Note: Descriptions are shown in the official language in which they were submitted.
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HAIR DYES COMPRISING 3-AMINO-2,6-DIMETHYLPHENOL
FIELD OF THE INVENTION
The subject matter of the present application are compositions and methods for
dyeing keratin
fibers containing the 3-amino-2,6-dimethylphenol and physiologically
compatible salts thereof.
BACKGROUND OF THE INVENTION
In the field of dyeing keratin fibers, in particular hair coloring, oxidation
dyes have achieved
significant importance. The coloration arises here as a result of the reaction
of certain developer
substances with certain coupler substances in the presence of a suitable
oxidizing agent. The
developer substances used here are, in particular, unsubstituted or
substituted
1,4-diaminobenzenes.
Besides dyeing to the desired intensity, numerous additional demands are made
on oxidation
dyes which are used for coloring human hair. For example, the dyes must be
acceptable from a
toxicological and dermatological point of view and the hair colorations
achieved must have good
light fastness, permanent wave fastness, acid fastness and rubbing fastness.
However, in any
case, such colorations must remain stable over a period of at least 4 to 6
weeks without being
affected by light, rubbing and chemical agents. Furthermore, it is required
that the suitable dyes
possess a good physiological compatibility.
The currently used colorants, however, do not satisfy the above mentioned
requirements in all
respects. Therefore there is still a need for novel coupler substances which
satisfy the above
mentioned requirements to a better degree.
SUMMARY OF THE INVENTION
Therefore there is a need for new o-aminophenol derivatives with improved
properties, especially
with regard to improved physiological compatibility.
DETAILED DESCRIPTION OF THE INVENTION
It has now been found that 3-amino-2,6-dimethylphenol and its salts have
improved properties,
especially they are non-sensitizing.
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The present invention therefore relates to compositions and methods for dyeing
keratin fibers,
especially wool, silk or hair, particularly human hair, using the 3-amino-2,6-
dimethylphenol
and/or its inorganic or organic salt.
Although the 3-amino-2,6-dimethylphenol and/or its inorganic or organic salt
are especially
suitable for dyeing kertain fibers, in principle it would also be possible to
dye other natural or
synthetic fibers, especially cotton or nylon 66, with the 3-amino-2,6-
dimethylphenol.
The 3-amino-2,6-dimethylphenol and/or its inorganic or organic salt may be
used alone or in
combination with known developer substances and/or coupler substances.
Suitable developers for use in the compositions described herein include, but
are not limited to:
p-phenylenediamine derivatives, e.g. benzene-1,4-diamine (commonly known as
p-phenylenediamine), 2-methyl-benzene-1,4-diamine, 2-chloro-benzene-1,4-
diamine, N-phenyl-
benzene-l,4-diamine, N-(2-ethoxyethyl)benzene-1,4-diamine, 2-[(4-amino-phenyl)-
(2-hydroxy-
ethyl)-amino]-ethanol, (commonly known as N,N-bis(2-hydroxyethyl)-p-
phenylenediamine) (2,5-
diamino-phenyl)-methanol, 1-(2'-Hydroxyethyl)-2,5-diaminobenzene, 2-(2,5-
diamino-phenyl)-
ethanol, N-(4-aminophenyl)benzene-1,4-diamine, 2,6-dimethyl-benzene-1,4-
diamine,
2-isopropyl-benzene-1,4-diamine, 1-[(4-aminophenyl)amino]-propan-2-ol, 2-
propyl-benzene-
1,4-diamine, 1,3-bis[(4-aminophenyl)(2-hydroxyethyl)amino]propan-2-ol, N4,N4,2-
trimethylbenzene-1,4-diamine, 2-methoxy-benzene-1,4-diamine, 1-(2,5-
diaminophenyl)ethane-
1,2-diol, 2,3-dimethyl-benzene-1,4-diamine, N-(4-amino-3-hydroxy-phenyl)-
acetamide, 2,6-
diethylbenzene-1,4-diamine, 1,4-diamino-2-methoxymethylbenzene, 2,5-
dimethylbenzene-1,4-
diamine, 2-thien-2-ylbenzene-1,4-diamine, 2-thien-3-ylbenzene-1,4-diamine, 2-
pyridin-3-
ylbenzene-1,4-diamine, 1,1'-biphenyl-2,5-diamine, 2-(methoxymethyl)-benzene-
1,4-diamine, 2-
(aminomethyl)benzene-1,4-diamine, 2-(2,5-diaminophenoxy)ethanol,
N-[2-(2,5-diaminophenoxy)ethyl]-acetamide, N,N-dimethylbenzene-1,4-diamine,
N,N-diethylbenzene-1,4-diamine, N,N-dipropylbenzene-1,4-diamine, 2-[(4-
aminophenyl)-
(ethyl)amino]ethanol, 2-[(4-amino-3-methyl-phenyl)-(2-hydroxy-ethyl)-amino]-
ethanol, N-(2-
methoxyethyl)-benzene-1,4-diamine, 3-[(4-aminophenyl)amino]propan-l-ol, 3-[(4-
aminophenyl)-amino]propane-1,2-diol, N-(4-[(4-aminophenyl)amino]butyl}benzene-
1,4-
diamine, and 2-[2-(2-{2-[(2,5-diaminophenyl)-oxy]ethoxy}ethoxy)ethoxy]benzene-
1,4-diamine;
1,3-Bis(N(2-Hydroxyethyl)-N-(4-amino-phenyl)amino)-2-propanol; 2,2'-[1,2-
Ethanediyl-bis-
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(oxy-2,l-ethanediyloxy)]-bis-benzene-1,4-diamine; N,N-Bis(2-hydroxyethyl)-p-
phenylinediamine; p-aminophenol derivatives such as: 4-amino-phenol (commonly
known as
p-aminophenol), 4-methylamino-phenol, 4-amino-3-methyl-phenol, 4-amino-2-
hydroxymethyl-
phenol, 4-amino-2-methyl-phenol, 4-amino-l-hydroxy-2-(2'-
hydroxyethylaminomethyl)benzene,
4-amino-2-methoxymethyl-phenol, 5-amino-2-hydroxy-benzoic acid, 1-(5-amino-2-
hydroxy-
phenyl)-ethane-1,2-diol, 4-amino-2-(2-hydroxy-ethyl)-phenol, 4-amino-3-
(hydroxymethyl)-
phenol, 4-amino-3-fluoro-phenol, 4-amino-2-(aminomethyl)-phenol, 4-amino-2-
fluoro-phenol;
1-Hydroxy-2,4-diaminobenzene; 1-(2'-Hydroxyethyloxy)-2,4-diaminobenzene; 2,4-
Diamino-5-
methylphenetol; o-phenylenediamine derivatives such as: 3,4-Diaminobenzoic
acid and salts
thereof; o-aminophenol derivatives such as: 2-amino-phenol (commonly known as
o-aminophenol), 2,4-diaminophenol, 2-amino-5-methyl-phenol, 2-amino-6-methyl-
phenol,
N-(4-amino-3-hydroxy-phenyl)-acetamide, and 2-amino-4-methyl-phenol; and
heterocyclic
derivatives such as: pyrimidine-2,4,5,6-tetramine (commonly known as 2,4,5,6-
tetraamino-
pyridine), 1-methyl-lH-pyrazole-4,5-diamine, 2-(4,5-diamino-lH-pyrazol-1-
yl)ethanol,
NZ,N2-dimethyl-pyridine-2,5-diamine, 2-[(3-amino-6-methoxypyridin-2-
yl)amino]ethanol,
6-methoxy-N2-methyl-pyridine-2,3-diamine, 2,5,6-triaminopyrimidin-4(1H)-one,
pyridine-2,5-
diamine, 1-isopropyl-lH-pyrazole-4,5-diamine, 1-(4-methylbenzyl)-1H-pyrazole-
4,5-diamine,
1-(benzyl)-1H-pyrazole-4,5-diamine, 1-(4-chlorobenzyl)-1H-pyrazole-4,5-
diamine, pyrazolo[1,5-
a]-pyrimidine-3,7-diamine, 5,6,7-trimethylpyrazolo[1,5-a]pyrimidin-3-ylamine
hydrochloride,
7-methylpyrazolo[1,5-a]pyrimidin-3-ylamine hydrochloride, 2,5,6,7-teramethyl-
pyrazolo[1,5-
a]pyrimidin-3-ylamine hydrochloride, 5,7-di-tert-butylpyrazolo[1,5-a]pyrimidin-
3-ylamine
hydrochloride, 5,7-di-trifluoromethyl-pyrazolo[ 1,5-a]pyrimidin-3-ylamine
hydrochloride,
2-methylpyrazolo[1,5-a]pyrimidin-3,7-diamine hydrochloride; 4-hydroxy-2,5,6-
triaminopyrimidine; 1-(2'hydroxyethyl)-amino-3,4-methylene dioxybenzene; and
1-hydroxyethyl-4,5-diaminopyrazole sulphate.
Additional developers include: N-(3-furylmethyl)benzene-1,4-diamine; N-
Thiophen-3-ylmethyl-
benzene- 1,4-diamine; N-(2-furylmethyl)benzene-1,4-diamine; N-Thiophen-2-
ylmethyl-benzene-
1,4-diamine; 4-Hydroxy-benzoic acid (2,5-diamino-benzylidene)-hydrazide; 3-
(2,5-Diamino-
phenyl)-N-ethyl-acrylamide; 2-[3 -(3 -Amino-phenylamino)-propenyl] -benzene-
1,4-diam ine;
2-[3-(4-Amino-phenylamino)-propenyl]-benzene-1,4-diamine; 2-(6-Methyl-pyridin-
2-yl)-
benzene-1,4-diamine; 2-Pyridin-2-yl-benzene-1,4-diamine; 2-[3-(4-Amino-
phenylamino)-
propenylj-benzene-1,4-diamine; 2-[3-(3-Amino-phenylamino)-propenyl]-benzene-
1,4-diamine;
3-(2,5-Diamino-phenyl)-N-ethyl-acrylamide; 2-Thiazol-2-yl-benzene-1,4-diamine;
4-Hydroxy-
benzoic acid (2,5-diamino-benzylidene)-hydrazide; 3'-Fluoro-biphenyl-2,5-
diamine; 2-Propenyl-
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benzene- 1,4-diamine; 2'-Chloro-biphenyl-2,5-diamine; N-Thiophen-3-ylmethyl-
benzene-1,4-
diamine; N-(3-furylmethyl)benzene-1,4-diamine; 4'-Methoxy-biphenyl-2,5-
diamine; N-(4-
Amino-benzyl)-benzene-1,4-diamine; 2-Methyl-5-[(1-H-pyrrol-2-ylmethyl)-amino]-
phenol;
5-[(Furan-2-ylmethyl)-amino]-2-methyl-phenol; 5-Isopropylamino-2-methyl-
phenol; Biphenyl-
2,4,4'-triamine hydrochloride; 5-(4-Amino-phenyl)aminomethyl-benzene-1,3-
diamine
hydrochloride; 5-Phenylaminomethyl-benzene-1,3-diamine hydrochloride; 2-[4-
Amino-2-(3,5-
diamino-benzylamino)-phenoxy]-ethanol hydrochloride; 5-(3-Amino-
phenyl)aminomethyl-
benzene-1,3-diamine hydrochloride; N-(2-Amino-benzyl)-benzene-1,3-diamine
hydrochloride;
N-Furan-2-ylmethyl-benzene-1,3-diamine hydrochloride; 2-[(3-Amino-phenylamino)-
methyl]-
phenol hydrochloride; 4-Amino-2-propylaminomethyl-phenol; hydrochloride;
N-Benzo[1,3]dioxol-5-ylmethyl-benzene-1,3-diamine hydrochloride; N-[4-Amino-2-
(2-hydroxy-
ethyl)-2H-pyrazol-3-yl]-3-(5-amino-2-hydroxy-phenyl)-acrylamide;
hydrochloride; 4-Amino-2-
(isopropylamino-methyl)-phenol; hydrochloride; 4-Thiophen-3-yl-benzene-1,3-
diamine;
hydrochloride hydrochloride; 5-Phenylaminomethyl-benzene-1,3-diamine
hydrochloride;
5-(3-Amino-phenyl)aminomethyl-benzene-1,3-diamine hydrochloride; 4-Thiophen-3-
yl-benzene-
1,3-diamine; hydrochloride; 2',4'-Diamino-biphenyl-4-ol; hydrochloride;
5-Cyclobutylamino-2-methyl-phenol; 5-Cyclobutylamino-2-methyl-phenol; 4-Amino-
2-(pyridin-
3-ylaminomethyl)-phenol; 5-(3-Amino-phenyl)aminomethyl-benzene-1,3-diamine
hydrochloride;
5-Allylaminomethyl-benzene-1,3-diamine hydrochloride; N-(4-Amino-benzyl)-
benzene-1,3-
diamine hydrochloride; N-Benzyl-benzene-1,3-diamine hydrochloride;
3-[(3-Amino-phenylamino)-methyl]-phenol hydrochloride; N-(4-Methoxy-benzyl)-
benzene-1,3-
diamine hydrochloride; N-Thiophen-2-ylmethyl-benzene-1,3-diamine
hydrochloride; 4-Amino-2-
[(2-hydroxy-5-nitro-phenylamino)-methyl]-phenol; hydrochloride; 2',4'-Diamino-
biphenyl-4-ol
hydrochloride; Biphenyl-2,4,4'-triamine; 5-(4-Amino-phenyl)aminomethyl-benzene-
1,3-diamine
hydrochloride; 2-[4-Amino-2-(3,5-diamino-benzylamino)-phenoxy]-ethanol
hydrochloride;
5-Allylaminomethyl-benzene-1,3-diamine hydrochloride; 5-(3-Amino-
phenyl)aminomethyl-
benzene- 1,3-diamine hydrochloride; N-(4-Amino-benzyl)-benzene-1,3-diamine
hydrochloride;
N-Benzyl-benzene-1,3-diamine hydrochloride; 3-[(3-Amino-phenylamino)-methyl]-
phenol
hydrochloride; N-(2-Amino-benzyl)-benzene-1,3-diamine hydrochloride; N-(4-
Methoxy-benzyl)-
benzene- 1,3-diamine hydrochloride; N-Furan-2-ylmethyl-benzene-1,3-diamine
hydrochloride; 2-
[(3-Amino-phenylamino)-methyl]-phenol hydrochloride; N-Thiophen-2-ylmethyl-
benzene-1,3-
diamine hydrochloride; N-Benzo[1,3]dioxol-5-ylmethyl-benzene-1,3-diamine
hydrochloride; N-
[4-Amino-2-(2-hydroxy-ethyl)-2H-pyrazol-3 -yl]-3-(5-amino-2-hydroxy-phenyl)-
acrylamide
hydrochloride; 4-Amino-2-propylaminomethyl-phenol; hydrochloride; 4-Amino-2-
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(isopropylamino-methyl)-phenol hydrochloride; 4-Amino-2-[(2-hydroxy-5-nitro-
phenylamino)-
methyl]-phenol hydrochloride; 2-Methyl-5-[(1-H-pyrrol-2-ylmethyl)-amino]-
phenol; 5-[(Furan-
2-ylmethyl)-amino]-2-methyl-phenol; 5-Isopropylamino-2-methyl-phenol; 5-
Cyclobutylamino-2-
methyl-phenol; 4-Amino-2-(pyridin-3-ylaminomethyl)-phenol; and 5-
Cyclobutylamino-2-
methyl-phenol.
The following compounds are especially suitable as developer compounds: 1,4-
diamino-2,6-
dimethylbenzene, 1,4-diamino-2-methoxymethylbenzene,1,4-diamino-2,5-
dimethylbenzene, 1,4-
diamino-2,3-dimethylbenzene, 2-chloro-1,4-diaminobenzene, 4-
phenylaminoaniline, 4-
dimethylaminoaniline, 4-diethylamino-aniline, 4-[di(2-
hydroxyethyl)amino]aniline, 4-[(2-
methoxyethyl)amino]-aniline, 4-[(3-hydroxypropyl)amino]aniline, 1,4-diamino-2-
(2-
hydroxyethyl)benzene, 1,4-diamino-2-(1-methylethyl)benzene, 1,3-bis-[(4-
aminophenyl)-(2-
hydroxyethyl)amino]-2-propanol, 1,8-bis-(2,5-diaminophenoxy)-3,6-dioxaoctane,
4-
aminophenol, 4-amino-3-methylphenol, 4-methyl-aminophenol, 4-amino-2-
(aminomethyl)phenol, 4-amino-2-[(2-hydroxyethyl)amino]-methylphenol, 4-amino-2-
(methoxymethyl)phenol, 4-amino-2-(2-hydroxyethyl)phenol, 5-amino-salicylic
acid, 2,5-
diaminopyridine, 2,4,5,6-tetraamino-pyrimidine, 2,5,6-triamino-4-(1H)-
pyrimidone, 4,5-diamino-
1-(2-hydroxyethyl)-1H-pyrazole, 4,5-diamino-l-(1-methylethyl)-1H-pyrazole, 4,5-
diamino-l-
[(4-methylphenyl)-methyl]-1H-pyrazole, 1-[(4-chlorophenyl)methyl]-4,5-diamino-
lH-pyrazole,
4,5-diamino-l-methyl-lH-pyrazole, 4,5-diamino-3-methyl-l-phenyl-lH-pyrazole,
4,5-diamino-
1-(2-hydroxyethyl)-3-methyl-lH-pyrazole, 2-amino-phenol and 2-amino-6-
methylphenol, or
their salts.
To produce special shades it is advantageous to use the 3-amino-2,6-
dimethylphenol ot its salts in
combination with additional coupler substances, such as phenols, resorcinol
and naphthol
derivatives such as: naphthalene- 1,7-diol, benzene- 1,3-diol, 4-chlorobenzene-
1,3-diol,
naphthalen-l-ol, 2-methyl-naphthalen-l-ol, naphthalene-1,5-diol, naphthalene-
2,7-diol, benzene-
1,4-diol, 2-methyl-benzene-1,3-diol, 7-amino-4-hydroxy-naphthalene-2-sulfonic
acid, 2-
isopropyl-5-methylphenol, 1,2,3,4-tetrahydro-naphthalene-1,5-diol, 2-chloro-
benzene-1,3-diol, 4-
hydroxy-naphthalene-l-sulfonic acid, benzene- 1,2,3-triol,naphthalene-2,3-
diol, 5-dichloro-2-
methylbenzene-1,3-diol, 4,6-dichlorobenzene-1,3-diol, 2,3-dihydroxy-
[1,4]naphthoquinone; and
1-Acetoxy-2-methylnaphthalene; m-phenylenediamines such as: 2,4-diaminophenol,
benzene-
1,3-diamine, 2-(2,4-diamino-phenoxy)-ethanol, 2-[(3-amino-phenyl)-(2-hydroxy-
ethyl)-amino]-
ethanol, 2-mehyl-benzene-1,3-diamine, 2-[[2-(2,4-diamino-phenoxy)-ethyl]-(2-
hydroxy-ethyl)-
amino]-ethanol, 4-{3-[(2,4-diaminophenyl)oxy]-propoxy}benzene-1,3-diamine, 2-
(2,4-diamino-
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phenyl)-ethanol, 2-(3-amino-4-methoxy-phenylamino)-ethanol, 4-(2-amino-ethoxy)-
benzene-1,3-
diamine, (2,4-diamino-phenoxy)-acetic acid, 2-[2,4-diamino-5-(2-hydroxy-
ethoxy)-phenoxy]-
ethanol, 4-ethoxy-6-methyl-benzene-1,3-diamine, 2-(2,4-diamino-5-methyl-
phenoxy)-ethanol,
4,6-dimethoxy-benzene-1,3-diamine, 2-[3-(2-hydroxy-ethylamino)-2-methyl-
phenylamino]-
ethanol, 3-(2,4-diamino-phenoxy)-propan-l-ol, N-[3-(dimethylamino)phenyl]urea,
4-methoxy-6-
methylbenzene-1,3-diamine, 4-fluoro-6-methylbenzene-1,3-diamine, 2-({3-[(2-
hydroxyethyl)amino]-4,6-dimethoxyphenyl}-amino)ethanol, 3-(2,4-diaminophenoxy)-
propane-
1,2-diol, 2-[2-amino-4-(methylamino)-phenoxy]ethanol, 2-[(5-amino-2-ethoxy-
phenyl)-(2-
hydroxy-ethyl)-amino]-ethanol, 2-[(3-aminophenyl)amino]ethanol, 2,4-Diamino-5-
(2'-
hydroxyethyloxy)toluene; N,N-Dimethyl-3-ureidoaniline; N-(2-aminoethyl)benzene-
1,3-diamine,
4- {[(2,4-diamino-phenyl)oxy]methoxy}-benzene-1,3-diamine, 1-methyl-2,6-bis(2-
hydroxyethylamino)benzene; and 2,4-dimethoxy-benzene-1,3-diamine; m-
aminophenols such as:
3-amino-phenol, 2-(3-hydroxy-4-methyl-phenylamino)-acetamide, 2-(3-hydroxy-
phenylamino)-
acetamide, 5-amino-2-methyl-phenol, 5-(2-hydroxyethylamino)-2-methyl-phenol, 5-
amino-2,4-
dichloro-phenol, 3-amino-2-methyl-phenol, 3-amino-2-chloro-6-methyl-phenol, 5-
amino-2-(2-
hydroxy-ethoxy)-phenol, 2-chloro-5-(2,2,2-trifluoro-ethylamino)-phenol, 5-
amino-4-chloro-2-
methyl-phenol, 3-cyclopentylamino-phenol, 5-[(2-hydroxyethyl)amino]-4-methoxy-
2-
methylphenol, 5-amino-4-methoxy-2-methylphenol, 3-(dimethylamino)phenol, 3-
(diethylamino)phenol, 5-amino-4-fluoro-2-methylphenol, 5-amino-4-ethoxy-2-
methylphenol, 3-
amino-2,4-dichloro-phenol, 3-[(2-methoxyethyl)amino]phenol, 3-[(2-
hydroxyethyl)amino]phenol, 5-amino-2-ethyl-phenol, 5-amino-2-methoxyphenol, 5-
[(3-hydroxy-
propyl)amino]-2-methylphenol, 3-[(3-hydroxy-2-methylphenyl)-amino]propane-1,2-
diol, 3-[(2-
hydroxyethyl)amino]-2-methylphenol; 1-Methyl-2-hydroxy-4-(2'-
hydroxyethyl)amino-benzene;
1,3-Bis-(2,4-Diaminophenoxy)propane; 1-Hydroxy-2-methyl-5-amino-6-
chlorobenzene; and
heterocyclic derivatives such as: 3,4-dihydro-2H-1,4-benzoxazin-6-ol, 4-methyl-
2-phenyl-2,4-
dihydro-3H-pyrazol-3-one, 6-methoxyquinolin-8-amine, 4-methylpyridine-2,6-
diol, 2,3-dihydro-
1,4-benzodioxin-5-ol, 1,3-benzodioxol-5-ol, 2-(1,3-benzodioxol-5-
ylamino)ethanol, 3,4-
dimethylpyridine-2,6-diol, 5-chloropyridine-2,3-diol, 2,6-dimethoxypyridine-
3,5-diamine, 1,3-
benzodioxol-5-amine, 2-{[3,5-diamino-6-(2-hydroxy-ethoxy)-pyridin-2-yl]oxy}-
ethanol, 1H-
indol-4-ol, 5-amino-2,6-dimethoxypyridin-3-ol, 1H-indole-5,6-diol, IH-indol-7-
ol, IH-indol-5-
ol, 1H-indol-6-ol, 6-bromo-1,3-benzodioxol-5-ol, 2-aminopyridin-3-ol, pyridine-
2,6-diamine, 3-
[(3,5-diaminopyridin-2-yl)oxy]propane-1,2-diol, 5-[(3,5-diaminopyridin-2-
yl)oxy]pentane-1,3-
diol, 1H-indole-2,3-dione, indoline-5,6-diol, 3,5-dimethoxypyridine-2,6-
diamine, 6-
methoxypyridine-2,3-diamine; 3,4-dihydro-2H-1,4-benzoxazin-6-amine; 4-hydroxy-
N-
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methylindole, 1H-5-methylpyrazol-5-one, 1-phenyl-3-methylpyrazol-5-one, 2,6-
dimethylpyrazolo[1,5-b]-1,2,4-triazole, 2,6-dimethyl[3,2-c]-1,2,4-triazole, 6-
methylpyrazolo-
[1,5-a]benzimidazole, 2,6-dihydroxypyridine, 2,6-dihydroxy-3,4-
dimethylpyridine, 5-
methylpyrazolo[5,1-e]-1,2,3-triazole, 5-methyl-6-chloropyrazolo[5,1-e]-1,2,3,-
triazole, 5-
phenylpyrazolo[5,1-e]-1,2,3-triazole and its addition salts, 1H-2,6-
dimethylpyrazolo[1,5-b]-1,2,4-
triazole tosylate, 7,8-dicyano-4-methylimidazolo-[3,2-a]imidazole, 2,7-
dimethylpyrazolo[1,5-
a]pyrimidin-5-one, 2,5-dimethylpyrazolo[1,5-a]pyrimidin-7-one, and 2-methyl-5-
methoxymethyl-pyrazolo[1,5-a]pyrimidin-7-one; 6-Hydroxybenzomorpholine; and 3-
Amino-2-
methylamino-6-methoxypyridine; 1-Phenyl-3-methyl-5-pyrazolone-2,4-dihydro-5,2-
phenyl-3H-
pyrazole-3-one, 2-amino-5-ethyl-phenol and 2-amino-5-methyl-phenol.
Preferred coupler substances include: N-(3-dimethylaminophenyl)urea, 2,6-
diaminopyridine,
2-amino-4-[(2-hydroxyethyl)amino]anisole, 2,4-diamino-l-fluoro-5-
methylbenzene,
2,4-diamino-l-methoxy-5-methylbenzene, 2,4-diamino-l-ethoxy-5-methylbenzene,
2,4-diamino-
1-(2-hydroxyethoxy)-5-methylbenzene, 2,4-di-[(2-hydroxyethyl)amino]-1,5-
dimethoxybenzene,
2,3-diamino-6-methoxypyridine, 3-amino-6-methoxy-2-(methylamino)-pyridine, 2,6-
diamino-
3,5-dimethoxypyridine, 3,5-diamino-2,6-dimethoxypyridine, 1,3-diaminobenzene,
2,4-diamino-
1-(2-hydroxyethoxy)benzene, 2,4-diamino-l-(3-hydroxypropoxy)benzene, 1-(2-
aminoethoxy)-
2,4-diaminobenzene, 2-amiono-l-(2-hydroxyethoxy)-4-methylaminobenzene,
2,4-diaminophenoxyacetic acid, 3-[di(2-hydroxyethyl)-amino]aniline, 4-amino-2-
di[(2-
hydroxyethyl)amino]-1-ethoxybenzene, 5-methyl-2-(1-methylethyl)phenol, 3-[(2-
hydroxyethyl)amino]aniline, 3-[(2-aminoethyl)amino]aniline, 1,3-di(2,4-
diaminophenoxy)propane, di-(2,4-diaminophenoxy)methane, 1,3-diamino-2,4-
dimethoxybenzene, 2,6-bis-(2-hydroxyethyl)aminotoluene, 4-hydroxyindol,
3-dimethylaminophenol, 3-diethylaminophenol, 5-amino-2-methylphenol, 5-amino-4-
fluoro-2-
methylphenol, 5-amino-4-methoxy-2-methylphenol, 5-amino-4-ethoxy-2-
methylphenol,
3-amino-2,4-dichlorophenol, 5-amino-2,4-dichlorophenol, 3-amino-2-
methylphenol, 3-amino-2-
chloro-6-methyl-phenol, 3-amino-phenol, 2-[(3-hydroxyphenyl)amino]acetamide,
5-[(2-hydroxyethyl)amino]-2-methylphenol, 3-[(2-hydroxyethyl)amino]-phenol, 3-
[(2-methoxy-
ethyl)amino]-phenol, 5-amino-2-ethylphenol, 2-amino-5-ethyl-phenol, 2-(4-amino-
2-
hydroxyphenoxy)-ethanol, 5-[(3-hydroxypropyl)amino]-2-methylphenol, 3-[(2,3-
dihydroxypropyl)-amino]-2-methyl-phenol, 3-[(2-hydroxyethyl)amino]-2-
methylphenol, 2-
amino-3-hydroxypyridine, 5-amino-4-chloro-2-methylphenol, 1-naphthol, 1,5-
dihydroxy-
naphthalene, 1,7-dihydroxy-naphthalene, 2,3-dihydroxynaphthalene, 2,7-
dihydroxynaphthalene,
2-methyl-l-naphthol acetate, 1,3-dihydroxy-benzene, 1-chloro-2,4-
dihydroxybenzene, 2-chloro-
CA 02646867 2008-12-16
W245FQ/JC 8
1,3-dihydroxybenzene, 1,2-dichloro-3,5-dihydroxy-4-methylbenzene, 1,5-dichloro-
2,4-
dihydroxybenzene, 1,3-dihydroxy-2-methylbenzene, 3,4-methylenedioxyphenol, 3,4-
methylenedioxy-aniline, 5-[(2-hydroxyethyl)amino]-1,3-benzodioxole, 6-bromo-l-
hydroxy-3,4-
methylendioxybenzene, 3,4-diaminobenzoic acid, 3,4-dihydro-6-hydroxy-1,4(2H)-
benzoxazine,
6-amino-3,4-dihydro-1,4(2H)-benzoxazine, 3-methyl-l-phenyl-5-pyrazolone, 5,6-
dihydroxyindole, 5,6-dihydroxyindoline, 5-hydroxy-indole, 6-hydroxyindole, 7-
hydroxy-indole
and 2,3-indolindione, or their salts.
The hair dye compositions of the present invention will generally comprise
from about 0.001 /a to
about 15% by weight of dye precursors. For example compositions providing low
intensity
dyeing such as natural blond to light brown hair shades generally comprise
from about 0.001% to
about 7% by weight, preferably from about 0.1% to about 5% by weight, more
preferably from
about 0.2% to about 2% by weight of dyeing composition of precursors and
couplers. Darker
shades such as browns and black typically comprise from 0.001% to about 15% by
weight,
preferably from about 0.05% to about 10% by weight, more preferably form about
1% to about
5% by weight of precursors and couplers.
The developer substances and coupler substances are generally used in
approximately equimolar
amounts; however, it is not disadvantageous if the developer substances are
present in this regard
in a certain excess or deficit, for example a coupler:developer ratio of 1:3
to 1:0.3.
The hair colouring compositions of the present invention are preferably hair
colouring
compositions which comprise oxidative dyeing compositions. Such compositions
comprise
oxidative hair dye precursors (also known as primary intermediates) that will
deliver a variety of
hair colors to the hair. These small molecules are activated by the oxidizing
agent and react with
further molecules to form a larger colored complex in the hair shaft. The
precursors may be used
alone or in combination with other precursors, and one or more may be used in
combination with
one or more couplers. Couplers (also known as color modifiers or secondary
intermediates) are
generally colorless molecules that can form colors in the presence of
activated precursors, and are
used with other precursors or couplers to generate specific color effects or
to stabilize the color.
The choice of precursors and couplers will be determined by the color, shade
and intensity of
coloration that is desired. The precursors and couplers may be used herein,
singly or in
combination, to provide dyes having a variety of shades ranging from ash
blonde to black.
CA 02646867 2008-12-16
W245FQ/JC 9
Nevertheless the hair colouring compositions of the present invention
comprising at least one
compound of formula (I) may also include non-oxidative hair dyes (i.e. direct
dyes) which may
be used alone or in combination with the above described oxidative dyes.
Suitable direct dyes
include: direct-dyeing anionic, cationic or non-ionic dye compounds.
The following are preferred examples of anionic direct-dyeing dye compounds
for use in the
compositions of the invention: 6-hydroxy-5-[(4-sulfophenyl)azo]-2-naphthalene
sulfonic acid
disodium salt (C.I. 15985; Food Yellow No. 3; FD&C Yellow No. 6), 2,4-dinitro-
l-naphthol-7-
sulfonic acid disodium salt (C.I. 10316; Acid Yellow No. 1; Food Yellow No.
