficiency and energy saving means are desirable for fenestration systems
such as
windows, doors, curtain walls, skylights or the like. Typically such systems
include
sealed insulating glass units filled with an inert gas. Traditionally these
insulating
systems have had an insulating air space or vacuum between the panels, which
recently included a gas such as Argon to improve thermal performance. The
2o inclusion of the gas is to provide additional insulation or resistance to
thermal
conductivity. Argon is the gas predominantly used due to its high benefit/cost
ratio.
Over time the gas may escape or dissipate due to faulty seals of the like,
which negates the beneficial effects of the insulating windows and results in
2s increased energy costs. Due to the nature of the gases involved as
described above,
it is difficult to determine how much of the gas has escaped, and therefore
what
concentration of gas is left in the glass assembly. Furthermore if the gas
concentration is found lower than the promised or the pre-selected level, the
sealed
insulating glass unit cannot generally be replenished without destroying the
frame or
3o seal of the fenestration system.


CA 02298806 2000-02-15
-.5 ,
-2-
Several methods for measuring gas concentration in insulating glass units do
exist today. However, such methods require sampling and analysis of the gas in
the
insulating glass unit's cavity. The use of such methods is severely limited,
as the
sampling of gas within the cavity cannot be performed on an insulating glass
unit
" 5 once it is glazed in place. Once the insulating unit is glazed in place,
the edge seal
becomes inaccessible. Any attempt to carry out sampling of the insulating
glass unit
is made at the risk of damaging the edge seal, which will promote insulating
unit
failure in a very short period of time.
to Presently, buyers of gas-filled sealed units can only rely on the
supplier's
assuring words that the supplied units do contain insulating gas within the
insulating
cavity. As the fill gas is colorless and odorless, and inaccessible, there is
no means
of verifying such claims. Currently, insulating gas unit manufacturers may be
certified that they comply with National Standards regarding gas concentration
test
t5 requirements. Due to the lack of a more practical test method, the only
reliable
method that has been adopted by the Standard is gas chromatography. This
method,
however, requires sampling of gas in inaccessible cavity, and use of highly
specialized analytical equipment and technicians to operate under strict
laboratory
conditions .
Current method of determining gas concentration involves measuring of
Oxygen concentration in the cavity as it relates to presence of air. Other
methods
(under development) may be used to measure the concentration of a gas within
the
sealed units consist of applying a high voltage electrical current in the
range of
2s 10,000 to 20,000 volts across the glazing cavity (i.e. across the outside
surfaces of
the spaced glass).
Therefore, while the existing methods of determining gas concentration in
insulating glass units can be used for laboratory research and testing of non-
glazed


CA 02298806 2000-02-15
-3-
sealed units, these methods cannot be employed effectively for routine quality
control and field-testing purposes.
Furthermore, the ability to access and measure the level of gas within the
glass assembly would allow the installer to add more gas when required and
therefore maintain the insulating benefits of the glass.
Prior art glass assemblies have been devised to try and address the
aforenoted problems. For example, United States Patent No. 5,299,399 which
to issued on April 5, 1994 to the inventors Bruce A. Baier et al. and was
assigned to
Pella Corporation of Pella, Iowa. This patent relates to a dual glazing window
that
has a removable glazing panel, which includes a breather system that connects
the
air chamber between the glazing panels with the outside ambient air by routing
an
outwardly facing channel into the window rail.
United States Patent No. 2,880,475 issued on April 7, 1959, and relates to a
double glazed window unit suitable for use in a window, in which the space
between
the glass panels is evacuated to provide good insulating qualities and to
prevent the
formation of condensation due to temperature differences between the inner and
outer panels.
United States Patent No. 2,125,372 was issued on August 2, 1938 and
relates to a fitting for a glass sheet having a perforation and comprises of a
metal
connection plug having a threaded passage, which fits into the perforation for
2s sealing the glass sheet.
United States Patent No. 1,336,211 was issued on April 6, 1920 to Henry
Duffy of Longmont, Colorado and relates to an exteriorly threaded plug having
a
central port and a lateral passage with a valve seated in the passage, and
having a
3o transverse port.