1), 2-(indan-l,3-
dion-2-yl)quinoline-x,x-sulfonic acid (mixture of mono- and disolfuonic acid)
(C.I.47005;D&C
Yellow No. 10; Food Yellow No. 13, Acid Yellow No. 3), 5-hydroxy-1-(4-
sulfophenyl)-4-[(4-
sulfophenyl)azo]pyrazole-3-carboxylic acid sodium salt (C.I. 19140; Food
Yellow No. 4; Acid
Yellow No. 23), 9-(2-carboxyphenyl)-6-hydroxy-3H-xanthen-3-one (C.I.45350;
Acid Yellow
No. 73; D&C Yellow No. 8), 5-[(2,4-dinitrophenyl)amino]-2-
phenylaminobenzenesulfonic acid
sodium salt (C.1.10385; Acid Orange No. 3), 4-[(2,4-dihydroxyphenyl)azo]-
benzene sulfonic acid
monosodium salt (C.I.14270; Acid Orange No. 6), 4-[(2-hydroxynaphth-l-
yl)azo]benzenesulfonic acid sodium salt (C.I. 15510; Acid Orange No. 7), 4-
[(2,4-dihydroxy-3-
[(2,4-dimethylphenyl)azo]phenyl)azo]-benzene sulfonic acid sodium salt
(C.I.20170; Acid
Orange No. 24), 4-hydroxy-3-[(4-sulfonaphth-l-yl)azo]-1-naphthalene sulfonic
acid disodium
salt (C.I. 14720; Acid Red No. 14), 6-hydroxy-5-[(4-sulfonaphth-l-yl)azo]-2,4-
naphthalene-
disulfonic acid trisodium salt (C.I. 16255; Ponceau 4R; Acid Red No. 18), 3-
hydroxy-4-[(4-
sulfonaphth-l-yl)azo]-2,7-naphthalene-disulfonic acid trisodium salt (C.I.
16185; Acid Red No.
27), 8-amino-l-hydroxy-2-(phenylazo)-3,6-naphthalene disulfonic acid disodium
salt (C.I.17200;
Acid Red No. 33), 5-(acetylamino)-4-hydroxy-3-[(2-methylphenyl)azo]-2,7-
naphthalene
disulfonic acid disodium salt (C.I.18065; Acid Red No. 35), 2-(3-hydroxy-
2,4,5,7-tetraiodo-
dibenzopyran-6-on-9-yl)-benzene sulfonic acid disodium salt (C.I. 45430; Acid
Red No. 51), N-
[6-(diethylamino)-9-(2,4-disulfophenyl)-3H-xanthen-3-yliden]-N-
ethylethanaminium hydroxide,
inner Salt, sodium salt (C.1.45100; Acid Red No. 52), 8-[(4-
(phenylazo)phenyl)azo]-7-naphthol-
1,3-disulfonic acid disodium salt (C.I. 27290; Acid Red No. 73),
2',4',5',7'-tetrabromo-3',6'-dihydroxyspiro[isobenzofuran-l-(3H),9'-
[9H]xanthen]-3-one disodium
salt (C.1.45380; Acid Red No. 87), 2',4',5',7'-tetrabromo-4,5,6,7-tetrachloro-
3',6'-
dihydroxyspiro[isobenzofuran-1(3H),9'[9H]xanthen]-3-one disodium salt (C.I.
45410; Acid Red
No. 92), 3',6'-dihydroxy-4',5'-diiodospiro[isobenzofuran-1(3H),9'(9H)-xanthen)-
3-one disodium
salt (C.I. 45425; Acid Red No. 95), (2-sulfophenyl)-di-[4-(ethyl-((4-
sulfophenyl)methyl)-
CA 02646867 2008-12-16
W245FQ/JC 10
amino)phenyl]carbenium disodium salt, betaine (C.I. 42090; Acid Blue No.9;
FD&C Blue No.1),
1,4-bis-[(2-sulfo-4-methyl-phenyl)amino]-9,10-anthraquinone disodium salt
(C.I. 61570; Acid
Green No. 25), bis-[4-(dimethylamino)phenyl]-(3,7-disulfo-2-hydroxynaphth-1-
yl)carbenium
inner salt, monosodium salt (C.I. 44090; Food Green No. 4; Acid Green No. 50),
bis-[4-
(diethylamino)phenyl](2,4-disulfophenyl)carbenium inner salt, sodium salt
(2:1) (C.I. 42045;
Food Blue No. 3; Acid Blue No. 1), bis[4-(diethylamino)phenyl]-(5-hydroxy-2,4-
disulfophenyl)carbenium inner salt, calcium salt (2:1) (C.I. 42051; Acid Blue
No. 3), 1-amino-4-
(cyclohexylamino)-9,10-anthraquinone-2-sulfonic acid sodium salt (C.I. 62045;
Acid Blue No.
62), 2-(1,3-dihydro-3-oxo-5-sulfo-2H-indol-2-yliden)-2,3-dihydro-3-oxo-lH-
indol-5-sulfonic
acid disodium salt (C.I. 73015; Acid Blue No. 74), 9-(2-carboxyphenyl)-3-[(2-
methylphenyl)-
amino] 6-[(2-methyl-4-sulfophenyl)amino]xanthylium inner salt, monosodium salt
(C.I. 45190;
Acid Violet No. 9), 1-hydroxy-4-[(4-methyl-2-sulfophenyl)amino]-9,10-
anthraquinone sodium
salt (C.I. 60730; D&C Violet No. 2; Acid Violet No. 43), bis-[3-nitro-4-[(4-
phenylamino)-3-
sulfophenylami no]phenyl]-sulfone (C.I. 10410; Acid Brown No. 13), 5-amino-4-
hydroxy-6-[(4-
nitrophenyl)azo]3-(phenylazo)-2,7-naphthalene disulfonic acid disodium salt
(C.1.20470; Acid
Black No. 1), 3-hydroxy-4-[(2-hydroxynaphth-1-yl)azo]-7-
nitronaphthalenesulfonic acid
chromium complex (3:2) (C.I. 15711; Acid Black No. 52), 3-[(2,4-dimethyl-5-
sulfophenyl)azo]-
4-hydroxy-l-naphthalene-sulfonic acid disodium salt (C.I. 14700; Food Red No.
1; Ponceau SX;
FD&C Red No. 4), 4-(acetylamino)-5-hydroxy-6-[(7-sulfo-4-[(4-
sulfophenyl)azo]naphth-1
yl)azo]-1,7-naphthalene disulfonic acid tetrasodium salt (C.I. 28440; Food
Black No. 1),
3-hydroxy-4-(3-methyl-5-oxo-l-phenyl-4,5-dihydro-1 H-pyrazole-4-yl-azo)-
naphthalene-l-
sulfonic acid sodium salt chromium complex (Acid Red No. 195), 6-hydroxy-5-((2-
methoxy-5-
methyl-4-sulfophenyl)azo)-2-naphthalene sulfonic acid disodium salt (FD&C Red
No.40; Red
40; C.I.16035), 3-hydroxy-4-[(4-methyl-2-sulfophenyl)azo]-2-
naphthalenecarboxylic acid
Disodium salt (Pigment Red 57; C.I.15850) and 4,4'-(4,5,6,7-tetrabromo-l, 1-
dioxido-3H-2, 1-
benzoxathiol-3-ylidene)bis[2,6-dibromophenol] (Tetrabromophenol Blue).
The following are preferred cationic direct-dyeing dye compounds: 9-
(dimethylamino)-
benzo[a]phenoxazin-7-ium chloride (C.I. 51175; Basic Blue No. 6), di[4-
(diethylamino)phenyl]-
[4-(ethylamino)naphthyl]carbenium chloride (C.I. 42595; Basic Blue No. 7),
3,7-di(dimethylamino)phenothiazin-5-ium chloride (C.I. 52015; Basic Blue No.
9), di[4-
dimethylamino)phenyl][4(phenylamino)naphthyl]carbenium chloride (C.I. 44045;
Basic Blue
No. 26), 2-[(4-(ethyl(2-hydroxyethyl )amino)phenyl )azo]-6-methoxy-3-
methylbenzothiazol ium
methylsulfate (C.I. 11154; Basic Blue No. 41), 8-amino-2-bromo-5-hydroxy-4-
imino-6-[(3-
CA 02646867 2008-12-16
W245FQ/JC 11
(trimethylammonio)phenyl)amino]-1 (4H)naphthalenone chloride (C.I.56059; Basic
Blue No.
99), bis-[4-(dimethylamino)phenyl][4-(methylamino)phenyl]carbenium chloride
(C.I. 42535;
Basic Violet No. 1), tris-(4-amino-3-methylphenyl)carbenium chloride (C.I.
42520; Basic Violet
No. 2), tris-[4-(dimethylamino)phenyl]carbenium chloride (C.I. 42555; Basic
Violet No. 3),
2-[3,6-(diethylamino)dibenzopyranium-9-yl]benzoic acid chloride (C.I. 45170;
Basic Violet No.
10), di(4-aminophenyl)(4-amino-3-methylphenyl)carbenium chloride (C.I. 42510;
Basic Violet
No. 14), 1,3-bis[(2,4-diamino-5-methylphenyl)azo]-3-methylbenzene (C.I.
21010;Basic Brown
No. 4), 1-[(4-aminophenyl)azo]-7-(trimethylammonio)-2-naphthol chloride (C.I.
12250; Basic
Brown No. 16), 1-[(4-amino-2-nitrophenyl)azo]-7-(trimethylammonio)-2-naphthol
chloride (C.I.
12251; Basic Brown No.l7), 1-[(4-amino-3-nitrophenyl)azo]-7-(trimethylammonio)-
2-naphthol
chloride (C.I. 12251; Basic Brown No. 17), 2-[(4-aminophenyl)azo]-1,3-dimethyl-
IH-
imidazolium chloride (Basic Orange No. 31), 3-[(4-amino-2,5-
dimethoxyphenyl)azo]-N,N,N-
trimethyl-benzeneaminium chloride (Basic Orange No. 69), 3,7-diamino-2,8-
dimethyl-5-
phenylphenazinium chloride (C.I. 50240; Basic Red No. 2), 1,4-dimethyl-5-
[(4(dimethylamino)phenyl)azo]-1,2,4-triazolium chloride (C.I. 11055; Basic Red
No. 22), 2-((4-
(Dimethylamino)-phenyl)azo)-1,3-dimethyl-IH-imidazolium chloride (Basic Red
No. 51), 2-
hydroxy-l-[(2-methoxyphenyl)azo]-7-(trimethylammonio)naphthalene chloride
(C.I. 12245;
Basic Red No. 76), 2-[2-((2,4-dimethoxyphenyl)amino)ethenyl]-1,3,3-trimethyl-
3H-indol-l-ium-
chloride (C.I. 48055; Basic Yellow No. 11), 3-methyl-l-phenyl-4-[(3-
(trimethylammonio)phenyl)azo]-pyrazole-5-one chloride (C.I. 12719; Basic
Yellow No. 57), 4-
Methyl-(phenyl-hydrazonomethyl)-pyridinium-methylsulfate (Basic Yellow No.
87), bis-[4-
(diethylamino)phenyl]phenylcarbenium hydrogen sulfate(1:1) (C.I. 42040; Basic
Green No. 1),
4-[(2,6-dichlorphenyl)(4-imino-3,5-dimethyl-2,5-cyclohexadien-l-
ylidene)methyl]-2,6-dimethyl-
benzeneamine phosphate (HC Blue No. 15; Basic Blue No. 77) and N,N-dimethyl-3-
{[4-
(methylamino)-9,10-dioxo-9,10-dihydro-l-anthracenyl]amino) -N-propyl-l-
propanamin.ium
bromide (HC Blue No. 16).
To improve the color balance and to produce special shades the following
nonionic direct-dyeing
dye compounds have proven to be useful in the compositions according to the
invention:
1-amino-2-[(2-hydroxyethyl)amino]-5-nitrobenzene (HC Yellow No. 5), 1-(2-
hydroxyethoxy)-2-
[(2-hydroxyethyl)amino]-5-nitrobenzene (HC Yellow No. 4), 1-[(2-
hydroxyethyl)amino]-2-
nitrobenzene (HC Yellow No. 2), 2-[(2-hydroxyethyl)amino]-1-methoxy-5-
nitrobenzene,
2-nitro-p-phenylenediamine, 4-nitro-p-phenylenediamine, N,N'-bis(2-
hydroxyethyl)-2-nitro-p-
phenylenediamine, 2-hydroxyethylamino-5-nitroanisole, 3-methylamino-4-
nitrophenoxyethanol,
CA 02646867 2008-12-16
W245FQ/JC 12
2-nitro-5-glyceryl-methylaniline, N-(2-nitro-4-aminophenyl)-allylamine, 2-
amino-3-nitrophenol,
1-(2-hydroxyethoxy)-3-methylamino-4-nitrobenzene, 2,3-(dihydroxy-propoxy)-3-
methylamino-
4-nitrobenzene, 2-[(2-hydroxyethyl)amino]-5-nitrophenol (HC Yellow No. 11), 3-
[(2-
aminoethyl)amino]-1-methoxy-4-nitrobenzene hydrochloride (HC Yellow No.9), 1-
[(2-
ureidoethyl)amino]-4-nitrobenzene, 4-[(2,3-dihydroxypropyl )amino]-3-nitro-l-
trifluoromethylbenzene (HC Yellow No. 6), 1-chloro-2,4-bis-[(2-
hydroxyethyl)amino]-5-
nitrobenzene (HC Yellow No. 10), 4-[(2-hydroxyethyl)amino]-3-nitro-l-
methylbenzene,
1-chloro-4-[(2-hydroxyethyl)amino]-3-nitrobenzene (HC Yellow No. 12), 4-[(2-
hydroxyethyl)-
amino]-3-nitro-l-trifluoromethylbenzene (HC Yellow No. 13), 4-[(2-
hydroxyethyl)amino]-3-
nitrobenzonitrile (HC Yellow No. 14), 4-[(2-hydroxyethyl)amino]-3-
nitrobenzamide (HC Yellow
No. 15), 1-amino-4-[(2-hydroxyethyl)amino]-2-nitrobenzene (HC Red No. 7), 2-
amino-4,6-
dinitrophenol, 2-ethylamino-4,6-dinitrophenol, 4-amino-2-nitrodiphenylamine
(HC Red No. 1),
1-amino-4-[di(2-hydroxyethyl)amino]-2-nitrobenzene hydrochloride (HC Red No.
13),
1-amino-5-chloro-4-[(2hydroxyethyl)amino]-2-nitrobenzene, 4-amino-l-[(2-
hydroxyethyl)-
amino]-2-nitrobenzene (HC Red No. 3), 4-amino-3-nitrophenol, 4-[(2-
hydroxyethyl)amino]-3-
nitrophenol, 1-[(2-aminoethyl)amino]4-(2-hydroxyethoxy)-2-nitrobenzene (HC
Orange No. 2),
4-(2,3-dihydroxypropoxy)-1-[(2-hydroxyethyl)amino]-2-nitrobenzene (HC Orange
No. 3),
1 -amino-5-chloro-4-[(2,3-dihydroxypropyl)amino]-2-nitrobenzene (HC Red No.
10), 5-chloro-
1,4-[di(2,3-dihydroxypropyl)amino]-2-nitrobenzene (HC Red No. 11), 2-[(2-
hydroxyethyl)-
amino]4,6-dinitrophenol, 4-ethylamino-3-nitrobenzoic acid, 2-[(4-amino-2-
nitrophenyl)amino]-
benzoic acid, 2-chloro-6-methylamino-4-nitrophenol2-chloro-6-[(2-
hydroxyethyl)amino]4-
nitrophenol, 2-chloro-6-ethylamino-4-nitrophenol, 2-amino-6-chloro-4-
nitrophenol,
4-[(3-hydroxypropyl )-amino]-3-nitrophenol, 2,5-diamino-6-nitropyridine,
1,2,3,4-tetrahydro-6-
nitrochinoxalin, 7-amino-3,4-dihydro-6-nitro-2H-1,4-benzoxazine (HC Red No.
14),1,4-bis-[(2-
hydroxyethyl )-amino]-2-nitrobenzene, 1-(2-hydroxyethyl )ami no-2-nitro-4-
[di(2-
hydroxyethyl)amino]benzene (HC Blue No. 2), 1-amino-3-methyl-4-[(2-
hydroxyethyl)amino]-6-
nitrobenzene (HC Violet No. 1), 4-[ethyl-(2-hydroxyethyl)amino]-1-[(2-
hydroxyethyl)amino]-2-
nitrobenzene hydrochloride (HC Blue No. 12), 4-[di(2-hydroxyethyl)amino]-1-[(2-
methoxyethyl
)amino] -2-nitrobenzene (HC Blue No. 11), 1-[(2,3-dihydroxy-propyl)amino]4-
[methyl-(2-
hydroxyethyl)amino]-2-nitrobenzene (HC Blue No. 10), 1-[(2,3-
dihydroxypropyl)amino]4-
[ethyl-(2-hydroxyethyl)amino]-2-nitrobenzene hydrochloride (HC Blue No. 9),
hydroxyethyl-2-
nitro-p-toluidine, 1-(3-hydroxypropylamino)-4-[di(2-hydroxyethyl)amino]-2-
nitrobenzene (HC
Violet No. 2), 1-methylamino-4-[methyl-(2,3-dihydroxypropyl)amino]-
2nitrobenzene (HC Blue
No. 6), 3-nitro-p-hydroxyethylaminophenol, 2-((4-amino-2-nitrophenyl)amino)-5-
CA 02646867 2008-12-16
W245FQ/JC 13
dimethylamino-benzoic acid (HC Blue No. 13), 1,4-Bis[2,3-Dihydroxypropylamino]-
9,10-
anthracenedione (HC Blue No. 14), 2-nitro-4'-hydroxy-diphenylamine (HC Orange
No. 1),
1-[(2-hydroxyethyl)amino]4-methylamino-9,10-anthraquinone (C.I. 61505,
Disperse Blue No. 3),
2,2'-[[4-[(4-aminophenyl)azo]phenyl]-imino]-bisethanol (Disperse Black No. 9),
2-[(2-aminoethyl)amino]-9,10-anthraquinone (HC Orange No. 5), 1 -hydroxy-4-[(4-
methyl-2-
sulfophenyl)amino]-9,10-anthraquinone, 1-[(3-aminopropyl)amino]-4-methylamino-
9,10-
anthraquinone (HC Blue No. 8), 1,4-diamino-anthraquinone (Disperse Violet No.
1), 1-[(3-
aminopropyl)amino]-9,10-anthraquinone (HC Red No. 8), 1,4-diamino-2-methoxy-
9,10-
anthraquinone (C.I.62015, disperse Red No. 11, Solvent Violet No. 26), 1,4-
dihydroxy-5,8-
bis[(2-hydroxyethyl)amino-9,10-anthraquinone (C.I. 62500, disperse Blue No. 7,
Solvent Blue
No. 69), 1-[di-(2-hydroxyethyl)amino]-3-methyl-4-[(4-nitrophenyl)azo]benzene
(C.I. 11210,
disperse Red No. 17), 4-amino-2-nitrophenylamine-2'-carboxylic acid, 4-[(4-
aminophenyl)azo]-
1-[di(2-hydroxyethyl)amino]-3-methylbenzene (HC Yellow No. 7), 2,6-diamino-3-
[(pyridine-3-
yl)azo]pyridine, hydroxyanthraquinone-aminopropylmethyl-morpholinium-
methosulfate, 2,5-
dihydroxy-3-methoxy-6-methyl-1,4-benzoquinone, 2-((4-(acetylamino)phenyl)-azo)-
4-
methylphenol (C.I. 11855; disperse Yellow No. 3), 2-hydroxy-1,4-naphthoquinone
(Lawsone), 4-
nitrophenyl-aminoethylurea, picramic acid, 2-hydroxyethyl-picramic acid, 1,4-
di((2-
hydroxyethyl)amino)-9,10-anthracendione, 1,4-di((3-hydroxypropyl)amino)-9,10-
anthracendione
and 1-((2-hydroxyethyl)amino)-4-((3-hydroxypropyl)amino)-9,10-anthracendione
(Disperse Blue
377; C.I.615061).
The following compounds may also be used as direct-dyeing dye compounds:
natural dyes like
Indigofera Tinctoria and Henna (Lawsonia lnermis) or nitrophenols like 2-amino-
4,6-
dinitrophenol, 2-ethylamino-4,6-dinitrophenol, 2-[(2-hydroxyethyl)-amino]4,6-
dinitrophenol and
dye compounds of the following general formula (VII):
H
CI NHR
NO2 formula (VII)
wherein R represents hydrogen, methyl, ethyl or hydroxyethyl.
CA 02646867 2008-12-16
W245FQ/JC 14
The hair dye compositions of the present invention will generally comprise
from about 0.001% to
about 10% by weight of direct dyes, preferably from about 0.1 % to about 5% by
weight, more
preferably from about 0.2% to about 2% by weight.
The composition of the present invention comprising at least one compound of
formula (I) and
optionally additional oxidation dye precursor compounds and/or direct-dyeing
dye compounds is
applied to the fibers to be dyed in a suitable dye-carrying composition.
The present invention also relates to ready-to-apply hair dye mixtures for the
oxidative dyeing of
hair, which are each made by mixing an oxidation dye precursor composition
with an oxidizing
agent immediately prior to application. They are characterized by a content of
at least one
compound of formula (I) as well as additional oxidation dye precursor
compounds and/or direct-
dyeing dye compounds as needed.
Any oxidizing agent known in the art (including air-oxgen and enzyme-based
oxidizing systems)
may be utilized in the present invention. Preferred water-soluble oxidizing
agents are inorganic
peroxygen materials capable of yielding hydrogen peroxide in an aqueous
solution. Water-
soluble peroxygen oxidizing agents are well known in the art and include
hydrogen peroxide,
inorganic alkali metal peroxides such as sodium periodate and sodium peroxide
and organic
peroxides such as urea peroxide, melamine peroxide, and inorganic perhydrate
salt bleaching
compounds, such as the alkali metal salts of perborates, percarbonates,
perphosphates,
persilicates, persulphates and the like. These inorganic perhydrate salts may
be incorporated as
monohydrates, tetrahydrates etc. Alkyl and aryl peroxides, and or peroxidases
may also be used.
Mixtures of two or more such oxidizing agents may also be used if desired. The
oxidizing agents
may be provided in aqueous solution or as a powder which is dissolved prior to
use. Preferred for
use in the compositions according to the present invention are hydrogen
peroxide, percarbonate,
persulphates and combinations thereof.
According to the present invention the compositions comprise from 0.1% to
about 15% by
weight, preferably from 1% to 10% by weight, and most preferably from 2% to 7%
by weight of
an oxidizing agent.
CA 02646867 2008-12-16
W245FQ/JC 15
Another preferred oxidizing agent for use herein is a source of
peroxymonocarbonate ions.
Preferably such a source is formed in situ from a source of hydrogen peroxide
and a hydrogen
carbonate ion source. Such an oxidizing agent has been found to be
particularly effective at a pH
of up to and including 9.5, preferably 7.5 to 9.5 more preferably pH 9.
Moreover, this system is
also particularly effective in combination with a source of ammonia or
ammonium ions. It has
been found that this oxidizing agent can deliver improvements to the desired
hair colour results
particularly with regard to the delivery of high lift, whilst considerably
reducing the odour, skin
and scalp irritation and damage to the hair fibres.
Accordingly, any source of these ions may be utilized. Suitable sources for
use herein include
sodium, potassium, guanidine, arginine, lithium, calcium, magnesium, barium,
ammonium salts
of carbonate, carbamate and hydrocarbonate ions and mixtures thereof such as
sodium carbonate,
sodium hydrogen carbonate, potassium carbonate, potassium hydrogen carbonate,
guanidine
carbonate, guanidine hydrogen carbonate, lithium carbonate, calcium carbonate,
magnesium
carbonate, barium carbonate, ammonium carbonate, ammonium hydrogen carbonate
and
mixtures thereof. Percarbonate salts may also be utilized to provide both the
source of carbonate
ions and oxidizing agent. Preferred sources of carbonate ions, carbamate and
hydrocarbonate ions
are sodium hydrogen carbonate, potassium hydrogen carbonate, ammonium
carbamate, and
mixtures thereof.
According to the present invention the compositions comprise from 0.1% to
about 15% by
weight, preferably from 1% to 10% by weight, and most preferably from 1% to 8%
by weight of
a hydrogencarbonate ion and from 0.1% to 10% by weight, preferably from 1% to
7% by weight,
and most preferably from 2% to 5% by weight of a source of hydrogen peroxide.
According to the present invention the composition may further optionally
comprise at least one
source of alkalizing agent, preferably a source of ammonium ions and or
ammonia. Any agent
known in the art may be used such as alkanolamides for example
monoethanolamine,
diethanolamine, triethanolamine, monopropanolamine, dipropanolamine,
tripropanolamine,
2-amino-2-methyl-1, 3-propanediol, 2-amino-2-methyl-l-propanol, and 2-amino-2-
hydroxymethyl-1,3-propanediol and guanidium salts. Particularly, preferred
alkalizing agents are
those which provide a source of ammonium ions. Any source of ammonium ions is
suitable for
use herein. Preferred sources include ammonium chloride, ammonium sulphate,
ammonium
nitrate, ammonium phosphate, ammonium acetate, ammonium carbonate, ammonium
hydrogen
CA 02646867 2008-12-16
W245FQ/JC 16
carbonate, ammonium carbamate, ammonium hydroxide, percarbonate salts, ammonia
and
mixtures thereof. Particularly preferred are ammonium carbonate, ammonium
carbamate,
ammonium hydrogen carbonate, ammonia and mixtures thereof. The compositions of
the present
invention may comprise from 0.1% to 10% by weight, preferably from 0.5% to 5%
by weight,
most preferably from 1% to 3% by weight, of an alkalizing agent, preferably
ammonium ions.
According to the present invention the compositions may further comprise a
source of radical
scavenger. As used herein the term radical scavenger refers to a species that
can react with a
reactive radical, preferably carbonate radicals, to convert the reactive
radical by a series of fast
reactions to a less reactive species.
Suitable radical scavengers for use herein include compounds according to the
general formula
(RSI):
R''-Y-C(H)(R3 )-R4 -(C(H)(RS )-Y-R6')n (RSI)
wherein Y is NRZ', 0, or S, preferably NR2', n is 0 to 2, and wherein R4' is
monovalent or
divalent and is selected from: (a) substituted or unsubstituted, straight or
branched, alkyl, mono-
or polyunsaturated alkyl, heteroalkyl, aliphatic, heteroaliphatic, or
heteroolefinic systems, (b)
substituted or unsubstituted, mono- or polycyclic aliphatic, aryl, or
heterocyclic systems, or (c)
substituted or unsubstituted, mono-, poly-, or perfluoro alkyl systems; the
systems of (a), (b) and
(c) comprising from 1 to 12 carbon atoms and 0 to 5 heteroatoms selected from
0, S, N, P, and
Si; and wherein R4' may be connected to R3' or RS' to create a 5, 6 or 7-
membered ring; and
wherein R'', R2', R3', RS', and R6' are monovalent and are selected
independently from: (a), (b)
and (c) described herein above, or H.
Preferably, R4' is selected from: (a) substituted or unsubstituted, straight
or branched, alkyl,
heteroalkyl, aliphatic, heteroaliphatic, or heteroolefinic systems, (b)
substituted or unsubstituted,
mono- or polycyclic aliphatic, aryl, or heterocyclic systems, or (c)
substituted or unsubstituted,
mono-, poly-, or perfluoro alkyl systems; more preferably R4' is selected from
(a) substituted or
unsubstituted, straight or branched, alkyl, heteroalkyl, aliphatic, or
heteroaliphatic systems, (b)
substituted or unsubstituted, aryl, or heterocyclic systems, or (c)
substituted or unsubstituted,
mono-, poly-, or perfluoro alkyl systems; more preferably substituted or
unsubstituted, straight or
branched, alkyl, or heteroalkyl systems.
CA 02646867 2008-12-16
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Preferably, the R4' systems of (a), (b), and (c), described herein above,
comprise from 1 to 8
carbon atoms, preferably from 1 to 6, more preferably from 1 to 4 carbon atoms
and from 0 to 3
heteroatoms; preferably from 0 to 2 heteroatoms; most preferably from 0 to I
heteroatoms.
Where the systems contain heteroatoms, preferably they contain 1 heteroatom.
Preferred
heteroatoms include 0, S, and N; more preferred are 0, and N; and most
preferred is O.
Preferably, R", R2', R3', R5', and R6' are selected independently from any of
the systems defined
for R4 above, and H.
In alternative embodiments, any of R'', R2', R3', R4', R5', and R6' groups are
substituted.
Preferably, the substituent(s) is selected from: (a) the group of C-linked
monovalent substituents
consisting of: (i) substituted or unsubstituted, straight or branched, alkyl,
mono- or poly-
unsaturated alkyl, heteroalkyl, aliphatic, heteroaliphatic, or heteroolefinic
systems, (ii) substituted
or unsubstituted, mono- or polycyclic aliphatic, aryl, or heterocyclic
systems, or (iii) substituted
or unsubstituted, mono-, poly-, or perfluoro alkyl systems; said systems of
(i), (ii) and (iii)
comprising from I to 10 carbon atoms and 0 to 5 heteroatoms selected from 0,
S, N, P, and Si;
(b) the group of S-linked monovalent substituents consisting of SA1, SCN,
SO2A', SO3A', SSA',
SOA', SO2NA'A2, SNA'AZ, and SONA'A2; (c) the group of 0-linked monovalent
substituents
consisting of OAI, OCN and ONAlA2; (d) the group of N-linked monovalent
substituents
consisting ofNA'AZ, (NA'A2A 3 )+, NC, NA'OA2, NA'SA2, NCO, NCS, NOZ, N NA',
N=NOA',
NA'CN, NA'NA2A3; (e) the group of monovalent substituents consisting of COOAi,
CON3,
CONA'2, CONA'COA2, C(=NA')NA'A2, CHO, CHS, CN, NC, and X; and (f) the group
consisting fluoroalkyl monovalent substituents consisting of mono-, poly-, or
per-fluoro alkyl
systems comprising from 1 to 12 carbon atoms and 0 to 4 heteroatoms.
For the groups (b) to (e), described above, A', AZ, and A3 are monovalent and
are independently
selected from: (1) H, (2) substituted or unsubstituted, straight or branched,
alkyl, mono- or poly-
unsaturated alkyl, heteroalkyl, aliphatic, heteroaliphatic, or heteroolefinic
systems, (3) substituted
or unsubstituted, mono- or polycyclic aliphatic, aryl, or heterocyclic
systems, or (4) substituted or
unsubstituted, mono-, poly-, or perfluoro alkyl systems; said systems of (2),
(3) and (4)
comprising from 1 to 10 carbon atoms and 0 to 5 heteroatoms selected from 0,
S, N, P, and Si;
and wherein X is a halogen selected from the group consisting of F, Cl, Br,
and I.
Preferred substituents for use herein include those having a Hammett Sigma
Para (ap) Value from
CA 02646867 2008-12-16
W245FQ/JC 18
-0.65 to +0.75, preferably from -0.4 to +0.5. Hammett Sigma Values are
described in Advanced
Organic Chemistry - Reactions, Mechanisms and Structure (Jerry March, 5`h ed.
(2001) at pages
368-375).
Alternative suitable radical scavengers for use herein are compounds according
to the general
formula (RSII)
H
R" R"
5 ~ 1
I /
R4" R
2"
R
3
(RSII)
wherein Rl >, RZ==, R3 , R4,=, and R5 are each independently selected from H,
COO-M+, Cl, Br,
SO3"M}, NO2, OCH3, OH or a C1 to C10 primary or secondary alkyl and M is
either H or alkali
metal. Preferably, the above-described radical scavengers have a pKa of more
than 8.5 to ensure
protonation of the hydroxy goup.
Other suitable radical scavengers for use herein include those selected from
group (III)
benzylamine, imidazole, di-tert-butylhydroxytoluene, hydroquinone, guanine,
pyrazine,
piperidine, morpholine, methylmorpholine, 2-methyoxyethylamine, and mixtures
thereof.
Preferred radical scavengers according to the present invention are selected
from the classes of
alkanolamines, amino sugars, amino acids, esters of amino acids and mixtures
thereof.
Particularly preferred compounds are: monoethanolamine, 3-amino-l-propanol, 4-
amino-l-
butanol,5-amino-l-pentanol, 1-amino-2-propanol, 1-amino-2-butanol, 1-amino-2-
pentanol,
1-amino-3-pentanol, 1-amino-4-pentanol, 3-amino-2-methylpropan-l-ol, 1-amino-2-
methylpropan-2-ol, 3-aminopropane-1,2-diol, glucosamine, N-acetylglucosamine,
glycine,
arginine, lysine, proline, glutamine, histidine, sarcosine, serine, glutamic
acid, tryptophan, and
mixtures thereof, and the salts such as the potassium, sodium and ammonium
salts thereof and
mixtures thereof. Especially preferred compounds are glycine, sarcosine,
lysine, serine,
2 methoxyethylamine, glucosamine, glutamic acid, morpholine, piperdine,
ethylamine, 3 amino-
1-propanol and mixtures thereof.
CA 02646867 2008-12-16
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The radical scavengers according to the present invention preferably have a
molecular weight of
less than 500, preferably less than 300, more preferably less than 250 in
order to facilitate
penetration of the radical scavenger into the hair fibre. The compositions of
the present invention
preferably comprise from 0.1% to 10% by weight, preferably from 1% to 7% by
weight of
radical scavenger. The radical scavenger is also preferably selected such that
it is not an identical
species as the alkalizing agent. According to one embodiment of the present
invention the
radical scavenger may be formed insitu in the hair dyeing compositions prior
to application to the
hair fibres.
The compositions of the present invention may further comprise additional
ingredients which
include, but are not limited to, thickeners, solvents, enzymes, surfactants,
conditioning agents,
carriers, antioxidants or.reducing agents, stabilizers, chelants, perfumes,
hair swelling agents
and/or polymers. Some of these additional components are detailed hereafter.
Thickeners: The composition of the present invention may optionally further
comprise at least
about 0.0 1% by weight, especially from 0.05 to 25% by weight, of thickeners.
Thickeners are
preferably comprised in amount sufficient to provide the composition with a
viscosity of from
about 1 Pa.s to 40 Pa.s (1,000 to 40,000 cP) at 26 C in order to provide a
composition that can
be readily applied to the hair without dripping.
The at least one thickener is chosen, for example, from:
(i) associative thickeners;
(ii) crosslinked acrylic acid homopolymers;
(iii) crosslinked copolymers of (meth)acrylic acid and of (C1-C6)alkyl
acrylate;
(iv) nonionic homopolymers and copolymers containing ethylenically unsaturated
monomers
of ester and amide type;
(v) ammonium acrylate homopolymers and copolymers of ammonium acrylate and of
acrylamide;
(vi) polysaccharides;
(vii) C12-C30 fatty alcohols and
(viii) particulate or crystalline thickeners.
(i) As used herein, the expression "associative thickener" means an
amphiphilic thickener
comprising both hydrophilic units and hydrophobic units, for example, at least
one C8-C30 fatty
CA 02646867 2008-12-16
W245FQ/JC 20
chain and at least one hydrophilic unit. Representative associative thickeners
that may be used are
associative polymers chosen from:
(a) nonionic amphiphilic polymers comprising at least one fatty chain and at
least one hydrophilic
unit;
(b) anionic amphiphilic polymers comprising at least one hydrophilic unit and
at least one fatty-
chain unit;
(c) cationic amphiphilic polymers comprising at least one hydrophilic unit and
at least one fatty-
chain unit; and
(d) amphoteric amphiphilic polymers comprising at least one hydrophilic unit
and at least one
fatty-chain unit;
The nonionic amphiphilic polymers comprising at least one fatty chain and at
least one
hydrophilic unit may, for example, be chosen from:
(1) celluloses modified with groups comprising at least one fatty chain; for
example:
hydroxyethylcelluloses modified with groups comprising at least one fatty
chain chosen from
alkyl, arylalkyl and alkylaryl groups, and in which the alkyl groups are, for
example, C8-C22,
such as the product Natrosol Plus Grade 330 CS(C 16 alkyls) sold by the
company Aqualon, and
the product Bermocoll EHM 100 sold by the company Berol Nobel, and celluloses
modified with
polyalkylene glycol alkylphenyl ether groups, such as the product Amercell
Polymer HM-1500
(polyethylene glycol (15) nonylphenyl ether) sold by the company Amerchol;
(2) hydroxypropyl guars modified with groups comprising at least one fatty
chain, such as the
product Esaflor HM 22 (C22 alkyl chain) sold by the company Lamberti, and the
products
Miracare XC95-3 (C14 alkyl chain) and RE205-1 (C20 alkyl chain) sold by the
company Rhodia
Chimie;
(3) polyether urethanes comprising at least one fatty chain, such as C10-C30
alkyl or alkenyl
groups, for instance the products Elfacos T 210 and Elfacos T 212 sold by the
company Akzo or
the products Aculyn 44 and Aculyn 46 and Aculyn 48 sold by the company Rohm &
Haas;
(4) copolymers of vinylpyrrolidone and of fatty-chain hydrophobic monomers;
examples that
may be mentioned include: the products Antaron V216 and Ganex V216
(vinylpyrrolidone/hexadecene copolymer) sold by the company I.S.P., the
products Antaron
V220 and Ganex V220 (vinylpyrrolidone/eicosene copolymer) sold by the company
I.S.P. ;
(5) copolymers of C1-C6 alkyl acrylates or methacrylates and of amphiphilic
monomers
comprising at least one fatty chain, such as the oxyethylenated methyl
methacrylate/stearyl
acrylate copolymer sold by the company Goldschmidt under the name Anti1208;
CA 02646867 2008-12-16
W245FQ/JC 21
(6) copolymers of hydrophilic acrylates or methacrylates and of hydrophobic
monomers
comprising at least one fatty chain, such as polyethylene glycol
methacrylate/lauryl methacrylate
copolymer; and
(7) polymers as described in WO 96/40815 comprising at least one hydrophobbic
group and at
least one hydrophilic group, such as the following polymers according INCI
designation:
Polyether-1, PEG-180/Laureth-50/TMMG Copolymer and PEG-180/Octoxynol-40/TMMG
Copolymer (sold by the company United Catalysts under the name Pure-Thix 1442,
Pure-Thix
1450, Pure-Thix HH, Pure-Thix L and Pure-Thix M).
The anionic amphiphilic polymers comprising at least one hydrophilic unit and
at least one
fatty-chain unit, may, for example, be chosen from those comprising at least
one fatty-chain allyl
ether unit and at least one hydrophilic unit comprising an ethylenic
unsaturated anionic
monomeric unit, for example, a vinylcarboxylic acid unit and further, for
example, chosen from
units derived from acrylic acids, methacrylic acids and mixtures thereof,
wherein the fatty-chain
allyl ether unit corresponds to the monomer of formula below:
CHZ=C(Rl)CH2OBõR (I)
in which R1 is chosen from H and CH3, B is an ethyleneoxy radical, n is chosen
from zero and
integers ranging from 1 to 100, R is chosen from hydrocarbon-based radicals
chosen from alkyl,
arylalkyl, aryl, alkylaryl and cycloalkyl radicals, comprising from 10 to 30
carbon atoms, and,
further, for example, from 10 to 24 carbon atoms and even further, for
example, from 12 to 18
carbon atoms.
In one embodiment, a unit of formula (I) is, for example, a unit in which Rl
may be H, n may
be equal to 10 and R may be a stearyl (C 18) radical.
Anionic amphiphilic polymers of this type are described and prepared,
according to an emulsion
polymerization process, in patent EP-0 216 479 B2.
In one embodiment, anionic amphiphilic polymers are, for example, polymers
formed from 20%
to 60% by weight of acrylic acid and/or of methacrylic acid, from 5% to 60% by
weight of lower
alkyl (meth)acrylates, from 2% to 50% by weight of fatty-chain allyl ether of
formula (I), and
from 0% to 1% by weight of a crosslinking agent which is a well-known
copolymerizable
unsaturated polyethylenic monomer, for example, diallyl phthalate, allyl
(meth)acrylate,
divinylbenzene, (poly)ethylene glycol dimethacrylate and
methylenebisacrylamide.
Examples of such polymers are crosslinked terpolymers of methacrylic acid, of
ethyl acrylate and
of polyethylene glycol (10 EO) stearyl ether (Steareth- 10), such as those
sold by the company
Ciba under the names Salcare SC 80 and Salcare SC 90, which are aqueous 30%
emulsions of a
CA 02646867 2008-12-16
W245FQ/JC 22
crosslinked terpolymer of methacrylic acid, of ethyl acrylate and of steareth-
10 allyl ether
(40/50/10).
The anionic amphiphilic polymers may further be chosen, for example, from
those
comprising at least one hydrophilic unit of unsaturated olefinic carboxylic
acid type, and at least
one hydrophobic unit of the type such as a (C 10-C30) alkyl ester of an
unsaturated carboxylic
acid. The hydrophilic unit of unsaturated olefinic carboxylic acid type
corresponds to, for
example, the monomer of formula (II) below:
CH2=CR'-COOH (II)
in which R' is chosen from H, CH3, and C2H5, i.e. acrylic acid, methacrylic
acid and ethacrylic
acid units. And the hydrophobic unit of the type such as a (C 10-C30) alkyl
ester of an unsaturated
carboxylic acid corresponds to, for example, the monomer of formula (III)
below:
CH2=CR' -COORZ (III)
in which R' is chosen from H, CH3, and C2H5 (i.e. acrylate, methacrylate and
ethacrylate units)
and is, for example, chosen from, for example, H (acrylate units) and CH3
(methacrylate units),
R2 is chosen from C 10-C30 alkyl radicals, for example, C 12-C22 alkyl
radical.
Examples of (C10-C30)alkyl esters of unsaturated carboxylic acids include
lauryl acrylate, stearyl
acrylate, decyl acrylate, isodecyl acrylate, and dodecyl acrylate, and the
corresponding
methacrylates, lauryl methacrylate, stearyl methacrylate, decyl methacrylate,
isodecyl
methacrylate and dodecyl methacrylate.
Anionic amphiphilic polymers of this type are disclosed and prepared, for
example, according to
U.S. Pat. Nos. 3,915,921 and 4,509,949.
Representative anionic amphiphilic polymers that may be used may further be
chosen from
polymers formed from a mixture of monomers comprising:
(1) acrylic acid, an ester of formula (IV) below:
CH2=CR'-COOR2 (N)
in which R' is chosen from H and CH3, RZ is chosen from C10-C30 alkyl
radicals, such as alkyl
radicals comprising from 12 to 22 carbon atoms, and a crosslinking agent; such
as polymers
derived from 95% to 60% by weight of the acrylic acid (hydrophilic unit), 4%
to 40% by weight
of C10-C30 alkyl acrylate (hydrophobic unit), and 0% to 6% by weight of
crosslinking
polymerizable monomer, or polymers derived from 98% to 96% by weight of the
acrylic acid
(hydrophilic unit), 1% to 4% by weight of C 10-C30 alkyl acrylate (hydrophobic
unit) and 0.1 %
to 0.6% by weight of crosslinking polymerizable monomer; or
(2) acrylic acid and lauryl methacrylate, such as the polymers formed from 66%
by weight of
acrylic acid and 34% by weight of lauryl methacrylate.
CA 02646867 2008-12-16
W245FQ/JC 23
The crosslinking agent may be a monomer comprising a group (V)
I
CH2=C (V)
1
with at least one other polymerizable group whose unsaturated bonds are not
conjugated with
respect to one another. Mention may be made, for example, of polyallyl ethers
such as
polyallylsucrose and polyallyl pentaerythritol.
Among said polymers above mention may be made, for example, of the products
sold by the
company Noveon under the trade names Pemulen TR 1, Pemulen TR2, Carbopol 1382,
and
further, for example, Pemulen TRI, and the product sold by the company
S.E.P.C. under the
name Coatex SX.
Suitable anionic amphiphilic fatty-chain polymers, include for example the
methacrylic
acid/methyl acrylate/ethoxylated alkyl dimethyl-meta-
isopropenylbenzylisocyanate copolymer
sold under the name Viscophobe DB 1000 by the company Amerchol.
Further suitable anionic amphiphilic fatty-chain polymers, include polymers
having the INCI
designation Acrylates/Ceteth-20 Itaconate Copolymer (sold by the company
National Starch
under the name Structure 3001) and Acrylates/Steareth-20 Itaconate Copolymer
(sold by the
company National Starch under the name Structure 2001).
The cationic amphiphilic polymers used are, for example, chosen from
quaternized cellulose
derivatives and polyacrylates comprising amino side groups.
The quaternized cellulose derivatives are, for example, chosen from;
quaternized celluloses
modified with groups comprising at least one fatty chain, such as alkyl,
arylalkyl and alkylaryl
groups comprising at least 8 carbon atoms, and mixtures thereof, quaternized
hydroxyethylcelluloses modified with groups comprising at least one fatty
chain, such as alkyl,
arylalkyl and alkylaryl groups comprising at least 8 carbon atoms, and
mixtures thereof.
Quaternized and non-quaternized polyacrylates comprising amino side groups
having for
example, hydrophobic groups, such as Steareth 20 (polyoxy-ethylenated(20)
stearyl alcohol) and
(C10-C30)alkyl PEG-20 itaconate.
The alkyl radicals borne by the above quaternized celluloses and
hydroxyethylcelluloses, for
example, contain from 8 to 30 carbon atoms. The aryl radicals, for example,
are chosen from
phenyl, benzyl, naphthyl and anthryl groups.
Examples of quaternized alkylhydroxyethyl-celluloses comprising C8-C30 fatty
chains are the
products Quatrisoft LM 200, Quatrisoft LM-X 529-18-A, Quatrisoft LM-X 529-18B
(C12 alkyl)
and Quatrisoft LM-X 529-8 (C 18 alkyl) sold by the company Amerchol, and the
products
Crodacel QM, Crodacel QL (C12 alkyl), Crodacel QS (C18 alkyl) sold by the
company Croda,
CA 02646867 2008-12-16
W245FQ/JC 24
Softcat Polymer SL-5, Softcat Polymer SL-30, Softcat Polymer SL-60 and Softcat
SL-100 sold
by the company Amerchol.
Examples of polyacrylates comprising amino side chains is Structure Plus from
the company
National Starch.
Among amphoteric amphiphilic polymers comprising at least one hydrophilic unit
and at least
one fatty-chain unit, mention may be made, for example, of
methacrylamidopropyltrimethylammonium chloride/acrylic acid/C10-C30 alkyl
methacrylate
copolymers, wherein the alkyl radical is, for example, a stearyl radical.
(ii) Among the crosslinked acrylic acid homopolymers that may be mentioned are
those
crosslinked with an allylic alcohol ether of the sugar series, such as the
products sold under the
names Carbopol 980, 981, 954, 2984 and 5984 by the company Noveon or the
products sold
under the names Synthalen M, Synthalen L and Synthalen K by the company 3V
Sigma.
(iii) Crosslinked copolymers of (meth)acrylic acid and of C 1-C6 alkyl
acrylate may be chosen
from crosslinked copolymers of methacrylic acid and of ethyl acrylate as an
aqueous dispersion
comprising 38% active material sold, for example, under the name Viscoatex
538C by the
company Coatex, and crosslinked copolymers of acrylic acid and of ethyl
acrylate as an aqueous
dispersion comprising 28% active material sold under the name Aculyn 33 by the
company Rohm
& Haas. Crosslinked copolymers of methacrylic acid and of ethyl acrylate
include an aqueous
dispersion comprising 30% active material manufactured and sold under the name
Carbopol
Aqua SF-1 by the company Noveon.
(iv) Among the nonionic homopolymers or copolymers comprising ethylenically
unsaturated
monomers of ester and/or amide type, mention may be made of the products sold
under the
names: Cyanamer P250 by the company Cytec (polyacrylamide); PMMA MBX-8C by the
company US Cosmetics (methyl methacrylate/ethylene glycol dimethacrylate
copolymer);
Acryloid B66 by the company Rohm & Haas (butyl methacrylate/methyl
methacrylate
copolymer); BPA 500 by the company Kobo (polymethyl methacrylate).
(v) Ammonium acrylate homopolymers that may be mentioned include the product
sold under the
name Microsap PAS 5193 by the company Hoechst.
Copolymers of ammonium acrylate and of acrylamide include the product sold
under the name
Bozepol C Nouveau or the product PAS 5193 sold by the company Hoechst (which
are described
and prepared in documents FR-2 416 723, U.S. Pat. Nos. 2,798,053 and
2,923,692).
(vi) The polysaccharides are, for example, chosen from glucans, modified and
unmodified
starches (such as those derived, for example, from cereals, for instance
wheat, corn or rice, from
vegetables, for instance yellow pea, and tubers, for instance potato or
cassaya), amylose,
CA 02646867 2008-12-16
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amylopectin, glycogen, dextrans, celluloses and derivatives thereof
(methylcelluloses,
hydroxyalkylcelluloses, ethyl hydroxyethylcellu loses, and
carboxymethylcelluloses), mannans,
xylans, lignins, arabans, galactans, galacturonans, chitin, chitosans,
glucuronoxylans,
arabinoxylans, xyloglucans, glucomannans, pectic acids and pectins, alginic
acid and alginates,
arabinogalactans, carrageenans, agars, glycosaminoglucans, succinoglucans, gum
arabics, gum
tragacanths, ghatti gums, karaya gums, carob gums, galactomannans, such as
guar gums, and
nonionic derivatives thereof (hydroxypropyl guar) and xanthan gums, and
mixtures thereof.
For example, suitable polysaccharides are described in "Encyclopedia of
Chemical Technology",
Kirk-Othmer, Third Edition, 1982, volume 3, pp. 896-900, and volume 15, pp.
439-458, in
"Polymers in Nature" by E. A. MacGregor and C. T. Greenwood, published by John
Wiley &
Sons, Chapter 6, pp. 240-328,1980, and in "Industrial Gums-Polysaccharides and
their
Derivatives", edited by Roy L. Whistler, Second Edition, published by Academic
Press Inc., the
content of these three publications being entirely incorporated by reference.
For example, starches, guar gums and celluloses and derivatives thereof may be
used. Suitable
starches include for example, of macromolecules in the form of polymers
comprising elemental
moieties that are anhydroglucose units. The number of these moieties and their
assembly make it
possible to distinguish between amylose (linear polymer) and amylopectin
(branched polymer).
The relative proportions of amylose and of amylopectin, and also their degree
of polymerization,
may vary as a function of the botanical origin of the starches. The botanical
origin of the starch
molecules used may be cereals or tubers. Thus, the starches may be, for
example, chosen from
corn starch, rice starch, cassaya starch, tapioca starch, barley starch,
potato starch, wheat starch,
sorghum starch and pea starch. Starches are generally in the form of a white
powder, which is
insoluble in cold water and which has an elementary particle size ranging from
3 to 100 microns.
The starches may optionally be C1-C6 hydroxyalkylated or C1-C6 acylated (such
as acetylated).
The starches may also have undergone heat treatments. Distarch phosphates or
of compounds rich
in distarch phosphate, for instance the products sold under the references
Prejel VA-70-T AGGL
(gelatinized hydroxypropylated cassaya distarch phosphate) or Prejel TKl
(gelatinized cassaya
distarch phosphate) or Prejel 200 (gelatinized acetylated cassaya distarch
phosphate) by the
company Avebe, or Structure ZEA from National Starch (hydroxypropylated corn
distarch
phosphate), Structure XL from National Starch (hydroxypropylated starch
phosphate) may also
be used.
The guar gums may be modified or unmodified. The unmodified guar gums are, for
example, the
products sold under the name Vidogum GH 175 by the company Unipectine and
under the names
Meyro-Guar 50 and Jaguar C by the company Meyhall. The modified nonionic guar
gums are, for
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example, modified with C1-C6 hydroxyalkyl groups. Among hydroxyalkyl groups,
mention may
be made, for example, of hydroxymethyl, hydroxyethyl, hydroxypropyl and
hydroxybutyl groups.
These guar gums are well known in the state of the art and may be prepared,
for example, by
reacting corresponding alkene oxides, such aspropylene oxides, with guar gum
so as to obtain a
guar gum modified with hydroxypropyl groups. The degree of hydroxyalkylation,
which
corresponds to the number of alkylene oxide molecules consumed by the number
of free hydroxyl
functions present on the guar gum, may, for example, range from 0.4 to 1.2.
Such nonionic guar gums optionally modified with hydroxyalkyl groups are sold,
for example,
under the trade names Jaguar HP8, Jaguar HP60 and Jaguar HP 120, Jaguar DC 293
and Jaguar
HP 105 by the company Rhodia Chimie (Meyhall) or under the name Galactasol
4H4FD2 by the
company Aqualon.
Suitable celluloses include for example, hydroxyethylcellulose and
hydroxypropylcelluloses,
such as the products sold under the names Klucel EF, Klucel H, Klucel LHF,
Klucel MF and
Klucel G by the company Aqualon.
(vii) The C12 - C30 fatty alcohols are, for example, chosen from myristyl
alcohol, cetyl alcohol,
stearyl alcohol, behenyl alcohol or mixture thereof. When fatty alcohols are
used as thickeners, at
least one additional surfactant with HLB value above about 6 is commonly
included to form bi-
layers with fatty alcohols. The most useful bi-layer structures include gel
network phase where
parallel bi-layers of fatty alcohols are swollen by water forming semi-solid
creams, and vesicle
dispersions where fatty alcohols bi-layers are curved into approximately
spherical uni-lamellar or
multi-lamellar aggregates.
(viii) The particulate and crystalline thickeners are for example, clays,
fumed silica,
microcrystalline cellulose, trihydroxystearin (ThixcinR), ethyleneglycol mono-
and di-stearate or
mixture thereof. The particulate or crystalline thickeners work via mechanisms
well known in the
art, for example particle aggregation, "house of card" particle arrangement or
crystalline fiber
formation.
In addition the dye compositions can be thickend by adding prior to use
anionic acrylic polymers
as described in WO 0 1/97772, which are sold by Arch Personal Care Products,
South Plainfield,
USA under the tradename ViscUp EZ.
Conditioning agent: The compositions of the present invention may comprise or
are used in
combination with a composition comprising a conditioning agent in an amount of
at least about
0.0 1% by weight, especially from 0.1 % to 10% by weight. Conditioning agents
suitable for use
CA 02646867 2008-12-16
W245FQ/JC 27
herein are selected from silicone materials, amino silicones, fatty alcohols,
polymeric resins,
polyol carboxylic acid esters, cationic polymers, cationic surfactants,
insoluble oils and oil
derived materials and mixtures thereof. Additional materials include mineral
oils and other oils
such as glycerin and sorbitol.
The conditioning agent will generally be used at levels of from about 0.05% to
about 20% by
weight of the composition, preferably of from about 0.1 % to about 15% by
weight, more
preferably of from about 0.2% to about 10% by weight, even more preferably of
from about 0.2%
to about 2% by weight.
Particularly useful conditioning materials are cationic polymers. Conditioners
of cationic polymer
type may be chosen from those already know by those skilled in the art as
improving at least one
cosmetic properties of keratin fibres treated with a cosmetic composition.
Cationic polymers may
be chosen from those comprising units of at least one amine group chosen from
primary,
secondary, tertiary and quaternary amine groups that may either form part of
the main polymer
chain, or be borne by a side substituant that is directly attached to the main
polymer chain. Such
cationic polymers generally have a number average molecular mass ranging from
500 to
5,000,000, or more preferably from 1000 to 3,000,000. Polymers of the
polyamine, polyamino
amide and polyquaternary ammonium type that may be used include but are not
limited to:
(1) homopolymers and copolymers derived from acrylic or methacrylic esters or
amides.
Copolymers of these polymers may also comprise at least one unit derived from
comonomers
which may be chosen from the family of acrylamides, methacrylamides, diacetone
acylamides,
acrylamides and methacrylicamides substituted on the nitrogen with at least
one group chosen
from lower (C1-C4) alkyls, acrylic and methacrylic acids and esters thereof,
vinlylactams such as
vinlypyrrolidone and vinylcaprolactam, and vinyl esters. Examples of such
polymers include:
Copolymers of acrylamide and of methacryloyloxyethyltrimethylammonium
methosulfate,
examples of which include polymers known via the INCI nomenclature as
Polquaternium-5,
such as the products sold under the names Reten 210, Reten 220, Reten 230,
Reten 240, Reten
1104, Reten 1105, Reten 1006 by the company Hercules and Merquat 5, Merquat 5
SF by the
company Nalco.
Copolymers of vinylpyrrolidone and dimethylaminopropyl methacrylamide,
examples of which
include polymers known via the INCI nomenclature as Polyquaternium-28, such as
the products
sold under the name Gafquat HS- 100 by the company International Speciality
Products (ISP).
Copolymers of vinyl pyrrolidone and dialkyaminoalkyl acrylates or
methactylates, examples of
which include polymers known via the INCI nomenclature as Polquaternium-11,
such as the
products sold under the name Gafquat 440, Gafquat 734, Gafquat 755, Gafquat
755N by the
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company International Speciality Products (ISP), and Luviquat PQ11 PM by the
company BASF
and Polyquat-11 SL by the company Sino Lion.
Copolymers vinylpyrrolidone, dimethylaminopropyl methacrylamide and
methacryloylaminopropyl lauryldimonium chloride, examples of which include
polymers known
via the INCI nomenclature as polyquatemium-55, such as the products sold under
the name
Styleze W-20 by the company International Speciality Products (ISP).
Copolymers of acrylic acid, acrylamide and methacrylamidopropyltrimonium
chloride, examples
of which include polymers known via the INCI nomenclature as Polyquaternium-
53, such as the
products sold under the name Merquat 2003 by the company Nalco.
Copolymers of dimethyaminopropylacrylate (DMAPA), acrylic acid and
acrylonitrogens and
diethyl sulfate, examples of which include polymers known via the INCI
nomenclature as
Polyquaternium-31, such as the products sold under the name Hypan QT 100 by
the company
Lipo.
Copolymers of acrylamide, acrylamidopropyltrimonium chloride, 2-
amidopropylacrylamide
sulfonate, and dimethyaminopropylacrylate (DMAPA), examples of which include
polymers
known via the INCI nomenclature as polyquaternium-43, such as the products
sold under the
name Bozequat 4000 by the company Clairant.
Copolymers of acrylic acid, methylacrylate and methacrylamidopropyltrimonium
chloride,
examples of which include polymers known via the INCI nomenclature as
Polyquaternium-47,
such as the products sold under the name Merquat 2001 and Merquat 2001N sold
commercially
by Nalco.
Copolymes of methacryloyl ethyl betaine, 2-hydroxyethyl methacrylate and
methacryloyl ethyl
trimethyl ammonium chloride, examples of which include polymers known via the
INCI
nomenclature as Polyquaternium-48, such as the products sold under the name
Plascize L-450 by
the company Goo Chemcial.
Copolymers of acrylic acid diallyl dimethyl ammonium chloride and acrylamide,
examples of
which include polymers known via the INCI nomenclature as polyquaternium 39,
such as the
products sold under the name Merquat 3330 and Merquat 3331 by the company
Nalco.
Further examples include copolymers of methacrylamide methacrylamido-
propyltrimonium and
methacryloylethyltrimethyl ammonium chloride and their derivatives, either
homo or
copolymerised with other monomers, examples of which include polymers known
via the INCI
nomenclature as: Polyquaternium-8, Polyquatemium-9, Polyquaternium-12,
Polyquaternium-13
Polyquaternium-14, Polyquaternium-15, such as the products sold under the name
Rohagit KF
720 F by the company Rohm, Polyquatemium-30, such as the products sold under
the name
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Mexomere PX by the company Chimex, Polyquaternium-33, Polyquatemium-35,
Polyquaternium-36, such as the products sold under the name Plex 3074 L by the
company
Rhon, Polyquaternium 45, such as the products sold under the name Plex 3073L
by the company
Rohn, Polyquaternium 49, such as the products sold under the name Plascize L-
440 by the
company Goo Chemicals, Polyquaternium 50 such as the products sold under the
name Plascize
L-441 by the company Goo Chemicals, Polyquatemium-52.
(2) Cationic polysaccharides, such as cationic celluloses and cationic
galactomannan gums.
Among the cationic polysaccharides that maybe mentioned, for example, are
cellulose ether
derivatives comprising quaternary ammonium groups and cationic cellulose
copolymers or
cellulose derivatives grafted with a water-soluble quaternary ammonium monomer
and cationic
galactomannan gums. Examples include but are not limited to:
Copolymers of hydroxyethylcelluloses and diallyldimethyl ammonium chlorides,
examples of
which include polymers known via the INCI nomenclature as Polyquaternium-4,
such as the
products sold under the name Celquat L 200 and Celquat H 100 by the company
National Starch.
Copolymers of hydroxyethylcelluloses and a trimethyl ammonium substituted
epoxide, examples
of which include polymers known via the INCI nomenclature as Polyquaternium-
10, such as the
products sold under the name AEC Polyquaternium-10 by the company A&E Connock,
Catinal
C-100 Catinal HC-35 Catinal HC-100 Catinal HC-200 Catinal LC-100 Catinal LC-
200 by the
company Toho, Celquat SC-240C Celquat SC-230M, by the company National Starch,
Dekaquat 400, Dekaquat 3000 by the company Dekker, Leogard GP by the company
Akzo
Nobel, RITA Polyquta 400 RITA, Polyquta 3000 by the company RITA, UCARE
Polymer JR-
125 UCARE Polymer JR-400 UCARE Polymer JR-30M UCARE Polymer LK UCARE Polymer
LR 400 UCARE Polymer LR 30M by the company Amerchol.
Copolymers of hydroxyethylcelluloses and lauryl dimethyl ammonium substituted
epoxides,
examples of which include polymers known via the INCI nomenclature as
Polyquaternium-24,
such as the products sold under the name Quatrisoft polymer LM-200 by the
company
Amerchol.
Derivatives of Hydroxypropyl Guar, examples of which include polymers known
via the INCI
nomenclature as Guar Hydroxypropyltrimonium Chloride, such as the products
sold under the
name Catinal CG-100, Catinal CG-200 by the company Toho, Cosmedia Guar C-261N,
Cosmedia Guar C-261N, Cosmedia Guar C-261N by the company Cognis, DiaGum P
5070 by
the company Freedom Chemical Diamalt, N-Hance Cationic Guar by the company
Hercules/Aqualon, Hi-Care 1000, Jaguar C-17, Jaguar C-2000, Jaguar C-13S,
Jaguar C-14S,
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Jaguar Excel by the company Rhodia, Kiprogum CW, Kiprogum NGK by the company
Nippon
Starch.
Hydroxypropyl derivatives of Guar Hydroxypropyltrimonium Chloride, examples of
which
include polymers known via the INCI nomenclature as Hydroxypropyl Guar
Hydroxypropyltrimonium Chloride, such as the products sold under the name
Jagaur C- 162 by
the company Rhodia.
(3) Polyamino amide derivatives resulting from the condensation of
polyalkylene polyamines
with polycarboxylic acids followed by alkylation with difunctional agents.
Among the
derivative, mention may be made for example to adipic acid /
dimethylaminohydroxypropyl /
diethylenetriamine.
(4) Polymers obtained by reaction of a polyalkylene polyamine comprising two
primary amines
groups and at last one secondary amine group with a decarboxylic acid chosen
from diglycolic
acids and saturated aliphatic dicarboxylic acids comprising from 3 to 8 carbon
atoms. Non-
limiting examples of such derivatives include the adipic acid / epxoypropyl /
diethylenetriamine.
(5) Cyclopolymers of dialkdiallylamine or of dialkyldiallyammonium, among
which polymers
mention may be made of:
Dimethyldiallyammonium chloride polymers, examples of which include polymers
known via
the INCI nomenclature as Polyquaternium-6, such as the products sold under the
name Merquat
100 by the company Nalco, Mirapol 100 by the company Rhodia, Rheocare CC6 by
the
company Cosmetic Rheologies, AEC polyquaternium-6 by the company A&E Connock,
Agequat 400 by the company CPS, Conditioner P6 by the company 3 V Inc.,
Flocare C 106 by the
company SNF, Genamin PDAC by the company Clariant, Mackernium 006 by the
company
McIntyre.
Copolymers of acrylamides and dimethyldiallylammonium chlorides monomers,
examples of
25, which include polymers known via the INCI nomenclature as Polyquatemium-7,
such as the
products sold under the name AEC Polyquatemium-7 by the company A&E Connock,
Agequat-
5008, Agequat C-505 by the company CPS, Conditioner P7 by the company 3V Inc.
Flocare C
107 by the company SNF Mackernium 007, Mackernium 007S by the company
McIntyre, ME
Polymer 09W by the company Toho, Merquat 550, Merquat 2200, Merquat S by the
company
Nalco, Mirapo1550 by the company Rhodia, Rheocare CC7, Rheocare CCP7 by the
company
Cosmetic Rheologies, Salcare HSP-7, Salcare SC 10, Salcare Super 7 by the
company Ciba.
Copolymers of dimethyldiallylammoniumchlorides and acrylic acids, examples of
which include
polymers known via the INCI nomenclature as polyquaternary-22, such as the
products sold
under the name Merquat 280 and Merquat 295 by the company Nalco.
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(6) Quaternary diammonium polymers comprising repeating units of formula
[-N+(R')(R2) -AN
' ' (R3)(R4)-B'-] [2X"], in which R', R2, R3 and R4, which may be identical or
different, are chosen from aliphatic, alicyclic and arylaliphatic radicals
comprising from 1 to 20
carbon atoms and from lower hydroxyalkylaliphatic radicals, or R', R2, R3 and
R4, together or
separately, constitute, with the nitrogen atoms to which they are attached,
heterocycles optionally
comprising a second heteroatom other then nitrogen, or R', R2, R3 and R4, are
choen from liner
or branched C1-C6 alkyl radicals substituted with at least one group chosen
from nitrile, ester,
acyl and amide groups and groups of -CO-O-R5-D and -CO-NH-R5-D wherein R5 is
chosen
from alkylene groups and D is chosen from quaternary ammonium groups. A' and
B', which
may be identical or different, are chosen from linear and branched, saturated
or unsaturated
polymethylene groups comprising 2 to 20 carbon atoms. The polymethylene groups
may
comprise, linked to or intercalated in the main ring, at least one entity
chosen from aromatic
rings, oxygen and sulphur atoms and sulphoxide, sulphone, disulphide, amino,
alkylamino,
hydroxyl, quaternary, ammonium, ureido, amide and ester groups, and X" is an
anion derived
from inorganic and organic acids. D is chosen from a glycol residue, a bis-
secondary diamine
residue, a bis-primary diamine residue or a ureylene group. An examples of
which include
polymers known via the INCI nomenclature as Hexadimethrine chloride, where R',
R2, R3 and
R4 are each methyl radicals, A' is (CH2)3 and B' is (CH2)6 and X = Cl. Further
examples of
which include polymers known via the INCI nomenclature as polyquatemium-34
where R'and
R2 are ethyl radicals and R3 and R4 are methyl radicals and A' is (CH2)3 and
B' is (CH2)3 and X
= Br, such as the products sold under the name Mexomere PAX by the company
Chimax.