CA 02298806 2000-02-15
-4-
Thus a gas concentration meter used for measuring the concentration of a gas
within a sealed insulating unit or glass assembly and method thereof is
desirable.
Furthermore a non-obtrusive means of providing access to the insulating cavity
to
s measure and/or replenish a gas within the cavity would be beneficial.
Summary of the Invention
An object of one aspect of the present invention is to provide a gas
Io concentration meter and improved insulating glass assembly and a method
thereof.
In accordance with one aspect of the present invention there is provided a
system for measuring the concentration of a gas within a sealed insulating
cavity
having an access means for communicating with the sealed insulating cavity, a
15 probing means for insertion through the access means to the gas and having
the
ability to sense the concentration of the gas, and a measuring means for
measuring
and displaying the concentration of the gas through the probing means.
Conveniently, the access means is further defined as an access port assembly
2o having a connecting means through the glazing spacer block and a stopping
means.
Preferrably, the connecting means spacer block may be defined as a
connecting tube being integrally molded to a spacer block for insertion
between the
glass panes of the insulating unit.
In accordance with another aspect of the present invention, the probing
means may be further defined as a pair of flexible electrodes which may be
separated by a predetermined distance to form a gap.


CA 02298806 2000-02-15
-5-
In accordance with still another aspect of the invention, the measuring means
may be defined as a meter having electronic circuitry to excite, control,
monitor the
excitation level, relate the excitation level to gas concentration through
calibration
means, and indicate or display the concentration level.
Another object of the present invention is to provide an improved method for
measuring the concentration of a gas in a gas filled sealed insulating glazing
assembly comprising of at least two spaced glass panes wherein the method
comprises the following steps:
to
a) inserting a probing means through an access means for communication with
the cavity of the gas filled insulating unit;
b) or placement of permanent probing means into the glazing cavity through the
edge seal of the insulating unit;
c) or placement of permanent probing means in a gas sampling device such as a
syringe or any other sampling container;
d) sensing the concentration of the gas with the probing means; and relaying
the
concentration of the gas to a measuring means for measuring the
concentration of the gas.
2s Advantages of the present invention are:
a) ability to measure actual gas concentration on site or at the plant,
b) ability to pressure equalize the glazing cavity in order to eliminate
3o glass distortion or breakage, and


CA 02298806 2000-02-15
-6-
c) ability to re-fill the insulated units with gas if gas-filling was deemed
inadequate, thereby reducing the number of gas-filled units that have
to be replaced.
Brief Description of the Drawings
A detailed description of the preferred embodiment is provided herein below
by way of example only and with reference to the following drawings, in which:
Figure 1 in a side cross-sectional view, illustrates a conventional insulating
glass assembly with the meter;
Figure 2 in a side cross-sectional view, illustrates the insulating glass
1s assembly in accordance with the preferred embodiment of the present
invention;
Figure 3 in a perspective view, illustrates the system in accordance with the
preferred embodiment of the present invention.
2o Figure 4 in a top plan view, illustrates the meter in accordance with the
preferred embodiment of the present invention.
Figure 5 in a cross-sectional view, illustrates the probing means being
inserted into the access means in accordance with the preferred embodiment of
the
25 present invention.
Figure 6 in a cross-sectional view, illustrates the probing means being
permanently installed into the glazing cavity in accordance with the preferred
embodiment of the present invention.