(7) Polyquaternary ammonium polymers comprising repeating units of formula
[-N+(R6)(R')-(CH2)r-NH-CO-(CH2)q-(CO)t-NH-(CH2)s-N+(Rg)(R9)-A-] [2X-], in
which R6,
R', R8 and R9 which may be identical or different, are chosen from a hydrogen
atom and a
methyl, ethyl, propyl, hydroxyethyl, hydroxypropyl, and -CH2CH2(OCH2CH2)pOH
radicals,
wherein p is equal to 0 or an integer ranging from 1 to 6, wherein R6, R7, R8
and R9 do not all
simultaneously represent a hydrogen atom. R and s which maybe identical or
different are each
an integer ranging from 1 to 6, q is equal to 0 or an integer ranging from 1
to 34 and X- is an
anion such as a halide. T is an integer chosen to be equal to 0 or 1. A is
chosen from divalent
radicals such as -CH2-CH2-O-CH2-CH2-. Examples of which include
Polymers known via the INCI nomenclature as polyquatemium-2, where r=s=3,
q=0,t=0, R6, R',
R8 and R9 are methyl groups, and A is -CH2-CH2-O-CH2-CH2, such as the products
sold
under the name Ethpol PQ-2 from Ethox and Mirapol A- 15 by the company Rhodia.
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Polymers known via the INCI nomenclature as polyquaternium-17 where 1=s=3,
q=4, t=1, R6,
R', R8 and R9 are methyl groups, and A is -CH2-CH2-O-CH2-CH2.
Polymers known via the INCI nomenclature as Polyquaternium 18, where r=s=3,
q=7, t=1, R6,
R', R8 and R9 are methyl groups, and A is -CH2-CH2-O-CH2-CH2
Polymers known via the INCI nomenclature as the block copolymer formed by the
reaction of
Polyquaternium-2 with Polyquaternium-17, known as Polyquaternium 27, such as
the products
sold under the name Mirapol 175 by the company Rhodia.
(8) Copolymers of vinylpyrrolidones and of vinylimidazoles and optionally
vinylcaprolactums,
examples of which include polymers known via the INCI nomenclature as
Polyquaternary-16
formed from methylvinylimidazolium chlorides and vinylpyrrolidones, such as
the products sold
under the name Luviquat FC370, Luviquat FC550, Luviquat FC905, Luviquat HM-552
by the
company BASF. Or copolymers of vinylcaprolactams and vinylpyrrolidones with
methylvinylimidazolium methosulfates, examples of which include polymers known
via the
INCI nomenclature as Polyquaternium-46, such as the products sold under the
name Luviquat
Hold by the company BASF. Or copolymers of vinylpyrrolidones and quaternized
imidazolines,
examples of which include polymers known via the INCI nomenclature
poylquaterary 44, such as
the products sold under the name Luviquat Care by the company BASF
(9) Polyamines such as the product Polyquart H sold by Cognis under the
reference name
polyethylene glycol (15) tallow polyamine in the CTFA dictionary.
(10) Cross linked methacryloyloxy(C1-C4)alkyltri(Cl-C4)alkylammonium salt
polymers such as
the polymers obtained by homopolymerisation of dimethylaminoethyl
methacrylates quaternized
with methyl chloride, or by copolymerisation of acrylamides with
dimethylaminoethyl
methacrylates quatemized with methyl chloride, the homo or copolymerisation
being followed by
crosslinking with a compound comprising olefinic unsaturation, such as
methylenebisacrylamides, examples of which include polymers known via the INCI
nomenclature as Polyquaternium-37, such as the products sold under the name
Synthalen, CN
Synthalen CR, Synthalen CU, sold by 3V sigma, or as a dispersion in another
media such as the
products sold under the name Salcare SC95 and Salcare SC96 by the company Ciba
or Rheocare
CTH(E) by the company Cosmetic Rheologies. Or in another example of which
include
polymers known via the INCI nomenclature as Polyquaternium-32, or when sold as
a dispersion
in mineral oil such as the products sold under the name Salcare SC92 by the
company Ciba.
(11) Further examples of cationic polymers include polymers known via the INCI
nomenclature
as Polyquaternium 51, such as the products sold under the name Lipidure-PMB by
the company
NOF, via the INCI nomenclature as Polyquatemium 54, such as the products sold
under the name
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Qualty-Hy by the company Mitsui, and via the INCI nomenclature as
Polyquatemium 56 such as
the products sold under the name Hairrol UC-4 by the company Sanyo chemicals.
(12) silicone polymers comprising cationic groups and/or groups which may be
ionised into
cationic groups. For example: cationic silicones of the general formula
(R10-N+(CH3)2)-R"-(Si(CH3)2-0)x-R"-(N+(CH3)2)-R'0), where Rl0 is an alkyl
derived from
coconut oil, and R" is (CH2CHOCH2O(CH2)3 and x is a number between 20 and
2000,
examples of which include polymers known by the INCI nomenclature as Quatemium
80, such
as the products sold under the name as Abil Quat 3272 and Abil Quat 3474 sold
commercially by
Goldschmidt.
Silicones containing groups which may be ionised into cationic groups, for
example
aminosilicones containing at least 10 repeating siloxane -(Si(CH3)2-O) units
within the polymer
chain, with either terminal, graft or a mixture of terminal and graft
aminofunctional groups.
Example functional groups are not limited to aminoethylaminopropyl,
aminoethylaminoisobutly,
aminopropyl. In the case of graft polymers, the terminal siloxane units may
either be (CH3)3Si-
0 or RIZ(CH3)2Si-0, where R12 may be either OH or OR13, where R13 is a C1-C8
alky group, or
a mixture of both functional terminal groups. These silicones are also
available as preformed
emulsions. Polymer with terminal siloxane units of (CH3)3Si-O examples of
which include
polymers known by the 1NCI nomenclature as trimethylsilylamodimethicone, such
as the
products sold under the name as DC-2-8566, DC 7224 and DC-2-8220 sold
commercially by
Dow Corning and SF1708 and SM 2125 sold commercially by GE Silicones and
Wacker Belsil
ADM 653 sold commercially by Wacker silicones. Further examples include
polymers with
terminal siloxane units of (R12O)(CH3)2Si-O where R12 may be either OH or
OR'3, where R13 is
a Cl-C8 alky group, or a mixture of both functional terminal groups, known by
the INCI
nomenclature as amodimethicone, such as the products sold under the name as
Wacker Belsil
ADM 1100, Wacker Belsil ADM 1600, Wacker Belsil ADM 652, Wacker Belsil ADM
6057E,
Wacker Belsil ADM 8020 sold commercial by Wacker Silicones, DC929, DC939 and
DC949
sold commercially by Dow Corning and SM2059 sold commercially by GE silicones.
Silicones containing groups which may be ionised into cationic groups - for
example silicones
containing at least 10 repeating siloxane -(Si(CH3)2-0) units within the
polymer chain, with
either terminal, graft or a mixture of terminal and graft aminofunctional
groups, together with
additional functional groups. Additional functional groups may include
polyoxyalkylene, the
reaction product of amines and carbinols, alky chains. For example products
know by the INCI
nomenclature as methoxy PEG/PPG-7/3 Aminopropyl Dimethicone, such as the
product sold
under the name of Abil Soft AF 100 sold commercially by Degussa. For example
products know
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W245FQ/JC 34
by the INCI nomenclature as Bis (C 13-15 Alkoxy) PG Amodimethicone, such as
the product
sold under the name of DC 8500 sold commercially by Dow Coming.
Surfactants: The compositions according to the present invention may further
comprise one or
more surfactants. Surfactants suitable for use herein generally have a
lipophilic chain length of
from about 8 to about 30 carbon atoms and may be selected from anionic,
nonionic, amphoteric
and cationic surfactants and mixtures thereof. The total level of surfactant
is from about 0.5% to
about 60% by weight, preferably from about 2% to about 30% by weight, more
preferably from
about 8% to about 25% by weight and especially from about 10% to about 20% by
weight.
The compositions of the invention preferably comprise a mixture of anionic and
amphoteric
surfactants with one or more nonionic surfactants. Anionic components, where
may be present in
the range of from about 0.1% to about 20% by weight, preferably from about
0.1% to about 15%
by weight, and more preferably from about 5% to about 15% by weight of the
composition;
amphoteric or nonionic components, may independently be present is in the
range from about
0.1 % to about 15% by weight, preferably from about 0.5% to about 10% by
weight, more
preferably from about 1% to about 8% by weight.
As examples of anionic surfactants, which may be used, alone or as mixtures,
mention may be
made, for example, of salts (such as alkaline salts, for example, sodium
salts, ammonium salts,
amine salts, amino alcohol salts and magnesium salts) of the following
compounds: alkyl
sulphates, alkyl ether sulphates, alkylamido ether sulphates,
alkylarylpolyether sulphates,
monoglyceride sulphates; alkyl sulphonates, alkyl phosphates, alkylamide
sulphonates, alkylaryl
sulphonates, a-olefin sulphonates, paraffin sulphonates; alkyl
sulphosuccinates, alkyl ether
sulphosuccinates, alkylamide sulphosuccinates; alkyl sulphosuccinamates; alkyl
sulphoacetates;
alkyl ether phosphates; acyl sarcosinates; acyl isethionates and N-
acyltaurates. The alkyl or acyl
radical of all of these various compounds, for example, comprises from 8 to 24
carbon atoms,
and the aryl radical, for example, is chosen from phenyl and benzyl groups.
Among the anionic
surfactants, which may also be used, mention may also be made of fatty acid
salts such as the
salts of oleic, ricinoleic, palmitic and stearic acids, coconut oil acid or
hydrogenated coconut oil
acid; acyl lactylates in which the acyl radical comprises from 8 to 20 carbon
atoms. Weakly
anionic surfactants may also be used, such as alkyl-D-galactosiduronic acids
and their salts, as
well as polyoxyalkylenated (C6-C24) alkyl ether carboxylic acids,
polyoxyalkylenated (C6-C24)
alkylaryl ether carboxylic acids, polyoxyalkylenated (C6-C24) alkylamido ether
carboxylic acids
and their salts, for example, those comprising from 2 to 50 ethylene oxide
groups, and mixtures
thereof. Anionic derivatives of polysaccharides, for example carboxyalkyl
ether of alkyl
CA 02646867 2008-12-16
W245FQ/JC 35
polyglucosides, may be also used.
The nonionic surfactants are compounds that are well known (see, for example,
in this respect
"Handbook of Surfactants" by M. R. Porter, published by Blackie & Son (Glasgow
and London),
1991, pp. 116-178). They may be chosen, for example, from polyethoxylated,
polypropoxylated
and polyglycerolated fatty acids, alkyl phenols, a-diols and alcohols
comprising a fatty chain
comprising, for example, from 8 to 18 carbon atoms, it being possible for the
number of ethylene
oxide or propylene oxide groups to range, for example, from 2 to 200 and for
the number of
glycerol groups to range, for example, from 2 to 30. Mention may also be made
of copolymers of
ethylene oxide and of propylene oxide, condensates of ethylene oxide and of
propylene oxide
with fatty alcohols; polyethoxylated fatty amides preferably having from 2 to
30 mol of ethylene
oxide and their momoethanolamine and diethanolamine derivatives,
polyglycerolated fatty
amides, for example, comprising on average from 1 to 5, and such as from 1.5
to 4, glycerol
groups; polyethoxylated fatty amines such as those containing from 2 to 30 mol
of ethylene
oxide; oxyethylenated fatty acid esters of sorbitan having from 2 to 30 mol of
ethylene oxide;
fatty acid esters of sucrose, fatty acid esters of polyethylene glycol,
alkylpolyglycosides,
N-alkylglucamine derivatives, amine oxides such as (Clo-C]4)alkylamine oxides
or
N-acylaminopropylmorpholine oxides.
The amphoteric surfactants may be chosen, for example, from aliphatic
secondary and
tertiary amine derivatives in which the aliphatic radical is chosen from
linear and branched
chains comprising from 8 to 22 carbon atoms and comprising at least one water-
soluble anionic
group (for example carboxylate, sulphonate, sulphate, phosphate or
phosphonate); mention may
also be made of (C8-C20)alkylbetaines, sulphobetaines, (Cg-CZo)alkylamido(CI-
C6)alkylbetaines
or (C8-C2o)alkylamido(C1-C6)alkylsulphobetaines.
Among the amine derivatives, mention may be made of the products sold under
the name
Miranol, as described, for example, in U.S. Pat. Nos. 2,528,378 and 2,781,354
and having the
structures of: RZ-CON HCHZCH2-N+(R3)(R4)(CH2COO-) (VI)
in which: R2 is chosen from alkyl radicals derived from an acid R2-COOH
present in hydrolysed
coconut oil, and heptyl, nonyl and undecyl radicals, R3 is a(3-hydroxyethyl
group and R4 is a
carboxymethyl group; and of R5-CONHCHZCHZ-N(B)(C) (VII)
wherein B represents -CH2CH2OX', C represents -(CHZ)Z Y', with z=1 or 2, X' is
chosen
from the -CH2CH2-COOH group and a hydrogen atom, Y' is chosen from -COOH and
-CH2-CHOH-SO3H radicals, R5 is chosen from alkyl radicals of an acid RS-COOH
present
in coconut oil or in hydrolysed linseed oil, alkyl radicals, such as C7, C9,
CII and C13 alkyl
radicals, a C 17 alkyl radical and its iso form, and unsaturated C 17 radical.
These compounds are
CA 02646867 2008-12-16
W245FQ/JC 36
classified in the CTFA dictionary, 5th edition, 1993, under the names disodium
cocoamphodiacetate, disodium lauroamphodiacetate, disodium
caprylamphodiacetate, disodium
capryloamphodiacetate, disodium cocoamphodipropionate, disodium
lauroamphodipropionate,
disodium caprylamphodipropionate, disodium capryloamphodipropionate,
lauroamphodipropionic acid, and cocoamphodipropionic acid. Salts of diethyl
aminopropyl
cocoaspartamid may be also used.
The cationic surfactants may be chosen from: A) the quaternary ammonium salts
of general
formula (VIII): [NR'R2R3R4]+ X" (VIII)
wherein X- is an anion chosen from halides (chloride, bromide and iodide), (C2-
C6)alkyl
sulphates, such as methyl sulphate, phosphates, alkyl and alkylaryl
sulphonates, and anions
derived from organic acids, such as acetate and lactate, and
(i) the radicals R' to R3, which may be identical or different, are chosen
from linear and branched
aliphatic radicals comprising from 1 to 4 carbon atoms, and aromatic radicals
such as aryl and
alkylaryl. The aliphatic radicals may comprise at least one hetero atom such
as oxygen, nitrogen,
sulphur and halogens. The aliphatic radicals are chosen, for example, from
alkyl, alkoxy and
alkylamide radicals, R4 is chosen from linear and branched alkyl radicals
comprising from 16 to
30 carbon atoms.
The cationic surfactant is, for example, a behenyltrimethylammonium salt (for
example a
chloride or bromide).
(ii) the radicals Rl and R2, which may be identical or different, are chosen
from linear and
branched aliphatic radicals comprising from 1 to 4 carbon atoms, and aromatic
radicals such as
aryl and alkylaryl. The aliphatic radicals may comprise at least one hetero
atom such as oxygen,
nitrogen, sulphur and halogens. The aliphatic radicals are chosen, for
example, from alkyl,
alkoxy, alkylamide and hydroxyalkyl radicals comprising from about 1 to 4
carbon atoms;
R3 and R4, which may be identical or different, are chosen from linear and
branched alkyl
radicals comprising from 12 to 30 carbon atoms, the said alkyl radicals
comprise at least one
function chosen from ester and amide functions.
R3 and R4 are chosen, for example, from (C12-C22)alkylamido(CZ-C6)alkyl and
(C12-
C22)alkylacetate radicals.
The cationic surfactant is, for example, a dicetyldimethyl ammonium salt (for
example chloride);
B) the quaternary ammonium salts of imidazolinium, such as that of formula
(IX) below:
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W245FQ/JC 37
+
Re
CH2-CH2-N(R8)-CO-R5 X
N / N\ /
R7
(IX)
in which R5 is chosen from alkenyl and alkyl radicals comprising from 8 to 30
carbon atoms, for
example fatty acid derivatives of tallow,
R6 is chosen from a hydrogen atom, C1-C4 alkyl radicals and alkenyl and alkyl
radicals
comprising from 8 to 30 carbon atoms, R7 is chosen from CI -C4 alkyl radicals,
R8 is chosen from
a hydrogen atom and CI-C4 alkyl radicals, and X- is an anion chosen from
halides, phosphates,
acetates, lactates, alkyl sulphates, alkyl sulphonates and alkylaryl
sulphonates.
In one embodiment, R5 and R6 are, for example, a mixture of radicals chosen
from alkenyl and
alkyl radicals comprising from 12 to 21 carbon atoms, such as fatty acid
derivatives of tallow, R7
is methyl and R8 is hydrogen. Such a product is, for example, Quaternium-27
(CTFA 1997) or
Quaternium-83 (CTFA 1997), which are sold under the names "Rewoquat " W75,
W90,
W75PG and W75HPG by the company Witco,
C) the diquaternary ammonium salts of formula (X):
[(R9)(R10)(Rl l)-N-(CH2)3-N(R12)(R13)(R14)]++ 2X" (X)
in which R9 is chosen from aliphatic radicals comprising from about 16 to 30
carbon atoms,
R10, R1 l, R12, R13 and R14, which may be identical or different, are chosen
from hydrogen and
alkyl radicals comprising from 1 to 4 carbon atoms, and
X- is an anion chosen from halides, acetates, phosphates, nitrates and methyl
sulphates. Such
diquatemary ammonium salts, for example, include propanetallowdiammonium
dichloride; and
D) the quatemary ammonium salts comprising at least one ester function, of
formula (XI) below:
(CrH2rO)z-R 18
1
R17-CO-(OCnH20y- i +-(CpH2pO)XR16 X-
R 15 (XI)
in which:
R15 is chosen from C1-C6 alkyl radicals and Cl-C6 hydroxyalkyl and
dihydroxyalkyl radicals;
R16 is chosen from: a radical R19C(O)-, linear and branched, saturated and
unsaturated C1-C22
hydrocarbon-based radicals R20, and a hydrogen atom, R18 is chosen from: a
radical R21C(O)-,
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W245FQ/JC 38
linear and branched, saturated and unsaturated Ci-C6 hydrocarbon-based
radicals R22, and
a hydrogen atom, R17, R19 and R21, which may be identical or different, are
chosen from linear
and branched, saturated and unsaturated C7-C21 hydrocarbon-based radicals; n,
p and r, which
may be identical or different, are chosen from integers ranging from 2 to 6; y
is chosen from
integers ranging from 1 to 10; x and z, which may be identical or different,
are chosen from
integers ranging from 0 to 10; X- is an anion chosen from simple and complex,
organic and
inorganic anions; with the proviso that the sum x+y+z is from I to 15, that
when x is 0, then R16
is R20 and that when z is 0, then R18 is R22.
In one embodiment, the ammonium salts of formula (XI) may be used, in which:
R15 is chosen from methyl and ethyl radicals, x and y are equal to 1; z is
equal to 0 or 1; n, p and
r are equal to 2; R16 is chosen from: a radical R19C(O)-,methyl, ethyl and C14-
C22
hydrocarbon-based radicals, and a hydrogen atom; R17, R19 and R21, which may
be identical or
different, are chosen from linear and branched, saturated and unsaturated C7-
C2 1, hydrocarbon-
based radicals; R18 is chosen from: a radical R21C(O)- and a hydrogen atom.
Such compounds
are sold, for example, under the names Dehyquart by the company Cognis,
Stepanquat by the
company Stepan, Noxamium by the company Ceca, and Rewoquat WE 18 by the
company
Rewo-Witco.
Chelants: According to the present invention the compositions may comprise
chelants.
Chelants are well known in the art and refer to a molecule or a mixture of
different molecules
each capable of forming a chelate with a metal ion. Chelants are well known in
the art and a non-
exhaustive list thereof can be found in AE Martell & RM Smith, Critical
Stability Constants, Vol.
1, Plenum Press, New York & London (1974) and AE Martell & RD Hancock, Metal
Complexes
in Aqueous Solution, Plenum Press, New York & London (1996) both incorporated
herein by
reference.
Chelants suitable for use herein are carboxylic acids (in particular
aminocarboxylic acids),
polyamines, phosphonic acids (in particular aminophosphonic acids) and
polyphosphoric acids
(in particular linear polyphosphoric acids), their salts and derivatives.
Examples of preferred chelants include ethylenediaminotetraacetic acid (EDTA),
nitrilotriacetic
acid, diethylenetriamine pentaacetic acid (DTPA), ethylenediamine disuccinic
acid (EDDS),
ethylenediamine diglutaric acid (EDGA), 2-hydroxypropylenediamine disuccinic
acid (HPDS),
glycinamide-N,N'-disuccinic acid (GADS), ethylenediamine-N-N'-diglutaric acid
(EDDG),
2-hydroxypropylenediamine-N-N'-disuccinic acid (HPDDS), salts thereof and
derivatives thereof.
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Chelants may be incorporated into the composition of the present invention as
stabilizers and or
preservatives. In addition it has also been found that chelants provide hair
fibre damage benefits
and thus they may be utilized in order to further improve the hair damage
profile of the present
invention. Levels of chelants in the present invention may be as low as about
0.1% by weight,
preferably at least about 0.25% by weight, more preferably about 0.5% by
weight, for the most
effective chelants such as diamine-N,N'-dipolyacid chelants and monoamine
monoamide-N,N'-
dipolyacid chelants (for example EDDS). Less effective chelants will be more
preferably used at
levels of at least about 1% by weight, even more preferably above about 2% by
weight of the
composition, depending of the efficiency of the chelant. Levels as high as
about 10% by weight
may be used, but above this level significant formulation issues may arise.
Solvents: Suitable solvents for use in the compositions of the present
invention include, but
are not limited to, water, butoxydiglycol, 1,2-propylene glycol, glycerol,
lower aliphatic alcohols
(e.g. ethanol, n-propanol or isoproanol), ethoxydiglycol, isopropylalcohol,
hexylene glycol,
benzyl alcohol and dipropylene glycol.
Antioxidants or reducing a eg nts: Suitable antioxidants or reducing agents
for use in the
compositions of the present invention include, but are not limited to,
ascorbic acid, thioglycolic
acid and sodium sulfite.
The form of the oxidation dye precursor composition and also for the ready-to-
apply dye mixture
may be, for example, a solution, especially an aqueous or aqueous-alcoholic
solution. However a
particularly preferred form of the composition according to the invention is a
cream, a gel or an
emulsion. Its composition comprises a mixture of the dye ingredients with the
conventional
additive ingredients usually used in this type of preparation.
According to a preferred embodiment of the present invention dye powders,
granules or pellets
are mixed with an appropriate dye carrier mass prior to use to form the
oxidation dye precursor
composition. Particularly preferred is the use of the dye-containing
granules/pellets according to
WO 2005/044208 which are mixed with an appropriate dye carrier mass prior to
use to form the
oxidation dye precursor composition. WO 2005/044208 herewith is explicitly
incorporated
herein by reference.
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W245FQ/JC 40
The ready-to-apply hair dye mixture according to the invention is preferably
made by a method
comprising mixing the oxidation dye precursor composition with a liquid
oxidizing agent
immediately prior to application.
Hydrogen peroxide, or its addition compounds with urea, melamine or sodium
bromate, in the
form of a 1 to 12 percent by weight, preferably 6 percent by weight, aqueous
solution, is
preferred as the oxidizing agent. Hydrogen peroxide is especially preferred.
The oxidation dye precursor composition and the oxidizing agent are mixed with
each other in a
weight ratio of from 5:1 to 1:3. A weight ratio of 1:1 to 1:2 is especially
preferred.
The pH of the ready-to-apply hair dye mixture according to the invention is
adjusted during the
mixing of the preferred alkaline oxidation dye precursor composition with the
mostly acidic
oxidizing agent. The resulting pH value of the mixture is determined by the
alkali content of the
dye-carrying or oxidation dye precursor composition, the acid content of the
oxidizing agent and
the mixing ratio. The pH of the ready-to-apply hair dye composition amounts to
3 to 11,
preferably from 6 to 10.5.
The pH values of both the oxidation dye precursor composition and the
oxidizing agent-
containing composition may both be adjusted by adding dilute organic or
inorganic acids, such as
phosphoric acid, ascorbic acid and lactic acid, or bases, such as
monoethanolamine,
triethanolamine, 2-amino-2-methyl-l-propanol, ammonia, sodium hydroxide,
potassium
hydroxide or tris(hydroxymethyl)aminomethane.
After mixing the above-described oxidation dye precursor composition with an
oxidizing agent,
an amount of the ready-to-apply hair dye mixture sufficient for dyeing the
hair, generally from 60
to 200 grams, is applied to the hair.
The hair dye mixture is allowed to act on the hair after application for 10 to
45 minutes at 15 to
50 C, preferably for 30 to 40 minutes at 30 C to 40 C. It is subsequently
rinsed from the hair
with water. If necessary the hair is washed with a shampoo after rinsing with
water and perhaps
with a dilute weak organic acid, for example citric or tartaric acid.
Subsequently the hair is dried.
CA 02646867 2008-12-16
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The new p-phenylenediamine derivatives of formula (I) allow the creation of
non-sensitizing
oxidative hair dyes with good dyeing properties.
The examples below are intended to illustrate the subject-matter of the
invention in more detail
without limiting it thereto.
EXAMPLES
Example lA to 3100A: Hair Dye Solution
Dye carrier mass A: 10.0 g Sodium lauryl ether sulfate (28 % strength aqueous
solution)
7.8 g Ethanol
0.3 g Ascorbic acid
0.3 g Sodium sulfite, anhydrous
0.3 g Ethylenediaminetetraacetic acid disodium salt hydrate
9.0 g Ammonium hydroxide (22 % strength aqueous solution)
X g Dyes (according to the below-mentioned table 2)
ad 100.0 g Water, demineralized
The pH of the solution was between 10 and 10.5.
Immediately prior to application 50 g of the above-described dye carrier mass
A are mixed with
50 grams of a 6% by weight aqueous hydrogen peroxide solution. The resulting
ready-to-apply
hair dye mixture is applied to the hair in the required amount. After an
acting time of 30 minutes
at 40 C the hair is washed with a shampoo, rinsed with water and dried.
Example 1 B to 3100B; Hair Dye Cream
Dye carrier mass B: 15.00 g Cetylstearylalcohol
2.30 g Glycerinmonostearate
0.80 g Lanolin
3,80 g Lanolinalcohol
3.50 g Sodium lauryl diglykolether sulfate (28 % strength aqueous
CA 02646867 2008-12-16
W245FQ/JC 42
solution)
1.42 g Steareth-20
7.80 g Ethanol
0.30 g Ascorbic acid
0.30 g Sodium sulfite, anhydrous
0.30 g ethylenediaminetetraacetic acid disodium salt hydrate
10.00 g Ammonium hydroxide (22 % strength aqueous solution)
0.20 g Perfume
X g Dyes (according to the below-mentioned table 2)
ad 100.00 g Water, demineralized
The pH of the cream was between 9.5 and 10.5.
Immediately prior to application 75 g of the above-described dye carrier mass
B are mixed with
50 grams of a 9% by weight aqueous hydrogen peroxide solution. The resulting
ready-to-use hair
dye mixture is applied to the hair in the required amount. After an acting
time of 30 minutes at 40
C the hair is washed with a shampoo, rinsed with water and dried.
Example 1C to 3100C: Hair Dye Gel
Dye carrier mass C: 15,00 g Oleic acid
3,00 g Glycerol
7,00 g Isopropanol
0,50 g Ascorbic acid
0,40 g Sodium sulfite, anhydrous
0,40 g Sodium hydroxide
10,00 g Ammonium hydroxide (25 % strength aqueous solution)
X g Dyes (according to the below-mentioned table 2)
ad 100,00 g Water, demineralized
Immediately prior to application 100 g of the above-described dye carrier mass
C are mixed with
100 grams of a 6% by weight aqueous hydrogen peroxide solution. The resulting
ready-to-apply
CA 02646867 2008-12-16
W245FQ/JC 43
hair dye mixture is applied to the hair in the required amount. After an
acting time of 30 minutes
at 40 C the hair is washed with a shampoo, rinsed with water and dried.
Example 1D to 3100D: Hair Dye
Dye carrier mass D: 9.500 g Propylene glycol
5.000 g Ammonium hydroxide
4.000 g Ethoxydiglycol
4.500 g Ethanolamine
1.000 g Oleic acid
6.000 g Hexylene glycol
3.500 g Cocamidopropyl betaine
0.300 g Oleth-10
0.300 g Oleth-2
1.500 g Dilinoleic acid
0.500 g C 12-C 15 Pareth-3
7.000 g Soytrimonium chloride
0.005 g Sodium metasilicate
0.500 g Erythorbic acid
0.300 g Ethylenediaminetetraacetic acid disodium salt
0.300 g Sodium sulfite
X g Dyes (according to the below-mentioned table 2)
ad 100.000 g Water, demineralized
Immediately prior to application 75 g of the above-described dye carrier mass
D are mixed with
50 grams of a 9% by weight aqueous hydrogen peroxide solution. The resulting
ready-to-use hair
dye mixture is applied to bleached hair in the required amount. After an
acting time of 40
minutes at 30 C the hair is washed with a shampoo, rinsed with water and
dried.
Example lE to 3100E: Nonionic Hair Dye
Dye carrier mass E: 7.00 g Cetylstearyl alcohol
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W245FQ/JC 44
2.00 g Glyceryl oleate
13.00 g Polysorbate 40
6.00 g Ceteareth-50
0.50 g Sodium sulfite, anhydrous
0.10 g Ethylenediaminetetraacetic acid disodium salt
8.00 g Ammonia (25% strength aqueous solution)
X g Dyes (according to the below-mentioned table 2)
ad 100.00 g Water
Hydrogen peroxide emulsion
3.0 g Cetylstearyl alcohol
0.8 g PEG-25 cetyl/stearyl ether
0.3 g Lanolin alcohol
6.0 g Hydrogen peroxide
0.1 g Phosphoric acid (85% strength aqueous solution)
ad 100.0 g Water
60 g of the above non-ionic dye carrier mass E are mixed prior to application
with 60 g of the
above hydrogen peroxide emulsion (pH = 2.5). The pH of the resulting ready-to-
use hair dye
composition is about 10. The resulting ready-to-use hair dye mixture is
applied to bleached hair
in the required amount. After an acting time of 30 minutes at 40 C the hair
is washed with a
shampoo, rinsed with water and dried.
Example 1F to 3100F: Hair Dye
Dye carrier mass F: 0.100 g Sodium sulphite
0.200 g Ascorbic Acid
0.003 g Ethylenediaminetetraacetic acid disodium salt
0.200 g Citric Acid
4.000 g Ammonia (30% strength aqueous solution)
1.000 g Acrylates Copolymer (Aculyn 33A)
0.500 g Oleth 5
1.000 g Oleth 2
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W245FQ/JC 45
0.900 g Oleic Acid
3.000 g Cocamidopropyl betaine
0.050 g Etidronic Acid
1.000 g Trisodium Ethylenediamine disuccinate
2.500 g Isopropyl alcohol
8.600 g Hydrogen Peroxide (35% aqueous solution)
3.000 g Soytrimonium Chloride and propylene glycol
0.003 g Simethicone
1.000 g Steareth-21
0.500 g PEG-50 Hydrogenated Palmamide
0.200 g Oleyl Alcohol
0.500 g Acrylates Steareth-20 Methacrylate Copolymer (Aculyn(V 22)
2.000 g Propylene Glycol
4.200 g Ethoxy Diglycol
0.500 g C 11-15 Pareth-9
0.800 g C12-15 Pareth-3
X g Dyes (according to the below-mentioned table 2)
ad 100.000 g Water
The pH of the ready-to-use hair dye composition is about 10. The ready-to-use
hair dye mixture
is applied to bleached hair in the required amount. After an acting time of 40
minutes at 30 C the
hair is washed with a shampoo, rinsed with water and dried.