CA 02298806 2000-02-15
Figure 7 in a top plan view, illustrates the circuitry in accordance with the
preferred embodiment of the present invention.
In the drawings, preferred embodiments of the invention are illustrated by
s way of example. It is to be expressly understood that the description and
drawings
are only for the purpose of illustration and as an aid to understanding, and
are not
intended as a definition of the limits of the invention.
Detailed Description of the Preferred Embodiment
Referring to Figures 1 and 2, there is illustrated in a cross-sectional side
view, a system for measuring the concentration of a gas within a sealed
insulating
cavity 10 comprising of a sealed insulating glass units 11 , defined by two
glass
panes 12 separated by edge spacer 28 and edge seal 36, in accordance with the
~ s preferred embodiment of the present invention.
The system 10 includes an access means 14 for communicating with the
sealed cavity 32 of the sealed insulating glass units 11, a probing means 16
for
insertion through the access means 14 to the gas filled sealed cavity 32 and
for
2o sensing the concentration of the gas, and a measuring means 18 for
measuring and
displaying the concentration of the gas that is sensed through the probing
means 16.
The access means 14 may be further defined as an access port assembly 20,
whereby the access port assembly 20 can comprise of a connecting means spacer
2s block 23 and a stopping means 24. The connecting means spacer block 23 may
include a connecting tube 26 that may be integrally molded to a conventional
spacer
block 22. The connecting tube 26, permanently inserted and sealed in passage
30
made through the edge seal 36 and edge spacer 28, connects the cavity 32
between
the glass panes 12 to the outside environment. More particularly the passage
30


CA 02298806 2000-02-15
_g_
may be a 90-degree bore 34 made through the spacer block 23 which terminates
at
the connecting tube 26.
The stopping means 24 may be further defined as a resealable knock-out cap
s 37 which allows for temporary access to the cavity 32 via the passage 30 and
the
connecting tube 26. The spacer block 23 with connecting tube 26 may be made
from a variety of materials and may be employed in any number positioned at
any
location around the perimeter of the sealed insulating glass unit 11 being
used.
to Alternatively, system 10 includes a probing means 16 permanently
incorporated into the gas filled insulating glass unit 11 by means of
insertion
through the edge seal 36 for sampling and sensing the concentration of the
gas, and
a measuring means 18 for measuring and displaying the concentration of the gas
that
is sensed through the probing means 16.
is
The probing means 16 may be further defined as a pair of flexible electrodes
38. The flexible electrodes 38 (by way of example 26 Gage fine electrical
wires)
may be separated from one another by a pre-determined distance to form a gap
40.
More specifically the flexible electrodes 38 may be in the form of a ribbon
having
2o exposed tips 42 or sensing means at one end that may be placed within the
cavity
32, while the other end of the flexible electrodes 38 are connected to the
measuring
means 18 by means of electrical connector 53.
The flexible electrodes 38 may be made from a variety of materials and may
2s have different distances for the gap 40 as the capacities, calibration and
environment
for the flexible electrodes 38 can vary. The location and connection of the
flexible
electrodes 38 can also vary. More specifically, the flexible electrodes 38 may
be
integrated with the spacer block 23 so that the sensing means 42 of the
flexible
electrodes 42 extend from the connecting tube 26 of the spacer block 23 and
the


CA 02298806 2000-02-15
-9-
exposed end 39 of the flexible electrodes 38 can be connected into the
measuring
means 18.
The sealed insulating glass units 11 may be contained within a frame 13,
s such as a window or doorframe, and secured within the frame 13 by a
removable
glazing stop 52. For measuring gas concentration in glazing cavity 32 or gas
replenishing should the gas concentration within the insulating unit get too
low, the
glazing stop 52 may be removed to reveal the stopping means 24 located at the
edge
of the spacer block 23. The glazing cavity 32 may be accessed by removing the
stopping means 24. Following gas concentration measurement or gas
replenishment, the stopping means 24 can then be placed back and resealed.
Alternatively, if a permanent probing means 16 is employed, the glazing stop
52
may be removed to reveal the exposed end 39 of the flexible electrodes 38
which
can be connected into the measuring means 18 for sampling and measuring the
gas
15 concentration.
The measuring means 18 may be further defined as a meter 44 having
electronic circuitry 46. The meter 44 excites the sensing end 42 of the
probing
means 16, controls, monitors the excitation level, relates the excitation
level to gas
2o concentration through calibration means, and indicates or displays the gas
concentration level. Through the electronic circuitry 46, and more
specifically a
circuit board 50, an excitation signal is applied to the flexible electrodes
38 so as to
create an arc therebetween at the sensing means 42. The meter 44 may be
developed into a hand-held instrument, battery operated or an electronic
stationary
2s device. In general, meter 44 could be operated by a battery requiring one
or more
1.S.V AA size batteries. The concentration of the gas may be calculated
through
calibration and scaling circuit, and displayed on the meter 44 through a
LCD/LED
display 19 or through a variety of other visual display methods such as
digital,
graphic, analogue or interfaced with a computer for logging or process
control. The
3o concentration of the gas may also be indicated visually by a colour change
of