Example 1 G to 3100G: Hair Dye
Dye carrier mass G: 0.100 g Sodium sulphite
0.200 g Ascorbic Acid
0.003 g Ethylenediaminetetraacetic acid disodium salt
0.200 g Citric Acid
4.000 g Ammonia (30% strength aqueous solution)
1.000 g Acrylates Copolymer (Aculyn(V 33A)
0.500 g Oleth 5
1.000 g Oleth 2
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W245FQ/JC 46
0.900 g Oleic Acid
3.000 g Cocamidopropyl betaine
0.050 g Etidronic Acid
1.000 g Trisodium Ethylenediamine disuccinate
2.500 g Isopropyl alcohol
13.000 g Hydrogen Peroxide (35% aqueous solution)
3.000 g Soytrimonium Chloride and propylene glycol
0.003 g Simethicone
1.000 g Steareth-21
0.500 g PEG-50 Hydrogenated Palmamide
0.200 g Oleyl Alcohol
1.000 g Acrylates Steareth-20 Methacrylate Copolymer (Aculyn 22)
2.000 g Propylene Glycol
4.200 g Ethoxy Diglycol
0.500 g C 11-15 Pareth-9
0.800 g C12-15 Pareth-3
X g Dyes (according to the below-mentioned table 2)
ad 100.000 g Water
The pH of the ready-to-use hair dye composition is about 10. The ready-to-use
hair dye mixture
is applied to bleached hair in the required amount. After an acting time of 30
minutes at 40 C the
hair is washed with a shampoo, rinsed with water and dried.
Example 1H to 3100H: Hair Dye
Dye carrier mass H: 0.1 g Sodium sulphite
0.1 g Ascorbic Acid
5.0 g Ammonium Carbonate
0.1 g Potassium Hydrogen Carbonate
0.2 g Ammonium Acetate
2.0 g Cetearyl Alcohol (and) Dicetyl Phosphate (and) Ceteth-10
Phosphate (Crodafos(V CES)
1.0 g Ceteareth-25 (Volpo(I CS25)
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W245FQ/JC 47
2,0 g Sodium Glycinate
2.0 g Stearyl Alcohol
0.3 g Sodium Hydroxide (50% aqueous solution)
0.1 g Ethylenediaminetetraacetic acid tetrasodium salt
0.5 g Etidronic Acid
8.6 g Hydrogen Peroxide (35% aqueous solution)
0.2 g Polyquaternium-22 (Merquat 295)
0.2 g Polyquaternium-37 & Mineral oil (Salcare SC95)
0.1 g Styrene-PVP Copolymer (Polectron(t 430)
0.1 g Xanthan gum
2.0 g Cetyl Alcohol
1.0 g Acrylates copolymer (Aculyn 33)
X g Dyes (according to the below-mentioned table 2)
ad 100.0 g Water
The pH of the ready-to-use hair dye composition is about 9. The ready-to-use
hair dye mixture is
applied to bleached hair in the required amount. After an acting time of 40
minutes at 30 C the
hair is washed with a shampoo, rinsed with water and dried.
Example lI to 3 1001: Hair Dye
Dye carrier mass I: 0.1 g Sodium sulphite
0.1 g Ascorbic Acid
6.0 g Ammonium Carbonate
0.1 g Potassium Hydrogen Carbonate
0.2 g Ammonium Acetate
2.0 g Cetearyl Alcohol (and) Dicetyl Phosphate (and) Ceteth-10
Phosphate (Crodafos(V CES)
0.3 g Sodium Hydroxide (50% aqueous solution)
0.1 g Ethylenediaminetetraacetic acid tetrasodium salt
0.5 g Etidronic Acid
8.6 g Hydrogen Peroxide (35% aqueous solution)
1.0 g Amodimethicone (Belsil ADM1100)
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W245FQ/JC 48
0.5 g Styrene-PVP Copolymer (Polectron(V 430)
0.5 g Acrylates/C10-30 Alkyl Acrylate Crosspolymer
1.0 g Acrylates Steareth-20 Methacrylate Copolymer (Aculyn (V 22)
1.0 g Acrylates copolymer (Aculyn(V 33)
X g Dyes (according to the below-mentioned table 2)
ad 100.0 g Water
The pH of the ready-to-use hair dye composition is about 9. The ready-to-use
hair dye mixture is
applied to bleached hair in the required amount. After an acting time of 30
minutes at 40 C the
hair is washed with a shampoo, rinsed with water and dried.
Example 1K to 3100K: Hair Dye
Synthesis of dye granules/pellets according to WO 2005/044208 (general method
for producin~
granules/pellets of each dye mixture 1 to 3100): In a Glatt fluidized bed
granulator and coater, 400
g of the respective dye mixture 1 to 3100 according to table 2 are heated to a
product temperature of
34 C with air at an incoming air temperature of 90 C and an air flow rate of
18 m3/h. A 20 %
aqueous polyvinylpyrrolidone solution ("spraying solution") is then sprayed
onto this mixture at an
initial spraying rate of 8 g/min and at a spraying air pressure of 0.5 bar. In
the course of the
granulation process, the spraying rate is increased to 12 g/min and the
incoming air temperature is
increased to 100 C, while the air flow rate is raised to a maximum of 30
m3/h. The product
temperature is kept at about 30-31 C throughout the entire procedure. After
310 g of the
polyvinylpyrrolidone solution has been sprayed on, the granules/pellets are
dried at a maximum
product temperature of 57 C and then cooled to about 30 C and screened.
Before use these granules/pellets (comprising the dye combinations 1 to 3100
as described in the
below-mentioned table 2) are mixed with the following peroxide solution or
emulsion in a 1:1 ratio.
Hydrogen Peroxide Emulsion: 9.00 g Hydrogen peroxide
1.80 g Cetylstearyl alcohol
3.30 g Polyvinylpyrrolidone-styrene copolymer
0.20 g Disodium phosphate
0.20 g Sodium laurylsulfate
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0.10 g Salicylic acid
0.08 g Phosphoric acid
to 100.00 g Water, demineralized
The resulting ready-to-apply dye mixture is applied to the hair in the
required amount. After an
acting time of 40 minutes at 30 C the hair is washed with a shampoo, rinsed
with water and
dried.
Example 1L to 3100 L: Hair Dye
S3nthesis of dye rg anules/pellets according to WO 2005/044208 (general method
for producing
apr nules/pellets of each dye mixture 1 to 3100): In a Glatt fluidized bed
granulator and coater, 400
g of the respective dye mixture 1 to 3100 according to table 2 are heated to a
product temperature of
34 C with air at an incoming air temperature of 90 C and an air flow rate of
18 m3/h. A 20 %
aqueous polyvinylpyrrolidone solution ("spraying solution") is then sprayed
onto this mixture at an
initial spraying rate of 8 g/min and at a spraying air pressure of 0.5 bar. In
the course of the
granulation process, the spraying rate was increased to 12 g/min and the
incoming air temperature is
increased to 100 C, while the air flow rate was raised to a maximum of 30
m3/h. The product
temperature is kept at about 30-31 C throughout the entire procedure. After
310 g of the
polyvinylpyrrolidone solution has been sprayed on, the granules/pellets are
dried at a maximum
product temperature of 57 C and then cooled to about 30 C and screened.
Before use these granules/pellets (comprising one of the dye combinations 1 to
3100 as described in
the below-mentioned table 2) are included in one of the above dye carrier
masses A to I as the "Xg
Dyes (according to the below-mentioned table 2)" in the needed ratio. Then 60
g of the resulting
composition are mixed with 60 grams of a 6% by weight aqueous hydrogen
peroxide solution.
The resulting ready-to-apply hair dye mixture is applied to the hair in the
required amount. After
an acting time of 30 minutes at 40 C the hair is washed with a shampoo,
rinsed with water and
dried.
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Table 1: Dyes Used in Dye Combinations of Table 2
El 1,4-diamino-2-(methoxymethyl)benzene sulfate
E2 1,4-diamino-2-methylbenzene sulfate
E3 1, 4-diaminobenzene
E4 1,4-diamino-2-(2-hydroxyethyl)benzene sulfate
E5 3-methyl-4-aminophenol
E6 4-aminophenol
E7 N,N-bis(2'-hydroxyethyl)-p-phenylenediamine sulfate
E8 4,5-diamino-l-(2-hydroxyethyl)-1H-pyrazole sulfate
E9 4-(methylamino)phenol
E10 2,4,5,6-pyrimidinetetramine
E11 4-hydroxy-2,5,6-triaminopyrimidine sulfate
Coupter substances
Kl 2-amino-4-((2'-hydroxyethyl)amino)anisole sulfate
K2 2,4-diamino-l-(2'-hydroxyethoxy)benzene sulfate
K3 3-amino-2-methylamino-6-methoxypyridine
K4 3,5-diamino-2,6-dimethoxypyridine dihydrochloride
K5 1,3-Bis(2,4-diaminophenoxy)propane tetrahydrochloride
K6 3-aminophenol
K7 5-amino-2-methylphenol
K8 5-amino-6-chlor-2-methylphenol
K9 5-[(2-hydroxyethyl)amino]-2-methylphenol
K10 5-amino-4-chloro-2-methylphenol
Kl l 1-naphthol
K12 resorcinol
K13 2-methylresorcinol
K14 4-chlororesorcinol
K15 4-(2'-hydroxyethyl)amino-l,2-methylendioxybenzene*HCl
K16 3-amino-2,6-dimethyl-phenol
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K17 1,5-naphthalenediol
K18 2,7-naphthalenediol
K19 3,4-dihydro-2H-1,4-benzoxazin-6-ol
K20 5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one
K21 3 -am ino-2, 4-dichlorophenol
K22 2,6-Dihydroxy-3,4-dimethylpyridine
K23 6-hydroxy-1 H-Indole
K24 2-amino-3-hydroxypyridine
K25 2-amino-5-ethylphenol
Direct Dyes
Dl 2,6-diamino-3-((pyridin-3 -yl)azo)pyridine
D2 6-chloro-2-ethylamino-4-nitrophenol
D3 2-amino-6-chloro-4-nitrophenol
3-((9,10-dihydro-9,10-dioxo-4-(methylamino)-1-anthracenyl)amino)-N,N-
J1
dimethyl-N-propyl-l-propanaminium bromide
Table 2: Dye Combinations 1 to 3100
1. 0.250g El + 1.935g K16 + 0.263g K12 + 0.250g E8 + 0.263g K6
2. 2.500g E2 + 2.625g K12 + 1.673g K16 + 2.500g E8 + 2.625g K7
3. 1.250g E3 + 1.313g K12 + 1.250g E8 + 0.185g K16 + 1.313g K9
4. 0.250g E4 + 0.263g K12 + 0.250g E8 + 0.263g K13 + 0.057g K16
5. 0.250g El + 0.057g K16 + 0.263g K12 + 0.250g E8 + 0.263g K1 + 0.065g K3
6. 2.500g E2 + 2.625g K12 + 0.057g K16 + 2.500g E8 + 0.l00g K23 + 2.625g K11
7. 0.250g E3 + 0.263g K12 + 0.250g E8 + 0.057g K16 + 0.263g K14
8. 0.250g E4 + 0.263g K12 + 0.250g E8 + 0.263g K24 + 0.057g K16
9. 0.250g El + 0.057g K16 + 0.263g K12 + 0.250g E8 + 0.263g K2
10. 0.200g E2 + 0.210g K12 + 0.057g K16 + 0.200g E8 + 0.210g K6 + 0.210g K7
11. 0.200g E3 + 0.210g K12 + 0.200g E8 + 0.057g K16 + 0.210g K6 + 0.210g K9
12. 1.000g E4 + 1.050g K12 + 1.000g E8 + 1.050g K6 + 0.057g K16 + 1.050g K22
13. 2.000g El + 2.100g K12 + 2.000g E8 + 2.100g K6 + 2.100g K1 + 0.057g K16
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14. 0.200gE10+0.057gK16+0.210gK12+0.200gE8+0.210gK6+0.210gK11
15. 0.200g E3 + 0.210g K12 + 0.057g K16 + 0.200g E8 + 0.210g K6 + 0.210g K14
16. 0.200g E4 + 0.210g K12 + 0.200g E8 + 0.057g K16 + 0.210g K6 + 0.210g K24
17. 1.000g E1 + 1.050g K12 + 1.000g E8 + 1.050g K6 + 0.057g K16 + 1.050g K2
18. 2.000g E2 + 2.100g K12 + 2.000g E8 + 2.100g K7 + 2.100g K9 + 0.057g K16
19. 2.000g E3 + 0.057g K16 + 2.100g K12 + 2.000g E8 + 2.100g K7 + 2.100g K13
20. 2.000g E4 + 2.100g K12 + 0.057g K16 + 2.000g E8 + 2.100g K7 + 2.100g K1
21. 1.000g El + 1.050g K12 + 1.000g E8 + 0.057g K16 + 1.050g K7 + 1.050g Kl 1
22. 1.000g E2 + 1.050g K12 + 1.000g E8 + 1.050g K7 + 0.057g K16 + 1.050g K14
23. 2.000g E3 + 2.100g K12 + 2.000g E8 + 2.100g K7 + 2.100g K24 + 0.057g K16
24. 2.000g E4 + 0.057g K16 + 2. l00g K12 + 2.000g E8 + 2.100g K8 + 2.100g K2
25. 1.000g El + 1.050g K12 + 0.057g K16 + 1.000g E8 + 1.050g K9 + 1.050g K13
26. 0.200g E2 + 0.210g K12 + 0.200g E8 + 0.057g K16 + 0.210g K9 + 0.210g K1
27. 1.000g E3 + 1.050g K12 + 1.000g E8 + 1.050g K9 + 0.057g K16 + 1.050g K11
28. 2.000g E4 + 2.100g K12 + 2.000g E8 + 2.l00g K9 + 2.l00g K14 + 0.057g K16
29. 0.200g El + 0.057g K16 + 0.210g K12 + 0.200g E8 + 0.210g K9 + 0.210g K24
30. 1.000g E2 + 1.050g K12 + 0.057g K16 + 1.000g E8 + 1.050g K9 + 1.050g K2
31. 2.000g E3 + 2.l00g K12 + 2.000g E8 + 0.057g K16 + 2.l00g K13 + 2.100g K1
32. 0.200g E4 + 0.210g K12 + 0.200g E8 + 0.210g K13 + 0.057g K16 + 0.210g Kl 1
33. 2.000gEl +2.100gK12+2.000gE8+2.100gK13+2.l00gK14+0.260gK16
34. 1.000g E2 + 0.260g K16 + 1.050g K12 + 1.000g E8 + 1.050g K13 + 1.050g K24
35. 2.000g E3 + 2.100g K12 + 0.260g K16 + 2.000g E8 + 2.l00g K13 + 2.100g K2
36. 0.200g E4 + 0.210g K12 + 0.200g E8 + 0.260g K16 + 0.210g K4 + 0.210g Kl 1
37. 1.000g El + 1.550g K12 + 1.000g E8 + 1.050g K1 + 0.050g K5 + 0.260g K16 +
1.050g K14
38. 1.000g E2 + 1.050g K12 + 1.000g E8 + 1.050g K1 + 1.050g K24 + 0.260g K16
39. 1.000g E3 + 0.260g K16 + 1.050g K12 + 1.000g E8 + 1.050g K1 + 1.050g K2
40. 0.200g E4 + 0.210g K12 + 0.260g K16 + 0.200g E8 + 0.210g K11 + 0.210g K14
41. 1.000g El + 1.050g K12 + 1.000g E8 + 0.260g K16 + 1.050g K11 + 1.050g K24
42. 0.200g E2 + 0.210g K12 + 0.200g E8 + 0.210g K11 + 0.260g K16 + 0.210g K2
43. 1.000g E3 + 1.050g K12 + 1.000g E8 + 1.050g K14 + 1.050g K24 + 0.260g K16
44. 2.000g E4 + 0.260g K16 + 2.100g K12 + 2.000g E8 + 2.100g K14 + 2.100g K2
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45. 0.200g E1 + 0.210g K12 + 0.260g K16 + 0.200g E8 + 0.210g K24 + 0.210g K2
46. 2.500g E2 + 2.625g K12 + 2.500g E6 + 0.260g K16 + 2.625g K6 + 0.135g K20
47. 2.500g E3 + 2.625g K12 + 2.500g E6 + 2.625g K7 + 0.260g K16
48. 2.500g E4 + 0.260g K16 + 2.625g K12 + 2.500g E6 + 2.625g K9 + 0.150g K20
49. 1.250g El + 1.313g K12 + 0.260g K16 + 1.250g E6 + 1.313g K13
50. 2.500g E2 + 2.625g K12 + 2.500g E6 + 0.260g K16 + 2.625g KI
51. 0.250g E3 + 0.263g K12 + 0.250g E6 + 0.263g K11 + 0.260g K16
52. 0.250g E4 + 0.260g K16 + 0.263g K12 + 0.250g E6 + 0.263g K14
53. 2.500g El + 2.625g K12 + 0.260g K16 + 2.500g E6 + 2.625g K24
54. 0.250g E2 + 0.263g K12 + 0.250g E6 + 0.260g K16 + 0.109g E9 + 0.263g K2
55. 1.000g E3 + 1.050g K12 + 1.000g E6 + 1.050g K6 + 0.260g K16 + 1.050g K7
56. 0.200g E4 + 0.210g K12 + 0.200g E6 + 0.210g K6 + 0.210g K9 + 0.260g K16
57. 0.200g El + 0.260g K16 + 0.210g K12 + 0.200g E6 + 0.210g K6 + 0.210g K13
58. 1.000g E2 + 1.050g K12 + 0.260g K16 + 1.000g E6 + 1.050g K6 + 1.050g K1
59. 2.000g E3 + 2.100g K12 + 2.000g E6 + 0.260g K16 + 2.100g K6 + 2.100g Kl 1
60. 1.000g E4 + 1.050g K12 + 1.000g E6 + 1.050g K6 + 0.260g K16 + 1.050g K14
61. 1.000g El + 1.050g K12 + 1.000g E6 + 1.050g K6 + 1.050g K24 + 0.260g K16
62. 0.200g K6 + 0.210g K12 + 0.200g K8 + 0.210g K16 + 0.210g K2 + 0.060g K19
63. 2.000g E10 + 0.383g K16 + 2.100g K12 + 2.000g E6 + 2.100g K8 + 2.100g K9
64. 0.200g E3 + 0.210g K12 + 0.383g K16 + 0.200g E6 + 0.210g K7 + 0.210g K13
65. 2.000g E4 + 2.100g K12 + 2.000g E6 + 0.090g E9 + 0.383g K16 + 2.100g K7 +
2.100g Kl
66. 1.000g E11 + 1.050g K12 + 1.000g K7 + 1.050g K16 + 1.050g K11
67. 0.200gE10+0.210gK12+0.200gE6+0.210gK7+ 1.531gK16+0.210gK14
68. 2.000g E2 + 2. l00g K12 + 2.000g E6 + 2.100g K7 + 2.100g K24 + 1.53 lg K16
69. 0.200gE3+1.531gK16+0.210gK12+0.200gE6+0.210gK7+0.210gK2
70. 2.000g E11 + 2.100g K12 + 2.000g K6 + 2.l00g K16 + 2.100g K13
71. 0.200g E4 + 0.210g K12 + 1.970g K16 + 0.200g E6 + 0.210g K9 + 0.210g Kl
72. 1.000g E1 + 1.050g K12 + 1.000g E6 + 1.970g K16 + 1.050g K9 + 1.050g K11
73. 1.000g E2 + 1.050g K12 + 1.000g E6 + 1.050g K9 + 1.970g K16 + 1.050g K14
74. 0.200g E3 + 0.210g K12 + 0.200g E6 + 0.210g K9 + 0.210g K24 + 1.970g K16
75. 1.000g E4 + 1.970g K16 + 1.050g K12 + 1.000g E6 + 1.050g K9 + 1.050g K2
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76. 2.000g E1 + 2.100g K12 + 1.970g K16 + 2.000g E6 + 2.100g K13 + 2.100g K1
77. 0.200g E2 + 0.210g K12 + 0.200g E6 + 1.970g K16 + 0.210g K13 + 0.210g K11
78. 2.000g E3 + 2.100g K12 + 2.000g E6 + 2.100g K13 + 1.970g K16 + 2.100g K14
79. 1.000g E4 + 1.050g K12 + 1.000g E6 + 1.050g K13 + 1.050g K24 + 1.970g K16
80. 0.200g El + 1.970g K16 + 0.210g K12 + 0.200g E6 + 0.210g K13 + 0.210g K2
81. 2.000g E2 + 2.100g K12 + 1.970g K16 + 2.000g E6 + 2.100g K1 + 2.100g K11
82. 1.000g E3 + 1.050g K12 + 1.000g E6 + 1.970g K16 + 1.050g Kl + 1.050g K14
83. 1.000g E4 + 1.050g K12 + 1.000g E6 + 1.050g Kl + 1.970g K16 + 1.050g K24
84. 1.000g El + 1.050g K12 + 1.000g E6 + 1.050g Kl + 1.050g K2 + 1.970g K16
85. 2.000g E2 + 1.970g K16 + 2.100g K12 + 2.000g E6 + 2.100g K11 + 2.100g K14
86. 1.000g E3 + 1.050g K12 + 1.970g K16 + 1.000g E6 + 1.050g Kl 1+ 1.050g K24
87. 2.000g E4 + 2.100g K12 + 2.000g E6 + 1.970g K16 + 2.100g K11 + 2.100g K2
88. 2.000g El + 2.100g K12 + 2.000g E6 + 2.100g K14 + 1.970g K16 + 2.100g K24
89. 0.200g E2 + 0.210g K12 + 0.200g E6 + 0.210g K14 + 0.210g K2 + 1.970g K16
90. 2.000g E3 + 1.970g K16 + 2.100g K12 + 2.000g E6 + 2.100g K24 + 2.100g K20
91. 1.250g E4 + 1.313g K12 + 1.970g K16 + 1.250g E5 + 1.313g K6
92. 0.250g El + 0.263g K12 + 0.250g E5 + 1.970g K16 + 0.263g K7
93. 2.500g E2 + 2.625g K12 + 2.500g E5 + 2.625g K9 + 1.970g K16 + O.OlOg K23
94. 0.250g E3 + 1.970g K16 + 0.263g K12 + 0.250g E5 + 0.263g K13
95. 0.250g E4 + 0.263g K12 + 1.970g K16 + 0.250g E5 + 0.263g K1
96. 1.250g E1 + 1.313g K12 + 1.250g E5 + 1.970g K16 + 1.313g K11
97. 1.250g E10 + 1.313g K12 + 1.250g E5 + 1.313g K14 + 1.970g K16
98. 0.250g E3 + 1.970g K16 + 0.263g K12 + 0.250g E5 + 0.263g K24
99. 0.250g E4 + 0.263g K12 + 0.173g K16 + 0.250g E5 + 0.263g K2
100. 1.000g El + 1.050g K12 + 1.000g E5 + 0.173g K16 + 1.050g K6 + 1'.050g K7
101. 2.000g E2 + 2.100g K12 + 2.000g E5 + 2.100g K6 + 0.173g K16 + 2.100g K9
102. 2.000g E3 + 2.100g K12 + 2.000g E5 + 2.100g K6 + 2.100g K13 + 0.173g K16
103. 1.000g E4 + 0.173g K16 + l.050g K12 + 1.000g E5 + 1.050g K6 + 1.050g K1
104. 2.000g El + 2.100g K12 + 0.173g K16 + 2.000g E5 + 2.100g K6 + 2.100g K11
105. 1.000g E2 + 1.050g K12 + 1.000g E5 + 0.173g K16 + 1.050g K6 + 1.050g K14
106. 2.000g E3 + 2.100g K12 + 2.000g E5 + 2.100g K6 + 0.173g K16 + 2.100g K24
107. 2.000g E4 + 2.100g K12 + 2.000g E5 + 2.100g K6 + 2.100g K2 + 0.173g K16
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108. 0.200g El + 0.173g K16 + 0.210g K12 + 0.200g E5 + 0.210g K7 + 0.210g K9
109. 1.000g E2 + 1.050g K12 + 0.173g K16 + 1.000g E5 + 1.050g K8 + 1.050g K13
110. 2.000g E3 + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.100g K7 + 2.100g Ki
111. 0.200g E4 + 0.210g K12 + 0.200g E5 + 0.210g K21 + 0.173g K16 + 0.210g K11
112. 1.000g El + 1.050g K12 + 1.000g E5 + 1.050g K8 + 1.050g K14 + 0.173g K16
113. 2.000g E2 + 0.173g K16 + 2.100g K12 + 2.000g E5 + 2.100g K7 + 2.100g K24
114. 1.000g E3 + 1.050g K12 + 0.173g K16 + 1.000g E5 + 1.050g K7 + 1.050g K2
115. 2.000g E4 + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.100g K9 + 2.100g K13
116. 0.200g El + 0.210g K12 + 0.200g E5 + 0.210g K9 + 0.173g K16 + 0.210g Kl
117. 0.200g E2 + 0.210g K12 + 0.200g E5 + 0.210g K9 + 0.210g K11 + 0.173g Kl6
118. 0.200g E3 + 0.173g K16 + 0.210g K12 + 0.200g E5 + 0.210g K9 + 0.210g K14
119. 2.000g E4 + 2.100g K12 + 0.173g K16 + 2.000g E5 + 2.100g K9 + 2.100g K24
120. 2.000g El + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.100g K9 + 2.100g K2
121. 2.000g E2 + 2.100g K12 + 2.000g E5 + 2.100g K13 + 0.173g K16 + 2.100g K1
122. 2.000g E3 + 2.100g K12 + 2.000g E5 + 2.100g K13 + 2.100g K11 + 0.173g K16
123. 1.000g E4 + 0.173g K16 + 1.050g K12 + 1.000g E5 + 1.050g K13 + 1.050g K14
124. 2.000g El + 2.100g K12 + 0.173g K16 + 2.000g E5 + 2. l00g K13 + 2.100g
K24
125. 0.200g E2 + 0.210g K12 + 0.200g E5 + 0.173g K16 + 0.210g K13 + 0.210g K2
126. 0.200g E3 + 0.210g K12 + 0.200g E5 + 0.210g K1 + 0.173g K16 + 0.210g K11
127. 1.000g E4 + 1.050g K12 + 1.000g E5 + l.050g K1 + 1.050g K14 + 0.173g K16
128. 0.200g E1 + 0.173g K16 + 0.210g K12 + 0.200g E5 + 0.210g K1 + 0.210g K24
129. 2.000g E2 + 2.100g K12 + 0.173g K16 + 2.000g E5 + 2.100g K1 + 2.100g K2
130. 2.000g E3 + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.IOOg K11 + 2.100g K14
131. 2.000g E4 + 2.100g K12 + 2.000g E5 + 2.100g K11 + 0.173g K16 + 2.100g K24
132. 0.200gE1 +0.210gK12+0.200gE5+0.210gK11 + 0.210g K2 + 0.173g K16
133. 0.200g E2 + 0.173g K16 + 0.210g K12 + 0.200g E5 + 0.210g K14 + 0.210g K24
134. 0.200g E3 + 0.210g K12 + 0.173g K16 + 0.200g E5 + 0.210g K14 + 0.210g K2
135. 2.000g E4 + 2.100g K12 + 2.000g E5 + 0.173g K16 + 2.100g K24 + 2.100g K2
136. 1.250g El + 1.313g K12 + 1.250g E7 + 1.313g K6 + 0.173g K16
137. 1.250g E2 + 0.173g K16 + 1.313g K12 + 1.250g E7 + 1.313g K7
138. 0.250g E3 + 0.263g K12 + 0.173g K16 + 0.250g E7 + 0.263g K9
139. 1.250g E4 + 1.313g K12 + 1.250g E7 + 0.173g K16 + 1.313g K13
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140. 2.500g El + 2.625g K12 + 2.500g E7 + 2.625g K4 + 0.173g K16
141. 2.500g E2 + 0.173g K16 + 2.625g K12 + 2.500g E7 + 2.625g Kl 1
142. 1.250g E3 + 1.313g K12 + 0.173g K16 + 1.250g E7 + 1.313g K14
143. 1.250g E4 + 1.313g K12 + 1.250g E7 + 0.173g K16 + 1.313g K24
144. 1.250g E1 + 1.313g K12 + 1.250g E7 + 1.313g K2 + 0.173g K16
145. 1.000g E2 + 0.173g K16 + 1.050g K12 + 1.000g E7 + 1.050g K6 + 1.050g K7
146. 1.000g E3 + 1.050g K12 + 0.173g K16 + 1.000g E7 + 1.050g K6 + 1.050g K9
147. 1.000g E4 + 1.050g K12 + 1.000g E7 + 0.173g K16 + 1.050g K6 + 1.050g K13
148. 2.000g El + 2.100g K12 + 2.000g E7 + 2.100g K6 + 0.173g K16 + 2.100g K1
149. 1.000g E2 + 1.050g K12 + 1.000g E7 + 1.050g K6 + 1.050g K11 + 0.173g K16
150. 2.000g E3 + 0.173g K16 + 2.100g K12 + 2.000g E7 + 2.100g K6 + 2.100g K14
151. 0.200g E4 + 0.210g K12 + 0.173g K16 + 0.200g E7 + 0.210g K6 + 0.210g K24
152. 0.200g E1 + 0.210g K12 + 0.200g E7 + 0.173g K16 + 0.210g K6 + 0.210g K2
153. 0.200g E2 + 0.210g K12 + 0.200g E7 + 0.210g K7 + 0.173g K16 + 0.210g K9
154. 0.200g E3 + 0.210g K12 + 0.200g E7 + 0.210g K7 + 0.210g K13 + 0.173g K16
155. 1.000g E4 + 0.173g K16 + 1.050g K12 + 1.000g E7 + 1.050g K7 + 1.050g K1
156. 0.200gE1 +0.210gK12+0.173gK16+0.200gE7+0.210gK7+0.210gK11
157. 0.200g E2 + 0.210g K12 + 0.200g E7 + 0.173g K16 + 0.210g K8 + 0.210g K14
158. 2.000g E3 + 2.100g K12 + 2.000g E7 + 2.100g K7 + 0.173g K16 + 2.100g K24
159. 2.000g E4 + 2.100g K12 + 2.000g E7 + 2.100g K7 + 2.100g K2 + 0.173g K16
160. 0.200gE1 + 0.173g K16 + 0.210g K12 + 0.200g E7 + 0.210g K9 + 0.210g K13
161. 2.000g E2 + 2.100g K12 + 0.173g K16 + 2.000g E7 + 2.100g K9 + 2.100g K1
162. 1.000g E3 + 1.050g K12 + 1.000g E7 + 0.173g K16 + 1.050g K9 + 1.050g K11
163. 0.200gE4+0.210gK12+0.200gE7+0.210gK9+0.173gK16+0.210gK14
164. 2.000g E1 + 2.100g K12 + 2.000g E7 + 2.100g K9 + 2.100g K24 + 0.173g K16
165. 2.000g E2 + 0.173g K16 + 2.100g K12 + 2.000g E7 + 2.100g K9 + 2.100g K2
166. 2.000g E3 + 2.100g K12 + 0.173g K16 + 2.000g E7 + 2.100g K13 + 2.100g K1
167. 1.000g E4 + 1.050g K12 + 1.000g E7 + 0.376g K16 + 1.050g K13 + 1.050g K11
168. 1.000g El + 1.050g K12 + 1.000g E7 + 1.050g K13 + 0.376g K16 + 1.050g K14
169. 2.000g E2 + 2.100g K12 + 2.000g E7 + 2.100g K13 + 2.100g K24 + 0.376g K16
170. 2.000g E3 + 0.376g K16 + 2.100g K12 + 2.000g E7 + 2.100g K13 + 2.100g K2
171. 0.200gE4+0.210gK12+0.376gK16+0.200gE7+0.210gK1+0.210gK11
CA 02646867 2008-12-16
W245FQ/JC 57
172. 2.000g El + 2.100g K12 + 2.000g E7 + 0.376g K16 + 2.100g K1 + 2.100g K14
173. 1.000g E2 + 1.050g K12 + 1.000g E7 + 1.050g K1 + 0.376g K16 + 1.050g K24
174. 1.000g E3 + 1.050g K12 + 1.000g E7 + 1.050g K1 + 1.050g K2 + 0.376g K16
175. 0.200g E4 + 0.376g K16 + 0.210g K12 + 0.200g E7 + 0.210g K11 + 0.210g K14
176. 1.000g E1 + 1.050g K12 + 0.376g K16 + 1.000g E7 + 1.050g K11 + 1.050g K24
177. 0.200gE2+0.210gK12+0.200gE7+0.376gK16+0.210gK11 +0.210gK2
178. 1.000g E3 + 1.050g K12 + 1.000g E7 + 1.050g K14 + 0.376g K16 + 1.050g K24
179. 1.000g E4 + 1.050g K12 + 1.000g E7 + 1.050g K14 + 1.050g K2 + 0.376g K16
180. 0.200g El + 0.376g K16 + 0.210g K12 + 0.200g E7 + 0.210g K24 + 0.210g K2
181. 2.500g El + 2.625g K12 + 0.376g K16
182. 1.667g E3 + 0.376g K16 + 1.750g K12 + 1.750g K6
183. 3.333g E4 + 3.500g K12 + 0.376g K16 + 3.500g K7 + 0.110g K23
184. 1.667g El + 1.750g K12 + 1.750g K9 + 0.376g K16
185. 0.333g E2 + 0.376g K16 + 0.350g K12 + 0.350g K13
186. 1.667g E3 + 1.750g K12 + 0.376g K16 + 1.750g Kl
187. 0.333g E4 + 0.350g K12 + 0.350g Kl 1+ 0.376g K16
188. 3.333g El + 0.376g K16 + 3.500g K12 + 3.500g K14
189. 0.333g E2 + 0.350g K12 + 0.376g K16 + 0.350g K24
190. 0.333g E3 + 0.350g K12 + 0.350g K2 + 0.376g K16
191. 2.500g E4 + 0.376g K16 + 2.625g K12 + 2.625g K6 + 2.625g K7
192. 1.250gE1 + 1.313g K12 + 0.376g K16 + 1.313gK6+ 1.313g K9
193. 2.500g E2 + 2.625g K12 + 2.625g K6 + 0.376g K16 + 2.625g K13
194. 2.500g E3 + 2.625g K12 + 2.625g K6 + 2.625g K1 + 0.376g K16
195. 0.250g E4 + 0.376g K16 + 0.263g K12 + 0.263g K6 + 0.263g K11
196. 0.250g El + 0.263g K12 + 0.376g K16 + 0.263g K6 + 0.263g K14
197. 1.250gE2+ 1.313gK12+ 1.313g K6 + 0.376g K16 + 1.313gK24
198. 1.250g E3 + 1.313g K12 + 1.313g K6 + 1.313g K2 + 0.376g K16
199. 2.500g E4 + 0.376g K16 + 2.625g K12 + 2.625g K7 + 2.625g K9
200. 1.250g El + 1.313g K12 + 0.376g K16 + 1.313g K7 + 1.313g K13
201. 0.250g E2 + 0.263g K12 + 0.263g K7 + 0.376g K16 + 0.263g KI
202. 0.250g E3 + 0.263g K12 + 0.263g K7 + 0.263g K11 + 0.376g K16
203. 2.500g E4 + 0.376g K16 + 2.625g K12 + 2.625g K7 + 2.625g K14
CA 02646867 2008-12-16
W245FQ/JC 58
204. 1.250g E1 + 1.313g K12 + 0.376g K16 + 1.313g K7 + 1.313g K24
205. 1.250g E2 + 1.313g K12 + 1.313g K7 + 0.376g K16 + 1.313g K2
206. 2.500g E3 + 2.625g K12 + 2.625g K9 + 2.625g K13 + 0.376g K16
207. 1.250g E4 + 0.376g K16 + 1.313g K12 + 1.313g K9 + 1.313g K1
208. 0.250g El + 0.263g K12 + 0.376g K16 + 0.263g K9 + 0.263g K11
209. 1.250g E2 + 1.313g K12 + 1.313g K9 + 0.376g K16 + 1.313g K14
210. 1.250gE3+ 1.313gK12+ 1.313gK9+ 1.313g K24 + 0.376g K16
211. 0.250g E4 + 0.376g K16 + 0.263g K12 + 0.263g K9 + 0.263g K2
212. 0.250g El + 0.263g K12 + 0.376g K16 + 0.263g K13 + 0.263g KI
213. 1.250g E2 + 1.313g K12 + 1.313g K13 + 0.376g K16 + 1.313g K11
214. 1.250g E3 + 1.313g K12 + 1.313g K13 + 1.313g K14 + 0.376g K16
215. 1.250g E4 + 0.376g K16 + 1.313g K12 + 1.313g K13 + 1.313g K24
216. 2.500g El + 2.625g K12 + 0.376g K16 + 2.625g K13 + 2.625g K2
217. 2.500g E2 + 2.625g K12 + 2.625g K1 + 0.376g K16 + 2.625g Kl 1
218. 2.500g E3 + 2.625g K12 + 2.625g K1 + 2.625g K14 + 0.376g K16
219. 2.500g E4 + 0.376g K16 + 2.625g K12 + 2.625g Kl + 2.625g K24
220. 2.500g El + 2.625g K12 + 0.376g K16 + 2.625g Kl + 2.625g K2
221. 1.250g E2 + 1.313g K12 + 1.313g K17 + 0.376g K16 + 1.313g K14
222. 1.250g E3 + 1.313g K12 + 1.313g K18 + 1.313g K24 + 0.376g K16
223. 1.250gE4+0.376gK16+1.313gK12+1.313gK11+1.313gK2
224. 0.250g El + 0.263g K12 + 0.376g K16 + 0.263g K14 + 0.263g K24
225. 2.500g E2 + 2.625g K12 + 2.625g K14 + 0.376g K16 + 2.625g K2
226. 1.250g E3 + 1.313g K12 + 1.313g K24 + 1.313g K2 + 0.376g K16
227. 2.000g E4 + 0.376g K16 + 2.100g K12 + 2.100g K6 + 2.100g K8 + 2.100g K9
228. 2.000g E1 + 2.100g K12 + 0.376g K16 + 2.100g K6 + 2.100g K21 + 2.100g K13
229. 1.000g E2 + 1.050g K12 + 1.050g K6 + 0.376g K16 + 1.050g K7 + 1.050g Ki
230. 1.000g E3 + 1.050g K12 + l.050g K6 + 1.050g K8 + 0.376g K16 + l.050g Kl 1
231. 1.000g E4 + 1.050g K12 + 1.050g K6 + 1.050g K7 + 1.050g K14 + 0.376g K16
232. 2.000g E1 + 0.376g K16 + 2.100g K12 + 2.100g K6 + 2.100g K7 + 2.100g K24
233. 0.200gE2+0.210gK12+0.376gK16+0.210gK6+0.2lOgK7+0.210gK2
234. 0.200gE3+0.210gK12+0.210gK6+0.376gK16+0.210gK9+0.210gK13
235. 1.000g E4 + 1.050g K12 + l.050g K6 + 1.050g K9 + 1.579g K16 + l.050g K1
CA 02646867 2008-12-16
W245FQ/JC 59
236. 1.000g E1 + 1.050g K12 + 1.050g K6 + 1.050g K9 + 1.050g K11 + 1.579g K16
237. 0.200gE2+ 1.579gK16+0.210gK12+0.210gK6+0.210gK9+0.210gK14
238. 2.000g E3 + 2.100g K12 + 1.579g K16 + 2.100g K6 + 2.100g K9 + 2.100g K24
239. 2.000g E4 + 2.100g K12 + 2. l00g K6 + 1.579g K16 + 2.100g K9 + 2.100g K2
240. 2.000g El + 2.100g K12 + 2.100g K6 + 2.100g K13 + 1.579g K16 + 2.100g Kl
241. 0.200g E2 + 0.210g K12 + 0.210g K6 + 0.210g K13 + 0.210g K11 + 1.579g K16
242. 0.200g E3 + 1.579g K16 + 0.210g K12 + 0.210g K6 + 0.210g K13 + 0.210g K14
243. 1.000g E4 + 1.050g K12 + 1.579g K16 + 1.050g K6 + 1.050g K13 + 1.050g K24
244. 0.200gE1 + 0.210g K12 + 0.210g K6 + 1.579g K16 + 0.210g K13 +0.210gK2
245. 0.200g E2 + 0.210g K12 + 0.210g K6 + 0.210g Kl + 1.579g K16 + 0.210g K11
246. 2.000g E3 + 2.100g K12 + 2.100g K6 + 2.100g K1 + 2.100g K14 + 1.579g K16
247. 0.200g E4 + 1.579g K16 + 0.210g K12 + 0.210g K6 + 0.210g Kl + 0.210g K24
248. 1.000g E1 + 1.050g K12 + 1.579g K16 + 1.050g K6 + 1.050g K1 + 1.050g K2
249. 2.000g E2 + 2.l00g K12 + 2.l00g K6 + 1.579g K16 + 2.100g K11 + 2.l00g K14
250. 1.000g E3 + 1.050g K12 + 1.050g K6 + 1.050g Kl 1+ 1.579g K16 + 1.050g K24
251. 0.200gE4+0.210gK12+0.210gK6+0.210gK11+0.210gK2+1.579gK16
252. 0.200gE1 + 1.579g K16 + 0.210g K12 + 0.210g K6 + 0.210g K14 + 0.210g K24
253. 1.000g E2 + 1.050g K12 + 1.579g K16 + 1.050g K6 + 1.050g K14 + 1.050g K2
254. 2.000g E3 + 2.100g K12 + 2.100g K6 + 1.579g K16 + 2.100g K24 + 2.100g K2
255. 1.000g E4 + 1.050g K12 + 1.050g K7 + 1.050g K9 + 1.579g K16 + 1.050g K13
256. 0.200g E1 + 0.210g K12 + 0.210g K7 + 0.210g K9 + 0.210g K1 + 1.579g K16
257. 2.000g E2 + 1.579g K16 + 2.100g K12 + 2.100g K7 + 2.100g K9 + 2.100g K11
258. 0.200g E3 + 0.210g K12 + 1.579g K16 + 0.210g K7 + 0.210g K9 + 0.210g K14
259. 2.000g E4 + 2.100g K12 + 2.100g K7 + 1.579g K16 + 2.100g K9 + 2.100g K24
260. 2.000g E1 + 2.100g K12 + 2.100g K8 + 2.100g K9 + 1.579g K16 + 2.100g K2
261. 1.000g E2 + 1.050g K12 + 1.050g K7 + 1.050g K13 + 1.050g K1 + 1.579g K16
262. 0.200g E3 + 1.579g K16 + 0.210g K12 + 0.210g K7 + 0.210g K13 + 0.210g K11
263. 2.000g E4 + 2.100g K12 + 1.579g K16 + 2. l00g K7 + 2.100g K13 + 2.100g
K14
264. 2.000g El + 2.l00g K12 + 2.l00g K7 + 1.579g K16 + 2.100g K13 + 2.100g K24
265. 1.000g E2 + 1.050g K12 + 1.050g K7 + 1.050g K13 + 1.579g K16 + 1.050g K2
266. 2.000g E3 + 2.l00g K12 + 2.l00g K7 + 2.l00g K1 + 2.100g K11 + 1.579g K16
267. 1.000g E4 + 1.579g K16 + 1.050g K12 + 1.050g K7 + 1.050g Kl + 1.050g K14
CA 02646867 2008-12-16
W245FQ/JC 60
268. 1.000g E1 + 1.050g K12 + 1.579g K16 + 1.050g K7 + 1.050g Kl + 1.050g K24
269. 0.200g E2 + 0.210g K12 + 0.210g K7 + 1.579g K16 + 0.210g K1 + 0.210g K2
270. 1.000g E3 + l.050g K12 + l.050g K7 + 1.050g K11 + 1.579g K16 + 1.050g K14
271. 2.000g E4 + 2.1OOg K12 + 2.1OOg K21 + 2.100g Kl l+ 2.1OOg K24 + 1.579g
K16
272. 2.000g El + 1.579g K16 + 2.100g K12 + 2.100g K7 + 2.100g Kl 1+ 2.100g K2
273. 1.000g E2 + 1.050g K12 + 1.579g K16 + 1.050g K8 + 1.050g K14 + 1.050g K24
274. 1.000g E3 + 1.050g K12 + 1.050g K7 + 1.579g K16 + 1.050g K14 + 1.050g K2
275. 0.200g E4 + 0.210g K12 + 0.210g K8 + 0.210g K24 + 1.579g K16 + 0.210g K2
276. 1.000g El + 1.050g K12 + 1.050g K9 + 1.050g K13 + 1.050g Kl + 1.579g K16
277. 1.000g E2 + 1.579g K16 + 1.050g K12 + 1.050g K9 + 1.050g K13 + 1.050g Kl
1
278. 0.200g E3 + 0.210g K12 + 1.579g K16 + 0.210g K9 + 0.210g K13 + 0.210g K14
279. 1.000g E4 + 1.050g K12 + 1.050g K9 + 1.579g K16 + 1.050g K13 + 1.050g K24
280. 0.200g E1 + 0.210g K12 + 0.210g K9 + 0.210g K13 + 1.579g K16 + 0.210g K2
281. 0.200g E2 + 0.210g K12 + 0.210g K9 + 0.210g K1 + 0.210g K11 + 1.579g K16
282. 0.200g E3 + 1.579g K16 + 0.210g K12 + 0.210g K9 + 0.210g K1 + 0.210g K14
283. 0.200g E4 + 0.210g K12 + 1.579g K16 + 0.210g K9 + 0.210g K1 + 0.210g K24
284. 2.000g El + 2.100g K12 + 2.100g K9 + 1.579g K16 + 2.100g K1 + 2.100g K2
285. 0.200g E2 + 0.210g K12 + 0.210g K9 + 0.210g K11 + 1.579g K16 + 0.210g K14
286. 2.000g E3 + 2.100g K12 + 2.100g K9 + 2.100g K11 + 2.100g K24 + 1.579g K16
287. 2.000g E4 + 1.579g K16 + 2.100g K12 + 2.100g K9 + 2.100g K11 + 2.100g K2
288. 0.200g E1 + 0.210g K12 + 1.579g K16 + 0.210g K9 + 0.210g K14 + 0.210g K24
289. 0.200g E2 + 0.210g K12 + 0.210g K9 + 1.579g K16 + 0.210g K14 + 0.210g K2
290. 2.000g E3 + 2.100g K12 + 2.100g K9 + 2.100g K24 + 1.579g K16 + 2.100g K2
291. 2.000g E4 + 2.100g K12 + 2.100g K13 + 2.100g K1 + 2.100g K11 + 1.579g K16
292. 2.000gE1 + 1.579gK16+2.100gK12+2.100gK13+2.100gK1 +2.100gK14
293. 0.200g E2 + 0.210g K12 + 1.579g K16 + 0.210g K13 + 0.210g K1 + 0.210g K24
294. 2.000g E3 + 2.100g K12 + 2.100g K13 + 1.579g K16 + 2.100g Kl + 2.100g K2
295. 2.000g E4 + 2.100g K12 + 2.100g K13 + 2.100g K11 + 1.579g K16 + 2.100g
K14
296. 0.200g El + 0.210g K12 + 0.210g K13 + 0.210g K11 + 0.210g K24 + 1.579g
K16
297. 1.000g E2 + 1.579g K16 + 1.050g K12 + 1.050g K13 + 1.050g K11 + 1.050g K2
298. 0.200g E3 + 0.210g K12 + 1.579g K16 + 0.210g K13 + 0.210g K14 + 0.210g
K24
299. 0.200gE4+0.210gK12+0.210gK13+1.579gK16+0.210gK14+0.210gK2
CA 02646867 2008-12-16
W245FQ/JC 61
300. 2.000g E1 + 2.100g K12 + 2.100g K13 + 2.100g K24 + 1.579g K16 + 2.100g K2
301. 0.200gE2+0.210gK12+0.2lOgK1 +0.210gK11 +0.210gK14+ 1.579gK16
302. 0.200g E3 + 1.782g K16 + 0.210g K12 + 0.210g K1 + 0.210g K11 + 0.210g K24
303. 0.200g E4 + 0.210g K12 + 1.782g K16 + 0.210g K1 + 0.210g K11 + 0.210g K2
304. 2.000g E1 + 2.100g K12 + 2.100g K1 + 1.782g K16 + 2.100g K14 + 2.100g K24
305. 1.000g E2 + 1.050g K12 + 1.050g K1 + 1.050g K14 + 1.782g K16 + 1.050g K2
306. 1.000g E3 + 1.050g K12 + 1.050g Kl + 1.050g K24 + 1.050g K2 + 1.782g K16
307. 1.000g E4 + 1.782g K16 + 1.050g K12 + 1.050g K11 + 1.050g K14 + 1.050g
K24
308. 2.000g E1 + 2.100g K12 + 1.782g K16 + 2.l00g K11 + 2.100g K14 + 2.100g K2
309. 1.000g E2 + 1.050g K12 + 1.050g K11 + 1.782g K16 + 1.050g K24 + 1.050g K2
310. 1.000g E3 + 1.050g K12 + 1.050g K14 + 1.050g K24 + 1.782g K16 + 1.050g K2
311. 2.500g E4 + 2.625g K6 + 2.500g E8 + 2.625g K12 + 1.782g K16
312. 2.500g El + 1.782g K16 + 2.625g K6 + 2.500g E8 + 2.625g K7
313. 1.250g E2 + 1.313g K6 + 1.782g K16 + 1.250g E8 + 1.313g K9
314. 0.250g E3 + 0.263g K6 + 0.250g E8 + 1.782g K16 + 0.263g K13
315. 1.250g E4 + 1.313g K6 + 1.250g E8 + 1.313g K1 + 1.782g K16
316. 1.250g E1 + 1.782g K16 + 1.313g K6 + 1.250g E8 + 1.313g K11
317. 2.500g E2 + 2.625g K6 + 1.782g K16 + 2.500g E8 + 2.625g K14
318. 1.250g E3 + 1.313g K6 + 1.250g E8 + 1.782g K16 + 1.313g K24
319. 0.250g E4 + 0.263g K6 + 0.250g E8 + 0.263g K2 + 1.782g K16
320. 0.200g El + 1.782g K16 + 0.210g K6 + 0.200g E8 + 0.210g K12 + 0.210g K7
321. 1.000g E2 + 1.050g K6 + 1.782g K16 + 1.000g E8 + 1.050g K12 + 1.050g K9
322. 1.000g E3 + 1.050g K6 + 1.000g E8 + 1.782g K16 + 1.050g K12 + 1.050g K13
323. 1.000g E4 + 1.050g K6 + 1.000g E8 + 1.050g K12 + 1.782g K16 + 1.050g K1
324. 0.200g El + 0.210g K6 + 0.200g E8 + 0.210g K12 + 0.210g Kl 1+ 1.782g K16
325. 2.000g E2 + 1.782g K16 + 2.100g K6 + 2.000g E8 + 2.100g K12 + 2.100g K14
326. 1.000g E3 + 1.050g K6 + 1.782g K16 + 1.000g E8 + 1.050g K12 + 1.050g K24
327. 0.200g E4 + 0.210g K6 + 0.200g E8 + 1.782g K16 + 0.210g K12 + 0.210g K2
328. 1.000g El + 1.050g K6 + 1.000g E8 + 1.050g K7 + 1.782g K16 + 1.050g K9
329. 2.000g E2 + 2.100g K6 + 2.000g E8 + 2.100g K7 + 2.100g K13 + 1.782g K16
330. 1.000g E3 + 1.782g K16 + 1.050g K6 + 1.000g E8 + 1.050g K7 + 1.050g Kl
331. 0.200g E4 + 0.210g K6 + 1.782g K16 + 0.200g E8 + 0.210g K7 + 0.210g KI I
CA 02646867 2008-12-16
W245FQ/JC 62
332. 1.000g El + 1.050g K6 + 1.000g E8 + 1.782g K16 + 1.050g K7 + 1.050g K14
333. 1.000g E2 + 1.050g K6 + 1.000g E8 + 1.050g K7 + 1.782g K16 + 1.050g K24
334. 0.200g E3 + 0.210g K6 + 0.200g E8 + 0.210g K7 + 0.210g K2 + 1.782g K16
335. 1.000g E4 + 1.782g K16 + 1.050g K6 + 1.000g E8 + 1.050g K9 + 1.050g K13
336. 0.200g E1 + 0.210g K6 + 1.782g K16 + 0.200g E8 + 0.210g K9 + 0.210g K1
337. 1.000g E2 + 1.050g K6 + 1.000g E8 + 1.782g K16 + 1.050g K9 + 1.050g Kl 1
338. 2.000g E3 + 2.100g K6 + 2.000g E8 + 2.100g K9 + 1.782g K16 + 2.100g K14
339. 2.000g E4 + 2.100g K6 + 2.000g E8 + 2.100g K9 + 2.100g K24 + 1.782g K16
340. 2.000g E l+ 1.782g K16 + 2.100g K6 + 2.000g E8 + 2.100g K9 + 2.100g K2
341. 0.200g E2 + 0.210g K6 + 1.782g K16 + 0.200g E8 + 0.210g K13 + 0.210g K1
342. 2.000g E3 + 2.100g K6 + 2.000g E8 + 1.782g K16 + 2.100g K13 + 2.100g K11
343. 1.000g E4 + 1.050g K6 + 1.000g E8 + 1.050g K13 + 1.782g K16 + 1.050g K14
344. 2.000g El + 2.100g K6 + 2.000g E8 + 2.100g K13 + 2.100g K24 + 1.782g K16
345. 0.200g E2 + 1.782g K16 + 0.210g K6 + 0.200g E8 + 0.210g K13 + 0.210g K2
346. 2.000g E3 + 2.100g K6 + 1.782g K16 + 2.000g E8 + 2.100g K1 + 2.100g K11
347. 0.200g E4 + 0.210g K6 + 0.200g E8 + 1.782g K16 + 0.210g K1 + 0.210g K14
348. 2.000g El + 2.100g K6 + 2.000g E8 + 2.100g K1 + 1.782g K16 + 2.100g K24
349. 2.000g E2 + 2.100g K6 + 2.000g E8 + 2.100g K1 + 2.100g K2 + 1.782g K16
350. 2.000g E3 + 1.782g K16 + 2.100g K6 + 2.000g E8 + 2.100g K11 + 2.100g K14
351. 1.000g E4 + 1.050g K6 + 1.782g K16 + 1.000g E8 + 1.050g K11 + 1.050g K24
352. 1.000g El + 1.050g K6 + 1.000g E8 + 1.782g K16 + 1.050g K11 + 1.050g K2
353. 1.000g E2 + 1.050g K6 + 1.000g E8 + 1.050g K14 + 1.782g K16 + 1.050g K24
354. 2.000g E3 + 2.100g K6 + 2.000g E8 + 2.100g K14 + 2.100g K2 + 1.782g K16
355. 2.000g E4 + 1.782g K16 + 2.100g K6 + 2.000g E8 + 2.100g K24 + 2.100g K2
356. 2.500g El + 2.625g K6 + 1.782g K16 + 2.500g E6 + 2.625g K12
357. 2.500g E2 + 2.625g K6 + 2.500g E6 + 1.782g K16 + 2.625g K7
358. 0.250g E3 + 0.263g K6 + 0.250g E6 + 0.263g K9 + 1.782g K16
359. 1.250gE4+ 1.782gK16+ 1.313gK6+ 1.250gE6+ 1.313gK13
360. 0.250g El + 0.263g K6 + 1.782g K16 + 0.250g E6 + 0.263g K1
361. 0.250g E2 + 0.263g K6 + 0.250g E6 + 1.782g K16 + 0.263g Kl 1
362. 1.250g E3 + 1.313g K6 + 1.250g E6 + 1.313g K14 + 1.782g K16
363. 1.250g E4 + 1.782g K16 + 1.313g K6 + 1.250g E6 + 1.313g K24
CA 02646867 2008-12-16
W245FQ/JC 63
364. 2.500g El + 2.625g K6 + 1.782g K16 + 2.500g E6 + 2.625g K20
365. 0.200g E2 + 0.210g K6 + 0.200g E6 + 1.782g K16 + 0.210g K12 + 0.210g K7
366. 2.000g E3 + 2.100g K6 + 2.000g E6 + 2.100g K12 + 1.782g K16 + 2.100g K9
367. 1.000g E4 + 1.050g K6 + 1.000g E6 + 1.050g K12 + 1.050g K13 + 1.782g K16
368. 1.000g El + 1.782g K16 + 1.050g K6 + 1.000g E6 + 1.050g K12 + 1.050g K1
369. 0.200g E2 + 0.210g K6 + 1.782g K16 + 0.200g E6 + 0.210g K12 + 0.210g K11
370. 0.200g E3 + 0.210g K6 + 0.200g E6 + 1.985g K16 + 0.210g K12 + 0.210g K14
371. 0.200g E4 + 0.210g K6 + 0.200g E6 + 0.210g K12 + 1.985g K16 + 0.210g K24
372. 0.200g El + 0.210g K6 + 0.200g E6 + 0.210g K12 + 0.210g K2 + 1.985g K16
373. 2.000g E2 + 1.985g K16 + 2.100g K6 + 2.000g E6 + 2.100g K7 + 2.100g K9
374. 1.000g E3 + 1.050g K6 + 1.985g K16 + 1.000g E6 + 1.050g K7 + 1.050g K13
375. 1.000g E4 + 1.050g K6 + 1.000g E6 + 1.985g K16 + 1.050g K7 + 1.050g K1
376. 1.000g El + 1.050g K6 + 1.000g E6 + 1.050g K7 + 1.985g K16 + 1.050g K11
377. 2.000g E2 + 2.100g K6 + 2.000g E6 + 2.100g K7 + 2.100g K14 + 1.985g K16
378. 1.000g E3 + 1.985g K16 + 1.050g K6 + 1.000g E6 + 1.050g K7 + 1.050g K24
379. 1.000g E4 + 1.050g K6 + 1.985g K16 + 1.000g E6 + 1.050g K21 + 1.050g K2
380. 0.200g El + 0.210g K6 + 0.200g E6 + 1.985g K16 + 0.210g K9 + 0.210g K13
381. 1.000g E2 + 1.050g K6 + 1.000g E6 + 1.050g K9 + 1.985g K16 + 1.050g K1
382. 1.000g E3 + 1.050g K6 + 1.000g E6 + 1.050g K9 + 1.050g K11 + 1.985g K16
383. 1.000g E4 + 1.985g K16 + 1.050g K6 + 1.000g E6 + 1.050g K9 + 1.050g K14
384. 2.000g El + 2.100g K6 + 1.985g K16 + 2.000g E6 + 2.100g K9 + 2.100g K24
385. 1.000g E2 + 1.050g K6 + 1.000g E6 + 1.985g K16 + 1.050g K9 + 1.050g K2
386. 2.000g E3 + 2.100g K6 + 2.000g E6 + 2.100g K13 + 1.985g K16 + 2.100g K1
387. 1.000g E4 + 1.050g K6 + 1.000g E6 + 1.050g K13 + 1.050g K11 + 1.985g K16
388. 2.000g El + 1.985g K16 + 2.l00g K6 + 2.000g E6 + 2.100g K13 + 2.100g K14
389. 2.000g E2 + 2. l00g K6 + 1.985g K16 + 2.000g E6 + 2.100g K13 + 2.100g K24
390. 1.000g E3 + 1.050g K6 + 1.000g E6 + 1.985g K16 + 1.050g K13 + 1.050g K2
391. 2.000g E4 + 2.100g K6 + 2.000g E6 + 2.100g K1 + 1.985g K16 + 2.100g K11
392. 1.000g El + 1.050g K6 + 1.000g E6 + 1.050g K4 + 1.050g K14 + 1.985g K16
393. 0.200g E2 + 1.985g K16 + 0.210g K6 + 0.200g E6 + 0.210g Kl + 0.210g K24
394. 1.000g E3 + 1.050g K6 + 1.985g K16 + 1.000g E6 + 1.050g K1 + 1.050g K2
395. 1.000g E4 + 1.050g K6 + 1.000g E6 + 1.985g K16 + 1.050g K11 + 1.050g K14
CA 02646867 2008-12-16
W245FQ/JC 64
396. 1.000g E1 + l.050g K6 + 1.000g E6 + 1.050g Kl 1+ 1.985g K16 + 1.050g K24
397. 0.200g E2 + 0.210g K6 + 0.200g E6 + 0.210g K11 + 0.210g K2 + 1.985g K16
398. 2.000g E3 + 1.985g K16 + 2.100g K6 + 2.000g E6 + 2.100g K14 + 2.100g K24
399. 2.000g E4 + 2.100g K6 + 1.985g K16 + 2.000g E6 + 2.100g K14 + 2.100g K2
400. 0.200g El + 0.210g K6 + 0.200g E6 + 1.985g K16 + 0.210g K24 + 0.210g K2
401. 2.500g E2 + 2.625g K6 + 2.500g E5 + 2.625g K12 + 1.985g K16
402. 1.250g E3 + 1.985g K16 + 1.313g K6 + 1.250g E5 + 1.313g K7
403. 0.250g E4 + 0.263g K6 + 1.985g K16 + 0.250g E5 + 0.263g K9
404. 0.250g El + 0.263g K6 + 0.250g E5 + 1.985g K16 + 0.263g K13
405. 0.250g E2 + 0.263g K6 + 0.250g E5 + 0.263g K1 + 1.985g K16
406. 2.500g E3 + 1.985g K16 + 2.625g K6 + 2.500g E5 + 2.625g Kl 1
407. 1.250g E4 + 1.313g K6 + 1.985g K16 + 1.250g E5 + 1.313g K14
408. 0.250g El + 0.263g K6 + 0.250g E5 + 1.985g K16 + 0.263g K24
409. 0.250g E2 + 0.263g K6 + 0.250g E5 + 0.263g K2 + 1.985g K16
410. 1.000g E3 + 1.985g K16 + 1.050g K6 + 1.000g E5 + 1.050g K12 + 1.050g K7
411. 1.000g E4 + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g K12 + 1.050g K9
412. 1.000g E1 + 1.050g K6 + 1.000g E5 + 1.985g K16 + 1.050g K12 + 1.050g K13
413. 2.000g E2 + 2.100g K6 + 2.000g E5 + 2.100g K12 + 1.985g K16 + 2.l00g K1
414. 0.200g E3 + 0.210g K6 + 0.200g E5 + 0.210g K12 + 0.210g K11 + 1.985g K16
415. 1.000g E4 + 1.985g K16 + 1.050g K6 + 1.000g E5 + 1.050g K12 + 1.050g K14
416. 1.000g El + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g K12 + 1.050g K24
417. 1.000g E2 + 1.050g K6 + 1.000g E5 + 1.985g K16 + 1.050g K12 + 1.050g K2
418. 2.000g E3 + 2. l00g K6 + 2.000g E5 + 2. l00g K7 + 1.985g K16 + 2.l00g K9
419. 0.200g E4 + 0.210g K6 + 0.200g E5 + 0.210g K8 + 0.210g K13 + 1.985g K16
420. 2.000g El + 1.985g K16 + 2.l00g K6 + 2.000g E5 + 2.l00g K7 + 2.l00g K1