CA 02298806 2002-08-07
tl7
chemically sensitized medium or identifier or through a sound effect such as a
buzzer.
The meter 44 may be calibrated to read a variety of gases such as Argon,
Krypton or any mixture of inert gases. Calibration of the meter 44 is
conducted
using the type of gas to be tested and either standard hardware or software
such as
an embedded programmed chip
in operation, the method for measuring the concentration of a gas the
probing means 16 creates an arc within the sealed insulating cavity 32 having
electrical breakdown voltage proportonate to the concentration of the gas as
governed by Paschen's law described below.
Paschen's law essentially states that the breakdown voltage characteristics of
a
gap are a function (generany not linear) of the product of the gas pressure
and the
gap length. usually written as V = f (p b) where "p" ~s the pressure and "d"
~s the
gap distance. In actuality, the gas density should replace the pressure
Paschen's law states that the breakdown voltage mil remain wnstant as long
as the gas density and gap length remain constant. By way of example, the
breakdown voltage is a constant where the gap length is halved and the gas
density
is doubled. Therefore the breakdown voltage will be dependent on the gas
density
and on the type, shape and spacing of the flexible electrodes 38 at the
sensing
means 42. Knowing the breakdown voltage of the arc developed across the
electrodes 38 at the sensing end means 42 having known electrode properties,
the
gas concentration is thus determined.
Referring to Figure 3, the user would temporarily remove the glazing stop
52 to reveal the stopping means or knockout cap 24 located at the side of the
spacer
block 23. The stopping means 24 may be removed and the probing means ~6 or


CA 02298806 2000-02-15
-11-
flexible electrodes 38 may then be inserted into the passage 30. As the
flexible
electrodes 38 are flexible, they will bend around the 90-degree bore 34
through the
spacer block 23 and the connecting tube 26 to the cavity 32 located between
the
glass panes 12. Alternatively, in permanent electrode installation, the
electrodes 38
s extend outside of the edge spacer 28 of the sealed unit as previously
described.
Upon placing the flexible electrodes 38 within the cavity 32, the sensing end
42 is excited, so that arcing occurs across the gap 40 between the exposed
tips 42 of
the flexible electrodes 38 through the gas. The electronic circuitry 46 and
more
to specifically the circuit board 50 controls the excitation level through
circuit 54, and
measures the breakdown voltage and the current through the electrodes 38
across the
electrode gap 40 at the sensing end 42.
Once the breakdown voltage is stabilized through means of circuit 55, the
15 gas concentration can then be sampled and calculated by calibration circuit
56 from
the breakdown voltage relayed to the meter 44 by the flexible electrodes 38
and
other parameters as governed by Paschen's law and derived through laboratory
calibration. The results may be displayed on the meter through circuit 57 and
a
variety of display modes outlined above and in a variety of measurements such
as
2o percentage, parts per million etc.
The accuracy of the method and measurements may be improved by
repeating the excitation of the sensing means 42 of the electrodes 38 several
times
and averaging all of the measured individual breakdown voltage values.
Averaging
25 of the results may be done automatically by programming the circuit's
controller
chip.
Other variations and modifications of the invention are possible. All such
modifications or variations are believed to be within the sphere and scope of
the
3o invention as defined by the claims appended hereto.

Representative Drawing
A single figure which represents the drawing illustrating the invention.
Administrative Status

For a clearer understanding of the status of the application/patent presented on this page, the site Disclaimer , as well as the definitions for Patent , Administrative Status , Maintenance Fee  and Payment History  should be consulted.

Administrative Status

Title Date
Forecasted Issue Date 2005-05-17
(22) Filed 2000-02-15
(41) Open to Public Inspection 2001-08-15
Examination Requested 2002-08-07
(45) Issued 2005-05-17
Expired 2020-02-17

Abandonment History

There is no abandonment history.

Payment History

Fee Type Anniversary Year Due Date Amount Paid Paid Date
Registration of a document - section 124 $100.00 2000-02-15
Application Fee $150.00 2000-02-15
Maintenance Fee - Application - New Act 2 2002-02-15 $50.00 2002-01-23
Request for Examination $400.00 2002-08-07
Maintenance Fee - Application - New Act 3 2003-02-17 $50.00 2003-02-14
Maintenance Fee - Application - New Act 4 2004-02-16 $50.00 2004-02-16
Final Fee $150.00 2005-02-15
Maintenance Fee - Application - New Act 5 2005-02-15 $100.00 2005-02-15
Maintenance Fee - Patent - New Act 6 2006-02-15 $100.00 2005-12-14
Maintenance Fee - Patent - New Act 7 2007-02-15 $100.00 2006-12-11
Maintenance Fee - Patent - New Act 8 2008-02-15 $100.00 2008-02-12
Maintenance Fee - Patent - New Act 9 2009-02-16 $100.00 2009-01-22
Maintenance Fee - Patent - New Act 10 2010-02-15 $125.00 2010-01-06
Maintenance Fee - Patent - New Act 11 2011-02-15 $125.00 2010-12-09
Maintenance Fee - Patent - New Act 12 2012-02-15 $125.00 2011-12-14
Maintenance Fee - Patent - New Act 13 2013-02-15 $125.00 2012-12-18
Maintenance Fee - Patent - New Act 14 2014-02-17 $125.00 2014-01-28
Maintenance Fee - Patent - New Act 15 2015-02-16 $225.00 2015-01-26
Maintenance Fee - Patent - New Act 16 2016-02-15 $225.00 2016-01-29
Maintenance Fee - Patent - New Act 17 2017-02-15 $425.00 2017-09-18
Maintenance Fee - Patent - New Act 18 2018-02-15 $225.00 2018-01-08
Maintenance Fee - Patent - New Act 19 2019-02-15 $225.00 2018-12-03
Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
CAN-BEST BUILDING SCIENCES CORPORATION
Past Owners on Record
ALKHOURY, ELIE
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
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Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
Representative Drawing 2001-08-09 1 8
Description 2002-08-07 11 453
Claims 2002-08-07 3 99
Abstract 2000-02-15 1 10
Cover Page 2001-08-09 1 34
Drawings 2001-05-04 7 70
Description 2000-02-15 11 454
Claims 2000-02-15 4 114
Drawings 2000-02-15 8 135
Cover Page 2005-04-15 1 34
Correspondence 2000-03-14 1 2
Assignment 2000-02-15 5 168
Correspondence 2001-05-04 8 101
Correspondence 2002-09-24 1 16
Correspondence 2003-02-14 2 69
Prosecution-Amendment 2002-08-07 7 222
Correspondence 2003-03-18 1 18
Fees 2003-02-14 1 33
Correspondence 2003-04-23 2 75
Fees 2002-01-23 1 35
Fees 2004-02-16 1 30
Correspondence 2005-02-15 1 27
Fees 2005-02-15 1 27
Maintenance Fee Payment 2017-09-18 2 53
Correspondence 2005-08-08 1 32
Correspondence 2005-09-08 1 14
Correspondence 2005-09-08 1 17
Fees 2005-12-14 1 45
Maintenance Fee Payment 2018-01-08 1 146
Fees 2006-12-11 2 117
Fees 2008-02-12 1 62
Fees 2009-01-22 1 50
Fees 2010-01-06 1 46
Maintenance Fee Payment 2018-12-03 1 75
Fees 2010-12-09 1 47
Fees 2011-12-14 1 240
Fees 2012-12-18 1 130
Fees 2014-01-28 2 135
Fees 2015-01-26 2 137
Maintenance Fee Payment 2016-01-29 2 58