421. 2.000g E2 + 2.100g K6 + 1.985g K16 + 2.000g E5 + 2.100g K7 + 2.100g K11
422. 2.000g E3 + 2.100g K6 + 2.000g E5 + 1.985g K16 + 2.100g K7 + 2.100g K14
423. 0.200g E4 + 0.210g K6 + 0.200g E5 + 0.210g K7 + 1.985g K16 + 0.210g K24
424. 2.000g E1 + 2.100g K6 + 2.000g E5 + 2.100g K7 + 2.100g K2 + 1.985g K16
425. 1.000g E2 + 1.985g K16 + 1.050g K6 + 1.000g E5 + 1.050g K9 + 1.050g K13
426. 1.000g E3 + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g K9 + 1.050g Kl
427. 1.000g E4 + 1.050g K6 + 1.000g E5 + 1.985g K16 + 1.050g K9 + 1.050g Kl l
CA 02646867 2008-12-16
W245FQ/JC 65
428. 2.000g El + 2.100g K6 + 2.000g E5 + 2.100g K9 + 1.985g K16 + 2.100g K14
429. 2.000g E2 + 2.100g K6 + 2.000g E5 + 2.100g K9 + 2.100g K24 + 1.985g K16
430. 2.000g E3 + 1.985g K16 + 2.100g K6 + 2.000g E5 + 2.100g K9 + 2.100g K2
431. 1.000g E4 + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g K13 + 1.050g K1
432. 1.000g El + 1.050g K6 + 1.000g E5 + 1.985g K16 + 1.050g K13 + 1.050g K11
433. 2.000g E2 + 2. l00g K6 + 2.000g E5 + 2.100g K13 + 1.985g K16 + 2.100g K14
434. 0.200g E3 + 0.210g K6 + 0.200g E5 + 0.210g K13 + 0.210g K24 + 1.985g K16
435. 1.000g E4 + 1.985g K16 + 1.050g K6 + 1.000g E5 + 1.050g K13 + 1.050g K2
436. 1.000g El + 1.050g K6 + 1.985g K16 + 1.000g E5 + 1.050g Kl + 1.050g K11
437. 2.000g E2 + 2.100g K6 + 2.000g E5 + 0.187g K16 + 2.100g K1 + 2.100g K14
438. 2.000g E3 + 2.100g K6 + 2.000g E5 + 2.100g K1 + 0.187g K16 + 2.100g K24
439. 2.000g E4 + 2.100g K6 + 2.000g E5 + 2.100g K1 + 2.100g K2 + 0.187g K16
440. 2.000g El + 0.187g K16 + 2.100g K6 + 2.000g E5 + 2.100g K11 + 2.100g K14
441. 1.000g E2 + 1.050g K6 + 0.187g K16 + 1.000g E5 + 1.050g K11 + 1.050g K24
442. 1.000g E3 + 1.050g K6 + 1.000g E5 + 0.187g K16 + 1.050g K11 + 1.050g K2
443. 2.000g E4 + 2.100g K6 + 2.000g E5 + 2.100g K14 + 0.187g K16 + 2.100g K24
444. 0.200g El + 0.210g K6 + 0.200g E5 + 0.210g K14 + 0.210g K2 + 0.187g K16
445. 0.200g E2 + 0.187g K16 + 0.210g K6 + 0.200g E5 + 0.210g K24 + 0.210g K2
446. 1.250g E3 + 1.313g K6 + 0.187g K16 + 1.250g E7 + 1.313g K12
447. 1.250g E4 + 1.313g K6 + 1.250g E7 + 0.187g K16 + 1.313g K7
448. 2.500g El + 2.625g K6 + 2.500g E7 + 2.625g K9 + 0.187g K16
449. 2.500g E2 + 0.187g K16 + 2.625g K6 + 2.500g E7 + 2.625g K13
450. 2.500g E3 + 2.625g K6 + 0.187g K16 + 2.500g E7 + 2.625g K1
451. 1.250g E4 + 1.313g K6 + 1.250g E7 + 0.187g K16 + 1.313g K11
452. 0.250g El + 0.263g K6 + 0.250g E7 + 0.263g K14 + 0.187g K16
453. 2.500g E2 + 0.187g K16 + 2.625g K6 + 2.500g E7 + 2.625g K24
454. 2.500g E3 + 2.625g K6 + 0.187g K16 + 2.500g E7 + 2.625g K2
455. 0.200g E4 + 0.210g K6 + 0.200g E7 + 0.187g K16 + 0.210g K12 + 0.210g K7
456. 2.000g E1 + 2.100g K6 + 2.000g E7 + 2.100g K12 + 0.187g K16 + 2.100g K9
457. 1.000g E2 + 1.050g K6 + 1.000g E7 + 1.050g K12 + 1.050g K13 + 0.187g K16
458. 1.000g E3 + 0.187g K16 + 1.050g K6 + 1.000g E7 + 1.050g K12 + 1.050g Kl
459. 1.000g E4 + 1.050g K6 + 0.187g K16 + 1.000g E7 + 1.050g K12 + 1.050g Kl 1
CA 02646867 2008-12-16
W245FQ/JC 66
460. 0.200g E1 + 0.210g K6 + 0.200g E7 + 0.187g K16 + 0.210g K12 + 0.210g K14
461. 0.200g E2 + 0.210g K6 + 0.200g E7 + 0.210g K12 + 0.187g K16 + 0.210g K24
462. 2.000g E3 + 2.100g K6 + 2.000g E7 + 2.100g K12 + 2.100g K2 + 0.187g K16
463. 1.000g E4 + 0.187g K16 + 1.050g K6 + 1.000g E7 + 1.050g K7 + 1.050g K9
464. 0.200g El + 0.210g K6 + 0.187g K16 + 0.200g E7 + 0.210g K7 + 0.210g K13
465. 2.000g E2 + 2.100g K6 + 2.000g E7 + 0.187g K16 + 2.100g K7 + 2.100g K1
466. 0.200g E3 + 0.210g K6 + 0.200g E7 + 0.210g K7 + 0.187g K16 + 0.210g K11
467. 1.000g E4 + 1.050g K6 + 1.000g E7 + 1.050g K7 + 1.050g K14 + 0.187g K16
468. 0.200g E1 + 0.187g K16 + 0.210g K6 + 0.200g E7 + 0.210g K8 + 0.210g K24
469. 1.000g E2 + 1.050g K6 + 0.187g K16 + 1.000g E7 + 1.050g K7 + 1.050g K2
470. 0.200g E3 + 0.210g K6 + 0.200g E7 + 0.187g K16 + 0.210g K9 + 0.210g K13
471. 2.000g E4 + 2.100g K6 + 2.000g E7 + 2.100g K9 + 0.187g K16 + 2.100g K1
472. 0.200g E1 + 0.210g K6 + 0.200g E7 + 0.210g K9 + 0.210g K11 + 0.187g K16
473. 0.200g E2 + 0.187g K16 + 0.210g K6 + 0.200g E7 + 0.210g K9 + 0.210g K14
474. 2.000g E3 + 2.100g K6 + 0.187g K16 + 2.000g E7 + 2.100g K9 + 2.100g K24
475. 0.200gE4+0.210gK6+0.200gE7+0.187gK16+0.210gK9+0.210gK2
476. 0.200g El + 0.210g K6 + 0.200g E7 + 0.210g K13 + 0.187g K16 + 0.210g K1
477. 0.200g E2 + 0.210g K6 + 0.200g E7 + 0.210g K13 + 0.210g Kl 1+ 0.187g K16
478. 1.000g E3 + 0.187g K16 + 1.050g K6 + 1.000g E7 + 1.050g K13 + 1.050g K14
479. 1.000g E4 + 1.050g K6 + 0.187g K16 + 1.000g E7 + 1.050g K13 + 1.050g K24
480. 1.000g El + 1.050g K6 + 1.000g E7 + 0.187g K16 + 1.050g K13 + 1.050g K2
481. 2.000g E2 + 2.100g K6 + 2.000g E7 + 2.100g K1 + 0.187g K16 + 2.100g K11
482. 1.000g E3 + 1.050g K6 + 1.000g E7 + 1.050g K4 + 1.050g K14 + 0.187g K16
483. 1.000g E4 + 0.187g K16 + 1.050g K6 + 1.000g E7 + 1.050g Kl + 1.050g K24
484. 0.200g E1 + 0.210g K6 + 0.187g K16 + 0.200g E7 + 0.210g K1 + 0.210g K2
485. 1.000g E2 + 1.050g K6 + 1.000g E7 + 0.187g K16 + 1.050g Kl 1+ 1.050g K14
486. 2.000g E3 + 2.100g K6 + 2.000g E7 + 2.100g K11 + 0.187g K16 + 2.100g K24
487. 1.000g E4 + 1.050g K6 + 1.000g E7 + 1.050g K11 + 1.050g K2 + 0.187g K16
488. 2.000g El + 0.187g K16 + 2.100g K6 + 2.000g E7 + 2.100g K14 + 2.100g K24
489. 1.000g E2 + 1.050g K6 + 0.187g K16 + 1.000g E7 + 1.050g K14 + 1.050g K2
490. 1.000g E3 + 1.050g K6 + 1.000g E7 + 0.187g K16 + 1.050g K24 + 1.050g K2
491. 3.333g E4 + 3.500g K6 + 3.500g K12 + 0.187g K16 + 0.015g K23
CA 02646867 2008-12-16
W245FQ/JC 67
492. 0.250g El + 0.187g K16 + 0.263g K6 + 0.263g K12 + 0.263g K7
493. 2.500g E2 + 2.625g K6 + 0.187g K16 + 2.625g K12 + 2.625g K9
494. 1.250g E3 + 1.313g K6 + 1.313g K12 + 0.187g K16 + 1.313g K13
495. 1.250g E4 + 1.313g K6 + 1.313g K12 + 1.313g K1 + 0.187g K16
496. 1.250g E1 + 0.187g K16 + 1.313g K6 + 1.313g K12 + 1.313g K11
497. 2.500g E2 + 2.625g K6 + 0.187g K16 + 2.625g K12 + 2.625g K14
498. 0.250g E3 + 0.263g K6 + 0.263g K12 + 0.187g K16 + 0.263g K24
499. 2.500g E4 + 2.625g K6 + 2.625g K12 + 2.625g K2 + 0.187g K16
500. 0.200g E1 + 0.187g K16 + 0.210g K6 + 0.210g K12 + 0.210g K7 + 0.210g K9
501. 2.000g E2 + 2.100g K6 + 0.187g K16 + 2.100g K12 + 2.100g K7 + 2.100g K13
502. 1.000g E3 + 1.050g K6 + 1.050g K12 + 0.187g K16 + 1.050g K21 + 1.050g K1
503. 2.000g E4 + 2.100g K6 + 2.100g K12 + 2.100g K7 + 0.187g K16 + 2.100g K11
504. 1.000g E1 + 1.050g K6 + 1.050g K12 + 1.050g K7 + 1.050g K14 + 0.187g K16
505. 2.000g E2 + 0.390g K16 + 2.100g K6 + 2.100g K12 + 2.100g K7 + 2.100g K24
506. 1.000g E3 + 1.050g K6 + 0.390g K16 + 1.050g K12 + 1.050g K7 + 1.050g K2
507. 0.200g E4 + 0.210g K6 + 0.210g K12 + 0.390g K16 + 0.210g K9 + 0.210g K13
508. 2.000g E1 + 2.100g K6 + 2.100g K12 + 2.100g K9 + 0.390g K16 + 2.100g K1
509. 1.000g E2 + 1.050g K6 + 1.050g K12 + 1.050g K9 + 1.050g K11 + 0.390g K16
510. 1.000g E3 + 0.390g K16 + 1.050g K6 + 1.050g K12 + 1.050g K9 + 1.050g K14
511. 0.200g E4 + 0.210g K6 + 0.390g K16 + 0.210g K12 + 0.210g K9 + 0.210g K24
512. 0.200gE1 + 0.210g K6 + 0.210g K12 + 0.390g K16 + 0.210g K9 + 0.210g K2
513. 2.000g E2 + 2.100g K6 + 2.100g K12 + 2.100g K13 + 0.390g K16 + 2.100g Kl
514. 0.200gE3+0.210gK6+0.210gK12+0.210gK13+0.210gK11 +0.390gK16
515. 0.200g E4 + 0.390g K16 + 0.210g K6 + 0.210g K12 + 0.210g K13 +0.210gK14
516. 1.000g E1 + 1.050g K6 + 0.390g K16 + 1.050g K12 + 1.050g K13 + 1.050g K24
517. 1.000g E2 + 1.050g K6 + 1.050g K12 + 0.390g K16 + 1.050g K13 + 1.050g K2
518. 1.000g E3 + 1.050g K6 + 1.050g K12 + 1.050g K1 + 0.390g K16 + 1.050g K11
519. 1.000g E4 + 1.050g K6 + 1.050g K12 + 1.050g K1 + 1.050g K14 + 0.390g K16
520. 2.000g El + 0.390g K16 + 2.100g K6 + 2.100g K12 + 2.100g K1 + 2.100g K24
521. 0.200gE2+0.210gK6+0.390gK16+0.210gK12+0.210gK1 +0.210gK2
522. 2.000g E3 + 2.100g K6 + 2.100g K12 + 0.390g K16 + 2.100g Kl 1+ 2.100g K14
523. 1.000g E4 + 1.050g K6 + 1.050g K12 + 1.050g K11 + 0.390g K16 + 1.050g K24
CA 02646867 2008-12-16
W245FQ/JC 68
524. 0.200g E1 + 0.210g K6 + 0.210g K12 + 0.210g K11 + 0.210g K2 + 0.390g K16
525. 2.000g E2 + 0.390g K16 + 2. l00g K6 + 2.100g K12 + 2.100g K14 + 2.100g
K24
526. 1.000g E3 + 1.050g K6 + 0.390g K16 + 1.050g K12 + 1.050g K14 + 1.050g K2
527. 0.200g E4 + 0.210g K6 + 0.210g K12 + 0.390g K16 + 0.210g K24 + 0.210g K2
528. 0.500g El + 0.525g K6 + 0.390g K16
529. 1.667g E2 + 0.390g K16 + 1.750g K6 + 1.750g K8
530. 3.333g E3 + 3.500g K6 + 0.390g K16 + 3.500g K9
531. 1.667g E4 + 1.750g K6 + 1.750g K13 + 0.390g K16
532. 1.667g El + 0.390g K16 + 1.750g K6 + 1.750g K1
533. 3.333gE2+3.500gK6+0.390gK16+3.500gK11
534. 1.667g E3 + 1.750g K6 + 1.750g K14 + 0.390g K16
535. 3.333g E4 + 0.390g K16 + 3.500g K6 + 3.500g K24
536. 3.333g El + 3.500g K6 + 0.390g K16 + 3.500g K2
537. 2.500g E2 + 2.625g K6 + 2.625g K7 + 0.390g K16 + 2.625g K9
538. 0.250g E3 + 0.263g K6 + 0.263g K7 + 0.263g K13 + 0.390g K16
539. 1.250g E4 + 0.390g K16 + 1.313g K6 + 1.313g K7 + 1.313g K1
540. 2.500g El + 2.625g K6 + 0.390g K16 + 2.625g K7 + 2.625g K11
541. 1.250g E2 + 1.313g K6 + 1.313g K7 + 0.390g K16 + 1.313g K14
542. 1.250g E3 + 1.313g K6 + 1.313g K7 + 1.313g K24 + 0.390g K16
543. 2.500g E4 + 0.390g K16 + 2.625g K6 + 2.625g K7 + 2.625g K2
544. 1.250g El + 1.313g K6 + 0.390g K16 + 1.313g K9 + 1.313g K13
545. 1.250g E2 + 1.313g K6 + 1.313g K9 + 0.390g K16 + 1.313g K1
546. 0.250g E3 + 0.263g K6 + 0.263g K9 + 0.263g Kl 1+ 0.390g K16
547. 2.500g E4 + 0.390g K16 + 2.625g K6 + 2.625g K9 + 2.625g K14
548. 2.500g El + 2.625g K6 + 0.390g K16 + 2.625g K9 + 2.625g K24
549. 1.250g E2 + 1.313g K6 + 1.313g K9 + 0.390g K16 + 1.313g K2
550. 1.250g E3 + 1.313g K6 + 1.313g K13 + 1.313g K1 + 0.390g K16
551. 1.250gE4+0.390gK16+1.313gK6+1.313gK13+1.313gK11
552. 1.250gE1+1.313gK6+0.390gK16+1.313gK13+1.313gK14
553. 2.500g E2 + 2.625g K6 + 2.625g K13 + 0.390g K16 + 2.625g K24
554. 2.500g E3 + 2.625g K6 + 2.625g K13 + 2.625g K2 + 0.390g K16
555. 1.250g E4 + 0.390g K16 + 1.313g K6 + 1.313g K1 + 1.313g K11
CA 02646867 2008-12-16
W245FQ/JC 69
556. 1.250gE1+1.313gK6+0.390gK16+1.313gK1+1.313gK14
557. 1.250gE2+ 1.313gK6+ 1.313gK1+0.390gK16+ 1.313g K24 + 0.313g K17
558. 0.250g E3 + 0.263g K6 + 0.263g KI + 0.263g K2 + 0.090g K16 + 0.313g K18
559. 1.250g E4 + 0.390g K16 + 1.313g K6 + 1.313g K11 + 1.313g K14
560. 1.250g E1 + 1.313g K6 + 0.390g K16 + 1.313g K11 + 1.313g K24
561. 1.250g E2 + 1.313g K6 + 1.313g K11 + 0.390g K16 + 1.313g K2
562. 2.500g E3 + 2.625g K6 + 2.625g K14 + 2.625g K24 + 0.390g K16
563. 2.500g E4 + 0.390g K16 + 2.625g K6 + 2.625g K14 + 2.625g K2
564. 2.500g El + 2.625g K6 + 0.390g K16 + 2.625g K24 + 2.625g K2
565. 2.000gE2+2.100gK6+2.l00gK7+0.390gK16+2.100gK9+2.100gK13
566. 0.200g E3 + 0.210g K6 + 0.210g K7 + 0.210g K9 + 0.390g K16 + 0.210g K1
567. 2.000g E4 + 2.100g K6 + 2.100g K7 + 2.100g K9 + 2.100g Kl l+ 0.390g K16
568. 2.000g E1 + 0.390g K16 + 2.l00g K6 + 2.100g K7 + 2.100g K9 + 2.100g K14
569. 2.000g E2 + 2.100g K6 + 0.390g K16 + 2.100g K7 + 2.100g K9 + 2.100g K24
570. 0.200g E3 + 0.210g K6 + 0.210g K7 + 0.390g K16 + 0.210g K9 + 0.210g K2
571. 0.200g E4 + 0.210g K6 + 0.210g K7 + 0.210g K13 + 0.390g K16 + 0.210g K1
572. 1.000g El + 1.050g K6 + 1.050g K7 + 1.050g K13 + 1.050g Kl 1+ 0.390g K16
573. 0.200gE2+1.593gK16+0.210gK6+0.210gK21+0.210gK13+0.210gK14
574. 0.200g E3 + 0.210g K6 + 1.593g K16 + 0.210g K7 + 0.210g K13 + 0.210g K24
575. 1.000g E4 + 1.050g K6 + 1.050g K7 + 1.593g K16 + 1.050g K13 + l.050g K2
576. 2.000g E1 + 2.100g K6 + 2.100g K7 + 2.100g K1 + 1.593g K16 + 2.100g K11
577. 1.000g E2 + 1.050g K6 + 1.050g K7 + 1.050g K1 + 1.050g K14 + 1.593g K16
578. 2.000g E3 + 1.593g K16 + 2.100g K6 + 2.100g K7 + 2.100g K1 + 2.100g K24
579. 2.000g E4 + 2.100g K6 + 1.593g K16 + 2.100g K8 + 2.100g K1 + 2.100g K2
580. 0.200g E1 + 0.210g K6 + 0.210g K7 + 1.593g K16 + 0.210g K11 + 0.210g K14
581. 1.000g E2 + 1.050g K6 + 1.050g K7 + 1.050g Kl 1+ 1.593g K16 + 1.050g K24
582. 1.000g E3 + 1.050g K6 + 1.050g K7 + 1.050g K11 + 1.050g K2 + 1.593g K16
583. 2.000g E4 + 1.593g K16 + 2.100g K6 + 2.100g K7 + 2.100g K14 + 2.100g K24
584. 0.200gE11 +0.210gK6+ 1.593gK16+0.210gK7+0.210gK14+0.210gK2
585. 2.000g E2 + 2.100g K6 + 2.100g K7 + 1.593g K16 + 2.100g K24 + 2.100g K2
586. 1.000g E3 + 1.050g K6 + 1.050g K9 + 1.050g K13 + 1.593g K16 + 1.050g K1
587. 1.000g E4 + 1.050g K6 + 1.050g K9 + 1.050g K13 + 1.050g K11 + 1.593g K16
CA 02646867 2008-12-16
W245FQ/JC 70
588. 1.000g El + 1.593g K16 + 1.050g K6 + 1.050g K9 + 1.050g K13 + 1.050g K14
589. 0.200g E2 + 0.210g K6 + 1.593g K16 + 0.210g K9 + 0.210g K13 + 0.210g K24
590. 2.000g E3 + 2.100g K6 + 2.100g K9 + 1.593g K16 + 2.100g Kl3 + 2.100g K2
591. 2.000g E4 + 2.100g K6 + 2.100g K9 + 2.100g Kl + 1.593g K16 + 2.100g K11
592. 2.000g E1 + 2.100g K6 + 2.100g K9 + 2.100g Kl + 2.100g K14 + 1.593g Kl6
593. 0.200g E2 + 1.593g K16 + 0.2l0g K6 + 0.2lOg K9 + 0.210g K1 + 0.2lOg K24
594. 0.200g E3 + 0.210g K6 + 1.593g K16 + 0.210g K9 + 0.210g K1 + 0.210g K2
595. 2.000g E4 + 2.100g K6 + 2.100g K9 + 1.593g K16 + 2.100g Kl 1+ 2.100g K14
596. 2.000g E1 + 2.100g K6 + 2.100g K9 + 2.100g Kl l+ 1.593g K16 + 2.100g K24
597. 0.200gE2+0.210gK6+0.210gK9+0.210gK11 + 0.210g K2 + 1.593gK16
598. 2.000g E3 + 1.593g K16 + 2.100g K6 + 2.100g K9 + 2.100g K14 + 2.100g K24
599. 1.000g E4 + 1.050g K6 + 1.593g K16 + 1.050g K9 + 1.050g K14 + 1.050g K2
600. 1.000g El + 1.050g K6 + 1.050g K9 + 1.593g K16 + 1.050g K24 + 1.050g K2
601. 2.000g E2 + 2.100g K6 + 2.100g K13 + 2.100g K1 + 1.593g K16 + 2.100g K11
602. 0.200gE3+0.210gK6+0.210gK13+0.210gK1 +0.210gK14+ 1.593gK16
603. 1.000g E4 + 1.593g K16 + 1.050g K6 + 1.050g K13 + 1.050g Kl + 1.050g K24
604. 1.000g El + 1.050g K6 + 1.593g K16 + 1.050g K13 + 1.050g K1 + 1.050g K2
605. 2.000g E2 + 2.100g K6 + 2.100g K13 + 1.593g K16 + 2.100g K11 + 2.100g K14
606. 0.200g E3 + 0.210g K6 + 0.210g K13 + 0.210g K11 + 1.593g K16 + 0.210g K24
607. 2.000g E4 + 2.100g K6 + 2.l00g K13 + 2.100g K11 + 2.100g K2 + 1.593g K16
608. 0.200g El + 1.593g K16 + 0.210g K6 + 0.210g K13 + 0.210g K14 + 0.210g K24
609. 0.200g E2 + 0.2lOg K6 + 1.593g K16 + 0.210g K13 + 0.210g K14 + 0.2l0g K2
610. 2.000g E3 + 2.100g K6 + 2.100g K13 + 1.593g K16 + 2.100g K24 + 2.100g K2
611. 0.200gE4+0.210gK6+0.210gK1+0.210gK11+1.593gK16+0.210gK14
612. 1.000g El + l.050g K6 + 1.050g K1 + 1.050g K11 + 1.050g K24 + 1.593g K16
613. 0.200gE2+1.593gK16+0.210gK6+0.210gK1+0.210gKl1 +0.210gK2
614. 1.000g E3 + 1.050g K6 + 1.593g K16 + 1.050g K1 + 1.050g K14 + 1.050g K24
615. 2.000g E4 + 2.100g K6 + 2.100g K1 + 1.593g K16 + 2.100g K14 + 2.100g K2
616. 1.000g El + l.050g K6 + 1.050g Kl + 1.050g K24 + 1.593g K16 + 1.050g K2
617. 1.000g E2 + 1.050g K6 + l.050g K1 l+ 1.050g K14 + l.050g K24 + 1.593g K16
618. 1.000g E3 + 1.593g K16 + 1.050g K6 + l.050g Kl l+ 1.050g Kl4 + l.050g K2
1 619. 1.000g E4 + 1.050g K6 + 1.593g K16 + 1.050g K11 + 1.050g K24 + 1.050g
K2
CA 02646867 2008-12-16
W245FQ/JC 71
620. 0.200gE1 + 0.210g K6 + 0.210g K14 + 1.593g K16 + 0.210g K24 + 0.210g K2
621. 2.500g E2 + 2.625g K7 + 2.500g E8 + 2.625g K12 + 1.593g K16
622. 2.500g E3 + 1.593g K16 + 2.625g K8 + 2.500g E8 + 2.625g K6
623. 2.500g E4 + 2.625g K7 + 1.796g K16 + 2.500g E8 + 2.625g K9
624. 2.500g E1 + 2.625g K7 + 2.500g E8 + 1.796g K16 + 2.625g K13
625. 1.250g E2 + 1.313g K7 + 1.250g E8 + 1.313g K1 + 1.796g K16
626. 0.250g E3 + 1.796g K16 + 0.263g K7 + 0.250g E8 + 0.263g K11
627. 2.500g E4 + 2.625g K7 + 1.796g K16 + 2.500g E8 + 2.625g K14
628. 1.250g E1 + 1.313g K7 + 1.250g E8 + 1.796g K16 + 1.313g K24
629. 0.250g E2 + 0.263g K7 + 0.250g E8 + 0.263g K2 + 1.796g K16
630. 1.000g E3 + 1.796g K16 + 1.050g K21 + 1.000g E8 + 1.050g K12 + 1.050g K6
631. 2.000g E4 + 2.100g K7 + 1.796g K16 + 2.000g E8 + 2.100g K12 + 2.100g K9
632. 0.200g El + 0.210g K7 + 0.200g E8 + 1.796g K16 + 0.210g K12 + 0.210g K13
633. 2.000g E2 + 2.100g K7 + 2.000g E8 + 2.100g K12 + 1.796g K16 + 2.100g Kl
634. 2.000g E3 + 2.100g K7 + 2.000g E8 + 2.100g K12 + 2.100g K11 + 1.796g K16
635. 0.200g E4 + 1.796g K16 + 0.210g K7 + 0.200g E8 + 0.210g K12 + 0.210g K14
636. 0.200g E1 + 0.210g K7 + 1.796g K16 + 0.200g E8 + 0.210g K12 + 0.210g K24
637. 0.200g E2 + 0.210g K8 + 0.200g E8 + 1.796g K16 + 0.210g K12 + 0.210g K2
638. 0.200g E3 + 0.210g K7 + 0.200g E8 + 0.210g K6 + 1.796g K16 + 0.210g K9
639. 2.000g E4 + 2.100g K7 + 2.000g E8 + 2.100g K6 + 2.100g K13 + 1.796g K16
640. 1.000g E1 + 1.796g K16 + 1.050g K7 + 1.000g E8 + 1.050g K6 + 1.050g Kl
641. 1.000g E2 + 1.050g K7 + 1.796g K16 + 1.000g E8 + l.050g K6 + l.050g K11
642. 0.200g E3 + 0.210g K7 + 0.200g E8 + 1.796g K16 + 0.210g K6 + 0.210g K14
643. 1.000g E4 + 1.050g K7 + 1.000g E8 + 1.050g K6 + 1.796g K16 + 1.050g K24
644. 2.000g E 1+ 2.100g K7 + 2.000g E8 + 2.100g K6 + 2.100g K2 + 1.796g K 16
645. 0.200g E2 + 1.796g K16 + 0.210g K7 + 0.200g E8 + 0.210g K9 + 0.210g K22
646. 2.000g E3 + 2.100g K7 + 1.796g K16 + 2.000g E8 + 2.100g K9 + 2.l00g Kl
647. 2.000g E4 + 2.100g K7 + 2.000g E8 + 1.796g K16 + 2.100g K9 + 2.100g K11
648. 1.000g El + 1.050g K7 + 1.000g E8 + 1.050g K9 + 1.796g K16 + 1.050g K14
649. 1.000g E2 + 1.050g K7 + 1.000g E8 + 1.050g K9 + 1.050g K24 + 1.796g K16
650. 1.000g E3 + 1.796g K16 + 1.050g K7 + 1.000g E8 + 1.050g K9 + 1.050g K2
651. 0.200g E4 + 0.210g K21 + 1.796g K16 + 0.200g E8 + 0.210g K13 + 0.210g Kl
CA 02646867 2008-12-16
W245 FQ/J C 72
652. 1.000g El + 1.050g K7 + 1.000g E8 + 1.796g K16 + 1.050g K13 + 1.050g K11
653. 0.200g E2 + 0.210g K7 + 0.200g E8 + 0.210g K13 + 1.796g K16 + 0.210g K14
654. 0.200g E3 + 0.210g K7 + 0.200g E8 + 0.210g K13 + 0.210g K24 + 1.796g K16
655. 1.000g E4 + 1.796g K16 + 1.050g K7 + 1.000g E8 + 1.050g K13 + 1.050g K2
656. 0.200g El + 0.210g K7 + 1.796g K16 + 0.200g E8 + 0.210g Kl + 0.210g Kl 1
657. 1.000g E2 + 1.050g K7 + 1.000g E8 + 1.796g K16 + 1.050g K1 + 1.050g K14
658. 1.000g E3 + 1.050g K7 + 1.000g E8 + 1.050g K1 + 1.796g K16 + 1.050g K24
659. 2.000g E4 + 2.100g K8 + 2.000g E8 + 2.100g K1 + 2.100g K2 + 1.796g K16
660. 2.000g El + 1.796g K16 + 2.100g K7 + 2.000g E8 + 2.100g K11 + 2.100g K14
661. 1.000g E2 + 1.050g K7 + 1.796g K16 + 1.000g E8 + 1.050g K11 + 1.050g K24
662. 1.000g E3 + 1.050g K7 + 1.000g E8 + 1.796g K16 + 1.050g Kl 1+ 1.050g K2
663. 1.000g E4 + 1.050g K7 + 1.000g E8 + 1.050g K14 + 1.796g K16 + 1.050g K24
664. 1.000g El + 1.050g K7 + 1.000g E8 + 1.050g K14 + 1.050g K2 + 1.796g K16
665. 2.000g E2 + 1.796g K16 + 2. l00g K7 + 2.000g E8 + 2.100g K24 + 2.100g K2
666. 1.250g E11 + 1.313g K7 + 1.796g K16 + 1.250g E6 + 1.313g K12
667. 2.500g E10 + 2.625g K7 + 2.500g E6 + 1.796g K16 + 2.625g K6
668. 0.250g El + 0.263g K7 + 0.250g E6 + 0.263g K9 + 1.796g K16
669. 2.500g E2 + 1.796g K16 + 2.625g K7 + 2.500g E6 + 2.625g K13
670. 2.500g E3 + 2.625g K7 + 1.796g K16 + 2.500g E6 + 2.625g Kl
671. 0.250g E4 + 0.263g K7 + 0.250g E6 + 1.796g K16 + 0.263g K11
672. 0.250g El + 0.263g K21 + 0.250g E6 + 0.263g K14 + 1.796g K16
673. 2.500g E2 + 1.796g K16 + 2.625g K7 + 2.500g E6 + 2.625g K24
674. 0.250g E3 + 0.263g K7 + 1.796g K16 + 0.250g E6 + 0.263g K2
675. 0.200g E4 + 0.210g K7 + 0.200g E6 + 1.796g K16 + 0.210g K12 + 0.210g K6
676. 0.200gE1+0.210g1(7+0.200gE6+0.210gK12+1.796gK16+0.210gK9
677. 2.000g E2 + 2.100g K7 + 2.000g E6 + 2.100g K12 + 2.100g K13 + 1.796g K16
678. 1.000g E3 + 1.796g K16 + 1.050g K7 + 1.000g E6 + 1.050g K12 + 1.050g K1
679. 0.200g E4 + 0.210g K8 + 1.796g K16 + 0.200g E6 + 0.210g K12 + 0.210g 1(11
680. 0.200g El + 0.210g K7 + 0.200g E6 + 1.796g K16 + 0.210g K12 + 0.210g K14
681. 1.000g E2 + 1.050g K7 + 1.000g E6 + 1.050g K12 + 1.796g K16 + 1.050g K24
682. 0.200g E3 + 0.210g K8 + 0.200g E6 + 0.210g K12 + 0.210g K2 + 1.796g K16
683. 1.000g E4 + 1.796g K16 + 1.050g K7 + 1.000g E6 + 1.050g K6 + 1.050g K9
CA 02646867 2008-12-16
W245FQ/JC 73
684. 1.000g E1 + 1.050g K7 + 1.796g K16 + 1.000g E6 + 1.050g K6 + 1.050g K13
685. 0.200g E2 + 0.210g K7 + 0.200g E6 + 1.796g K16 + 0.210g K6 + 0.210g K1
686. 0.200g E3 + 0.210g K7 + 0.200g E6 + 0.210g K6 + 1.796g K16 + 0.210g K11
687. 0.200g E4 + 0.210g K7 + 0.200g E6 + 0.210g K6 + 0.210g K14 + 1.796g K16
688. 2.000g El + 1.796g K16 + 2.100g K7 + 2.000g E6 + 2.100g K6 + 2.100g K24
689. 0.200g E2 + 0.210g K7 + 1.796g K16 + 0.200g E6 + 0.210g K6 + 0.210g K2
690. 1.000g E3 + 1.050g K7 + 1.000g E6 + 1.796g K16 + 1.050g K9 + 1.050g K13
691. 0.200g E4 + 0.210g K7 + 0.200g E6 + 0.210g K9 + 1.999g K 16 + 0.210g K 1
692. 0.200g E 1+ 0.210g K7 + 0.200g E6 + 0.210g K9 + 0.210g K 11 + 1.999g K16
693. 0.200g E2 + 1.999g K16 + 0.210g K7 + 0.200g E6 + 0.210g K9 + 0.210g K14
694. 0.200g E 10 + 0.210g K21 + 1.999g K 16 + 0.200g E6 + 0.210g K9 + 0.210g
K24
695. 1.000g E4 + 1.050g K7 + 1.000g E6 + 1.999g K16 + 1.050g K9 + 1.050g K2
696. 0.200g El + 0.210g K7 + 0.200g E6 + 0.210g K13 + 1.999g K16 + 0.210g K1
697. 1.000g E2 + 1.050g K7 + 1.000g E6 + 1.050g K13 + 1.050g K11 + 1.999g K16
698. 2.000g E3 + 1.999g K16 + 2.100g K8 + 2.000g E6 + 2.100g K13 + 2.100g K14
699. 2.000g E4 + 2.100g K7 + 1.999g K16 + 2.000g E6 + 2.100g K13 + 2.100g K24
700. 1.000g E1 + 1.050g K7 + 1.000g E6 + 1.999g K16 + 1.050g K13 + 1.050g K2
701. 0.200g E2 + 0.210g K7 + 0.200g E6 + 0.210g K1 + 1.999g K16 + 0.210g K11
702. 0.200g E3 + 0.210g K7 + 0.200g E6 + 0.210g K1 + 0.210g K14 + 1.999g K16
703. 1.000g E4 + 1.999g K16 + 1.050g K7 + 1.000g E6 + 1.050g Kl + 1.050g K24
704. 0.200g E1 + 0.210g K7 + 1.999g K16 + 0.200g E6 + 0.210g K1 + 0.210g K2
705. 1.0009 E2 + 1.050g K8 + 1.000g E6 + 1.999g K16 + 1.050g K11 + 1.050g K14
706. 0.200g E3 + 0.210g K7 + 0.200g E6 + 0.210g Kl 1 + 1.999g K16 + 0.210g K24
707. 1.000g E4 + 1.050g K7 + 1.000g E6 + 1.050g K11 + 1.050g K2 + 1.999g K16
708. 0.200g E1 + 1.999g K16 + 0.210g K7 + 0.200g E6 + 0.210g K14 + 0.210g K24
709. 2.000g E2 + 2.100g K7 + 1.999g K16 + 2.000g E6 + 2.100g K14 + 2.l00g K2
710. 2.000g E3 + 2.100g K7 + 2.000g E6 + 1.999g K16 + 2.100g K24 + 2.100g K2
711. 0.250g E4 + 0.263g K7 + 0.250g E5 + 0.263g K12 + 1.999g K16
712. 1.250g E1 + 1.999g K16 + 1.313g K7 + 1.250g E5 + 1.313g K6
713. 0.250g E2 + 0.263g K7 + 1.999g K16 + 0.250g E5 + 0.263g K9
714. 0.250g E3 + 0.263g K7 + 0.250g E5 + 1.999g K16 + 0.263g K13
715. 0.250g E4 + 0.263g K7 + 0.250g E5 + 0.263g K1 + 1.999g K16
CA 02646867 2008-12-16
W245FQ/JC 74
716. 0.250g El + 1.999g K16 + 0.263g K21 + 0.250g E5 + 0.263g K11
717. 2.500g E2 + 2.625g K7 + 1.999g K16 + 2.500g E5 + 2.625g K14
718. 0.250g E3 + 0.263g K7 + 0.250g E5 + 1.999g K16 + 0.263g K24
719. 2.500g E4 + 2.625g K7 + 2.500g E5 + 2.625g K2 + 1.999g K16
720. 2.000g E1 + 1.999g K16 + 2.100g K7 + 2.000g E5 + 2.100g K12 + 2.100g K6
721. 2.000g E2 + 2.100g K7 + 1.999g K16 + 2.000g E5 + 2.100g K12 + 2.100g K9
722. 0.200g E3 + 0.210g K7 + 0.200g E5 + 1.999g K16 + 0.210g K12 + 0.210g K13
723. 0.200g E4 + 0.210g K7 + 0.200g E5 + 0.210g K12 + 1.999g K16 + 0.210g K1
724. 2.000g E1 + 2.100g K7 + 2.000g E5 + 2.100g K12 + 2.100g Kl 1+ 0.009g K17
+
1.999g K16
725. 1.000g E2 + 1.999g K16 + 1.050g K7 + 1.000g E5 + 1.050g K12 + 1.050g K14
726. 1.000g E3 + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K12 + 1.050g K24
727. 2.000g E4 + 2.100g K8 + 2.000g E5 + 1.999g K16 + 2.100g K12 + 2.100g K2
728. 2.000g El + 2.100g K7 + 2.000g E5 + 2.100g K6 + 1.999g K16 + 2.100g K9
729. 2.000g E2 + 2.100g K7 + 2.000g E5 + 2.100g K6 + 2.100g K13 + 1.999g K16
730. 1.000g E3 + 1.999g K16 + 1.050g K7 + 1.000g E5 + 1.050g K6 + 1.050g Kl
731. 1.000g E4 + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K6 + 1.050g K11
732. 0.200g El + 0.210g K7 + 0.200g E5 + 2.009g K16 + 0.210g K6 + 0.210g K14
733. 2.000g E2 + 2.100g K7 + 2.000g E5 + 2.100g K6 + 1.999g K16 + 2.100g K24
734. 2.000g E3 + 2.100g K7 + 2.000g E5 + 2.100g K6 + 2.100g K2 + 1.999g K16
735. 1.000g E4 + 1.999g K16 + 1.050g K7 + 1.000g E5 + 1.050g K9 + 1.050g K13
736. 1.000g El + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K9 + 0.050g K17
737. 2.000g E2 + 2.100g K8 + 2.000g E5 + 1.999g K16 + 2.100g K9 + 2.100g K11
738. 0.200g E3 + 0.210g K21 + 0.200g E5 + 0.210g K9 + 1.999g K16 + 0.210g K14
739. 2.000g E4 + 2.100g K7 + 2.000g E5 + 2.100g K9 + 2.100g K24 + 1.999g K16
740. 0.200g E1 + 1.999g K16 + 0.210g K7 + 0.200g E5 + 0.210g K9 + 0.210g K2
741. 1.000g E2 + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K13 + 1.050g K1
742. 0.200g E3 + 0.210g K7 + 0.200g E5 + 1.999g K16 + 0.210g K13 + 0.210g K11
743. 0.200g E4 + 0.210g K7 + 0.200g E5 + 0.210g K13 + 1.999g K16 + 0.210g K14
744. 1.000g El + 1.050g K7 + 1.000g E5 + 1.050g K13 + 1.050g K24 + 1.999g K16
745. 1.000g E2 + 1.999g K16 + 1.050g K7 + 1.000g E5 + 1.050g K13 + 1.050g K2
746. 1.000g E3 + 1.050g K7 + 1.999g K16 + 1.000g E5 + 1.050g K1 + 1.050g Kl 1
CA 02646867 2008-12-16
W245FQ/JC 75
747. 1.000g E4 + 1.050g K7 + 1.000g E5 + 1.999g K16 + 1.050g Kl + 1.050g K14
748. 1.000g El + 1.050g K7 + 1.000g E5 + 1.050g Kl + 1.999g K16 + 1.050g K24
749. 2.000g E2 + 2.100g K7 + 2.000g E5 + 2.100g K1 + 2.100g K2 + 1.999g K16
750. 0.200g E3 + 1.999g K16 + 0.210g K8 + 0.200g E5 + 0.210g K11 + 0.210g K14
751. 2.000g E4 + 2.100g K7 + 0.202g K16 + 2.000g E5 + 2. l00g Kl 1+ 2.100g K24
752. 2.000g E1 + 2.100g K7 + 2.000g E5 + 0.202g K16 + 2.100g K11 + 2.100g K2
753. 2.000g E2 + 2.100g K7 + 2.000g E5 + 2.100g K14 + 0.202g K16 + 2.100g K24
754. 1.000g E3 + 1.050g K7 + 1.000g E5 + 1.050g K14 + 1.050g K2 + 0.202g K16
755. 1.000g E4 + 0.202g K16 + 1.050g K7 + 1.000g E5 + 1.050g K24 + 1.050g K2
756. 0.250g El + 0.263g K7 + 0.202g K16 + 0.250g E7 + 0.263g K12
757. 2.500g E2 + 2.625g K7 + 2.500g E7 + 0.202g K16 + 2.625g K6
758. 0.250g E3 + 0.263g K7 + 0.250g E7 + 0.263g K9 + 0.202g K16
759. 2.500g E4 + 0.202g K16 + 2.625g K21 + 2.500g E7 + 2.625g K13
760. 2.500g El + 2.625g K7 + 0.202g K16 + 2.500g E7 + 2.625g Kl
761. 0.250g E2 + 0.263g K7 + 0.250g E7 + 0.202g K16 + 0.263g K11
762. 2.500g E3 + 2.625g K7 + 2.500g E7 + 2.625g K14 + 0.202g K16
763. 2.500g E4 + 0.202g K16 + 2.625g K7 + 2.500g E7 + 2.625g K24
764. 0.250g El + 0.263g K7 + 0.202g K16 + 0.250g E7 + 0.263g K2
765. 2.000g E2 + 2.100g K7 + 2.000g E7 + 0.202g K16 + 2.100g K12 + 2.100g K6
766. 0.200g E3 + 0.210g K7 + 0.200g E7 + 0.210g K12 + 0.202g K16 + 0.210g K9
767. 2.000g E4 + 2.100g K7 + 2.000g E7 + 2.100g K12 + 2.100g K13 + 0.202g K16
768. 2.000g E1 + 0.202g K16 + 2.100g K7 + 2.000g E7 + 2.100g K12 + 2.100g K1
769. 1.000g E2 + 1.050g K7 + 0.202g K16 + 1.000g E7 + 1.050g K12 + 1.050g K11
770. 1.000g E3 + 1.050g K7 + 1.000g E7 + 0.202g K16 + 1.050g K12 + 1.050g K14
771. 1.000g E4 + 1.050g K7 + 1.000g E7 + 1.050g K12 + 0.202g K16 + 1.050g K24
772. 2.000g E 1+ 2.100g K8 + 2.000g E7 + 2.100g K12 + 2.100g K2 + 0.202g K16
773. 0.2009 E2 + 0.202g K16 + 0.210g K7 + 0.200g E7 + 0.210g K6 + 0.210g K9
774. 1.000g E3 + 1.050g K7 + 0.202g K16 + 1.000g E7 + 1.050g K6 + 1.050g K13
775. 1.000g E4 + 1.050g K7 + 1.000g E7 + 0.202g K16 + 1.050g K6 + 1.050g Kl
776. 2.000g E1 + 2.100g K7 + 2.000g E7 + 2.100g K6 + 0.202g K16 + 2.100g K11
777. 0.200g E2 + 0.210g K7 + 0.200g E7 + 0.210g K6 + 0.210g K14 + 0.202g K16
778. 1.000g E3 + 0.202g K16 + 1.050g K7 + 1.000g E7 + 1.050g K6 + 1.050g K24
CA 02646867 2008-12-16
W245FQ/JC 76
779. 1.000g E4 + 1.050g K7 + 0.202g K16 + 1.000g E7 + 1.050g K6 + 1.050g K2
780. 0.200g E1 + 0.210g K21 + 0.200g E7 + 0.202g K16 + 0.210g K9 + 0.210g K13
781. 2.000g E2 + 2.100g K7 + 2.000g E7 + 2.100g K9 + 0.202g K16 + 2.100g Kl
782. 1.000g E3 + 1.050g K7 + 1.000g E7 + 1.050g K9 + 1.050g K11 + 0.202g K16
783. 2.000g E4 + 0.202g K16 + 2. l00g K7 + 2.000g E7 + 2.l00g K9 + 2.l00g K14
784. 0.200g E1 + 0.210g K7 + 0.202g K16 + 0.200g E7 + 0.210g K9 + 0.210g K24
785. 1.000g E2 + 1.050g K7 + 1.000g E7 + 0.202g K16 + 1.050g K9 + 1.050g K2
786. 1.000g E3 + 1.050g K7 + 1.000g E7 + 1.050g K13 + 0.202g K16 + 1.050g K1
787. 1.000g E4 + 1.050g K7 + 1.000g E7 + 1.050g K13 + 1.050g K11 + 0.202g K16
788. 2.000g El + 0.202g K16 + 2.100g K7 + 2.000g E7 + 2.100g K13 + 2.100g K14
789. 0.200g E2 + 0.210g K7 + 0.202g K16 + 0.200g E7 + 0.210g K13 + 0.210g K24
790. 2.000g E3 + 2.100g K7 + 2.000g E7 + 0.202g K16 + 2.100g K13 + 2.100g K2
791. 2.000g E4 + 2.100g K7 + 2.000g E7 + 2.100g Kl + 0.202g K16 + 2.100g K11
792. 2.000g E1 + 2.100g K7 + 2.000g E7 + 2.100g Kl + 2.100g K14 + 0.202g K16
793. 1.000g E2 + 0.202g K16 + 1.050g K7 + 1.000g E7 + 1.050g Kl + 1.050g K24
794. 0.200g E3 + 0.210g K8 + 0.202g K16 + 0.200g E7 + 0.210g K1 + 0.210g K2
795. 2.000g E4 + 2.100g K7 + 2.000g E7 + 0.202g K16 + 2.100g K11 + 2.100g K14
796. 1.000g E1 + 1.050g K7 + 1.000g E7 + 1.050g K11 + 0.202g K16 + 1.050g K24
797. 0.200g E2 + 0.210g K7 + 0.200g E7 + 0.210g Kl 1+ 0.210g K2 + 0.202g K16
798. 1.000g E3 + 0.202g K16 + 1.050g K7 + 1.000g E7 + 1.050g K14 + 1.050g K24
799. 0.200g E4 + 0.210g K7 + 0.202g K16 + 0.200g E7 + 0.210g K14 + 0.210g K2
800. 2.000g El + 2.100g K7 + 2.000g E7 + 0.202g K16 + 2.100g K24 + 2.100g K2
801. 3.333g E2 + 3.500g K21 + 3.500g K12 + 0.202g K16
802. 1.250g E3 + 0.202g K16 + 1.313g K7 + 1.313g K12 + 1.313g K6
803. 1.250g E4 + 1.313g K7 + 0.202g K16 + 1.313g K12 + 1.313g K9
804. 0.250g El + 0.263g K7 + 0.263g K12 + 0.202g K16 + 0.263g K13
805. 1.250g E2 + 1.313g K7 + 1.313g K12 + 1.313g K1 + 0.202g K16
806. 1.250g E3 + 0.202g K16 + 1.313g K7 + 1.313g K12 + 1.313g K11
807. 2.500g E4 + 2.625g K7 + 0.202g K16 + 2.625g K12 + 2.625g K14
808. 0.250g El + 0.263g K8 + 0.263g K12 + 0.202g K16 + 0.263g K24
809. 1.250g E2 + 1.313g K7 + 1.313g K12 + 1.313g K5 + 0.202g K16
810. 0.200gE3 +0.202gK16+0.210gK7+0.210gK12+0.210gK6+0.210gK9
CA 02646867 2008-12-16
W245FQ/JC 77
811. 2.000g E4 + 2.100g K7 + 0.202g K16 + 2.100g K12 + 2.100g K6 + 2.100g K13
812. 1.000g El + 1.050g K7 + 1.050g K12 + 0.202g K16 + 1.050g K6 + 1.050g Kl
813. 2.000g E2 + 2.100g K7 + 2.l00g K12 + 2.100g K6 + 0.202g K16 + 2.100g K11
814. 0.200gE3 +0.210gK7+0.210gK12+0.210gK6+0.210gK14+0.202gK16
815. 0.200g E4 + 0.202g K16 + 0.210g K7 + 0.210g K12 + 0.210g K6 + 0.210g K24
816. 2.000g E 1+ 2.100g K7 + 0.202g K16 + 2.100g K12 + 2.100g K6 + 2.100g K2
817. 1.000g E2 + 1.050g K8 + 1.050g K12 + 0.202g K16 + 1.050g K9 + 1.050g K13
818. 1.000g E3 + 1.050g K7 + 1.050g K12 + 1.050g K9 + 0.202g K16 + 1.050g Ki
819. 2.000g E4 + 2.100g K7 + 2.100g K12 + 2.100g K9 + 2.100g K11 + 0.405g K16
820. 1.000g El + 0.405g K16 + 1.050g K7 + 1.050g K12 + 1.050g K9 + 1.050g K14
821. 0.200g E2 + 0.210g K7 + 0.405g K16 + 0.210g K12 + 0.210g K9 + 0.210g K24
822. 2.000g E3 + 2.100g K7 + 2.100g K12 + 0.405g K16 + 2.100g K9 + 2.100g K2
823. 0.200g E4 + 0.210g K21 +0.210gK12+0.210gK13+0.405gK16+0.210gK1
824. 2.000g E1 + 2.100g K7 + 2.100g K12 + 2.100g K13 + 2.100g K11 + 0.405g K16
825. 0.200g E2 + 0.405g K16 + 0.210g K7 + 0.210g K12 + 0.210g K13 + 0.210g K14
826. 0.200g E3 + 0.210g K7 + 0.405g K16 + 0.210g K12 + 0.210g K13 + 0.210g K24
827. 0.200gE4+0.210gK7+0.2lOgK12+0.405gK16+0.210gK13+0.210gK2
828. 0.200gE1 +0.210gK7+0.210gK12+0.210gK1 +0.405gK16+0.210gK11
829. 2.000g E2 + 2.100g K7 + 2.100g K12 + 2.l00g K1 + 2.100g K14 + 0.405g K16
830. 2.000g E3 + 0.405g K16 + 2.100g K7 + 2.100g K12 + 2.100g K1 + 2.100g K24
831. 0.200gE4+0.210gK7+0.405gK16+0.210gK12+0.210gK1 +0.210gK2
832. 0.200g E1 + 0.210g K7 + 0.210g K12 + 0.405g K16 + 0.210g Kl 1+ 0.210g K14
833. 0.200gE2+0.2lOgK7+0.210gK12+0.210gK11 +0.405gK16+0.210gK24
834. 2.000g E3 + 2.100g K7 + 2.100g K12 + 2.100g Kl l+ 2.100g K2 + 0.405g K16
835. 2.000g E4 + 0.405g K16 + 2.100g K7 + 2.100g K12 + 2.100g K14 + 2.100g K24
836. 2.000g El + 2.100g K7 + 0.405g K16 + 2.100g K12 + 2.100g K14 + 2.100g K2
837. 2.000g E2 + 2.100g K7 + 2.100g K12 + 0.405g K16 + 2.100g K24 + 2.100g K2
838. 3.333g E3 + 3.500g K7 + 3.500g K6 + 0.405g K16
839. 0.250g E4 + 0.405g K16 + 0.263g K8 + 0.263g K6 + 0.263g K9
840. 2.500g El + 2.625g K7 + 0.405g K16 + 0.625g K3 + 2.625g K6 + 2.625g K13
841. 0.250g E2 + 0.263g K7 + 0.263g K6 + 0.405g K16 + 0.263g K19
842. 0.250g E3 + 0.263g K7 + 0.263g K6 + 0.263g K11 + 0.405g K16
CA 02646867 2008-12-16
W245FQ/JC 78
843. 2.500g E4 + 0.405g K16 + 2.625g K7 + 2.625g K6 + 2.625g K14
844. 0.250g El + 0.263g K21 + 0.405g K16 + 0.263g K6 + 0.263g K24
845. 0.250g E2 + 0.263g K7 + 0.263g K6 + 0.405g K16 + 0.263g K2
846. 2.000g E3 + 2.100g K7 + 2.100g K6 + 2.100g K9 + 0.405g K16 + 2.100g K13
847. 2.000g E4 + 2.100g K7 + 2.100g K6 + 2.100g K9 + 2.100g K1 + 0.405g K16
848. 1.000g El + 0.405g K16 + 1.050g K7 + 1.050g K6 + 1.050g K9 + 1.050g K11
849. 2.000g E2 + 2.100g K7 + 0.405g K16 + 2.100g K6 + 2.100g K9 + 2.100g K14
850. 1.000g E3 + 1.050g K7 + 1.050g K6 + 0.405g K16 + 1.050g K9 + 1.050g K24
851. 1.000g E4 + 1.050g K7 + 1.050g K6 + 1.050g K9 + 0.405g K16 + 1.050g K2
852. 0.200g El + 0.210g K7 + 0.210g K6 + 0.210g K13 + 0.210g Kl + 0.405g K16
853. 2.000g E2 + 0.405g K16 + 2.100g K7 + 2.100g K6 + 2.100g K13 + 2.100g K11
854. 2.000g E3 + 2.100g K7 + 0.405g K16 + 2.100g K6 + 2.100g K13 + 2.100g K14
855. 1.000g E4 + 1.050g K7 + 1.050g K6 + 0.405g K16 + 1.050g K13 + 1.050g K24
856. 2.000g El + 2.100g K7 + 2.100g K6 + 2.100g K13 + 0.405g K16 + 2.100g K2
857. 2.000g E2 + 2.100g K7 + 2.100g K6 + 2.100g K1 + 2.100g K11 + 0.405g K16
858. 2.000g E3 + 0.405g K16 + 2.100g K7 + 2.100g K6 + 2.100g Kl + 2.100g K14
859. 2.000g E4 + 2.100g K7 + 0.405g K16 + 2.100g K6 + 2.100g Kl + 2.100g K24
860. 0.200g El + 0.210g K7 + 0.210g K6 + 0.405g K16 + 0.210g KI + 0.210g K2
861. 0.200g E2 + 0.210g K8 + 0.210g K6 + 0.210g K11 + 0.405g K16 + 0.210g K14
862. 1.000g E3 + 1.050g K7 + 1.050g K6 + 1.050g K11 + 1.050g K24 + 0.405g K16
863. 1.000g E4 + 0.405g K16 + 1.050g K7 + 1.050g K6 + 1.050g K11 + 1.050g K2
864. 1.000g El + 1.050g K7 + 0.405g K16 + 1.050g K6 + 1.050g K14 + 1.050g K24
865. 0.200g E2 + 0.210g K21 + 0.210g K6 + 0.405g K16 + 0.210g K14 + 0.210g K2
866. 1.000g E3 + 1.050g K7 + 1.050g K6 + 1.050g K24 + 0.405g K16 + 1.050g K2
867. 0.500g El + 0.525g K7 + 0.405g K16 + 0.040g K17 + 0.045g K18
868. 1.667g El + 0.405g K16 + 1.750g K7 + 1.750g K9
869. 1.667g E2 + 1.750g K7 + 0.405g K16 + 1.750g K13
870. 3.333g E3 + 3.500g K7 + 3.500g K1 + 0.405g K16
871. 3.333g E4 + 0.405g K16 + 3.500g K7 + 3.500g K11
872. 3.333g El + 3.500g K7 + 0.405g K16 + 3.500g K14
873. 0.333g E2 + 0.350g K7 + 0.350g K24 + 0.405g K16
874. 0.333g E3 + 0.405g K16 + 0.350g K7 + 0.350g K2
CA 02646867 2008-12-16
W245FQ/JC 79
875. 2.500g E4 + 2.625g K7 + 0.405g K16 + 2.625g K9 + 2.625g K13
876. 1.250gE1+1.313gK7+1.313gK9+0.405gK16+1.313gK1
877. 0.250g E2 + 0.263g K7 + 0.263g K9 + 0.263g K11 + 0.405g K16
878. 0.250g E3 + 0.405g K16 + 0.263g K7 + 0.263g K9 + 0.263g K14
879. 1.250gE4+ 1.313g K7 + 0.405g K16 + 1.313g K9 + 1.313g K24
880. 0.250g El + 0.263g K7 + 0.263g K9 + 0.405g K16 + 0.263g K2
881. 1.250gE2+1.313gK7+1.313gK13+1.313gK1+0.405gK16
882. 2.500g E3 + 0.405g K16 + 2.625g K7 + 2.625g K13 + 2.625g Kl 1
883. 0.250g E4 + 0.263g K8 + 0.405g K16 + 0.263g K13 + 0.263g K14
884. 1.250g E1 + 1.313g K7 + 1.313g K13 + 0.405g K16 + 1.313g K24
885. 0.250g E2 + 0.263g K7 + 0.263g K13 + 0.263g K2 + 0.405g K16
886. 1.250gE3+1.608gK16+1.313gK21+1.313gK1+1.313gK11
887. 1.250gE4+1.313gK7+1.608gK16+1.313gK1+1.313gK14
888. 0.250g El + 0.263g K7 + 0.263g K1 + 1.608g K16 + 0.263g K24
889. 1.250g E2 + 1.313g K7 + 1.313g K1 + 1.313g K2 + 1.608g K16
890. 2.500g E3 + 1.608g K16 + 2.625g K7 + 2.625g K11 + 2.625g K14
891. 2.500g E4 + 2.625g K7 + 1.608g K16 + 2.625g K11 + 2.625g K24
892. 0.250g El + 0.263g K7 + 0.263g K11 + 1.608g K16 + 0.263g K2
893. 0.250g E2 + 0.263g K7 + 0.263g K14 + 0.263g K24 + 1.608g K16
894. 2.500g E3 + 1.608g K16 + 2.625g K7 + 2.625g K14 + 2.625g K2
895. 0.250g E4 + 0.263g K7 + 1.608g K16 + 0.263g K24 + 0.263g K2
896. 1.000g El + 1.050g K7 + 1.050g K9 + 1.608g K16 + 1.050g K13 + 1.050g K1
897. 0.200g E2 + 0.210g K7 + 0.210g K9 + 0.210g K13 + 1.608g K16 + 0.210g K11
898. 0.200g E3 + 0.210g K7 + 0.210g K9 + 0.210g K13 + 0.210g K14 + 1.608g K16
899. 2.000g E4 + 1.608g K16 + 2.l00g K7 + 2.l00g K9 + 2.l00g K13 + 2.100g K24
900. 1.000g E1 + 1.050g K7 + 1.608g K16 + 1.050g K9 + 1.050g K13 + 1.050g K2
901. 0.200g E2 + 0.210g K7 + 0.210g K9 + 1.608g K16 + 0.210g K1 + 0.210g K11
902. 2.000g E3 + 2.100g K7 + 2.100g K9 + 2.100g K1 + 1.608g Kl6 + 2.100g K14
903. 0.200g E4 + 0.210g K7 + 0.210g K9 + 0.210g K1 + 0.210g K24 + 1.608g K16
904. 1.000g El + 1.608g K16 + 1.050g K7 + 1.050g K9 + 1.050g Kl + 1.050g K2
905. 1.000g E2 + 1.050g K8 + 1.608g K16 + 1.050g K9 + 1.050g 1(11 + 1.050g K14
906. 2.000g E3 + 2.100g K7 + 2.100g K9 + 1.608g K16 + 2.100g Kl l+ 2.100g K24
CA 02646867 2008-12-16
W245FQ/JC 80
907. 2.000g E4 + 2.100g K21 + 2.100g K9 + 2.100g K11 + 1.608g K16 + 2.I OOg K2
908. 0.200g El + 0.210g K7 + 0.210g K9 + 0.210g K14 + 0.210g K24 + 1.608g K16
909. 0.200g E2 + 1.608g K16 + 0.210g K7 + 0.210g K9 + 0.210g K14 + 0.210g K2
910. 2.000g E3 + 2.100g K8 + 1.608g K16 + 2.100g K9 + 2.100g K24 + 2.100g K2
911. 1.000g E4 + 1.050g K7 + 1.050g K13 + 1.608g K16 + 1.050g K1 + 1.050g Kl 1
912. 0.200gE1+0.210gK7+0.210gK13+0.210gK1+1.608gK16+0.210gK14
913. 2.000g E2 + 2.100g K7 + 2.100g K13 + 2.100g K1 + 2.100g K24 + 1.608g K16
914. 1.000g E3 + 1.608g K16 + 1.050g K7 + 1.050g K13 + 1.050g K1 + 1.050g K2
915. 1.000g E4 + 1.050g K7 + 1.608g K16 + 1.050g K13 + 1.050g K11 + 1.050g K14
916. 0.200g E1 + 0.210g K7 + 0.210g K13 + 1.608g K16 + 0.210g K11 + 0.210g K24
917. 2.000g E2 + 2.100g K7 + 2.100g K13 + 2.100g K11 + 1.608g K16 + 2.100g K2
918. 0.200g E3 + 0.210g K7 + 0.210g K13 + 0.210g K14 + 0.210g K24 + 1.608g K16
919. 1.000g E4 + 1.608g K16 + 1.050g K7 + 1.050g K13 + 1.050g K14 + 1.050g K2
920. 2.000g E1 + 2.100g K7 + 1.608g K16 + 2.100g K13 + 2.100g K24 + 2.100g K2
921. 2.000g E2 + 2.l00g K7 + 2.100g Kl + 1.608g K16 + 2.100g K11 + 2.100g K14
922. 0.200g E3 + 0.210g K7 + 0.210g K1 + 0.210g K11 + 1.608g K16 + 0.210g K24
923. 1.000g E4 + 1.050g K7 + 1.050g K1 + 1.050g K11 + 1.050g K2 + 1.608g K16
924. 0.200g E1 + 1.608g K16 + 0.210g K7 + 0.210g K1 + 0.210g K14 + 0.210g K24
925. 2.000g E2 + 2.100g K7 + 1.608g K16 + 2.100g K1 + 2.100g K14 + 2.100g K2
926. 2.000g E3 + 2.100g K7 + 2.100g K1 + 1.608g K16 + 2.100g K24 + 2.100g K2
927. 0.200g E4 + 0.210g K7 + 0.210g K11 + 0.210g K14 + 1.608g K16 + 0.210g K24
928. 2.000g El + 2.100g K8 + 2.100g K11 + 2.100g K14 + 2.100g K2 + 1.608g K16
929. 0.200g E2 + 1.608g K16 + 0.210g K21 + 0.210g K11 + 0.210g K24 + 0.210g K2
930. 1.000g E3 + 1.050g K7 + 1.608g K16 + 1.050g K14 + 1.050g K24 + 1.050g K2
931. 2.500g E4 + 2.625g K9 + 2.500g E8 + 1.608g K16 + 2.625g K12 + 0.655g K10
932. 2.500g El + 2.625g K9 + 2.500g E8 + 2.625g K6 + 1.608g K16
933. 0.250g E2 + 1.608g K16 + 0.263g K9 + 0.250g E8 + 0.263g K7
934. 0.250g E3 + 0.263g K9 + 1.608g K16 + 0.250g E8 + 0.263g K13
935. 2.500g E4 + 2.625g K9 + 2.500g E8 + 1.608g K16 + 2.625g K1
936. 1.250g El + 1.313g K9 + 1.250g E8 + 1.313g K11 + 1.608g K16
937. 0.250g E2 + 1.608g K16 + 0.263g K9 + 0.250g E8 + 0.263g K14
938. 0.250g E3 + 0.263g K9 + 1.608g K16 + 0.250g E8 + 0.263g K24
CA 02646867 2008-12-16
W245FQ/JC 81
939. 1.250g E4 + 1.313g K9 + 1.250g E8 + 1.608g K16 + 1.313g K2
940. 1.000g El + 1.050g K9 + 1.000g E8 + 1.050g K12 + 1.608g K16 + 1.050g K6
941. 2.000g E2 + 2.100g K9 + 2.000g E8 + 2.100g K12 + 2.100g K7 + 1.608g K16
942. 0.200g E3 + 1.608g K16 + 0.210g K9 + 0.200g E8 + 0.210g K12 + 0.210g K13
943. 2.000g E4 + 2.100g K9 + 1.608g K16 + 2.000g E8 + 2.100g K12 + 2.100g Kl
944. 2.000g El + 2.100g K9 + 2.000g E8 + 1.608g K16 + 2.100g K12 + 2.100g K11
945. 2.000g E2 + 2.100g K9 + 2.000g E8 + 2.100g K12 + 1.608g K16 + 2.100g K14
946. 1.000g E3 + 1.050g K9 + 1.000g E8 + 1.050g K12 + 1.050g K24 + 1.608g K16
947. 1.000g E4 + 1.608g K16 + 1.050g K9 + 1.000g E8 + 1.050g K12 + 1.050g K2
948. 1.000g El + 1.050g K9 + 1.608g K16 + 1.000g E8 + 1.050g K6 + 1.050g K7
949. 0.200g E2 + 0.210g K9 + 0.200g E8 + 1.608g K16 + 0.210g K6 + 0.210g K13
950. 0.200g E3 + 0.210g K9 + 0.200g E8 + 0.210g K6 + 1.608g K16 + 0.210g KI
951. 2.000g E4 + 2.100g K9 + 2.000g E8 + 2.100g K6 + 2.100g K1 l+ 1.608g K16
952. 2.000g E1 + 1.608g K16 + 2.100g K9 + 2.000g E8 + 2.100g K6 + 2.100g K14
953. 2.000g E2 + 2.100g K9 + 1.608g K16 + 2.000g E8 + 2.100g K6 + 2.100g K24
954. 2.000g E3 + 2. l 00g K9 + 2.000g E8 + 1.811 g K16 + 2.100g K6 + 2.100g K2
955. 0.200g E4 + 0.210g K9 + 0.200g E8 + 0.210g K7 + 1.811g K16 + 0.210g K13
956. 2.000g El + 2.100g K9 + 2.000g E8 + 2.100g K7 + 2.100g K1 + 1.811g K16
957. 1.000g E2 + 1.811g K16 + 1.050g K9 + 1.000g E8 + 1.054g K7 + 1.050g K11
958. 0.200g E3 + 0.210g K9 + 1.811g K16 + 0.200g E8 + 0.210g K7 + 0.210g K14
959. 2.000g E4 + 2.100g K9 + 2.000g E8 + 1.811g K16 + 2.100g K7 + 2.100g K24
960. 2.000g E1 + 2.100g K9 + 2.000g E8 + 2.100g K7 + 1.811g K16 + 2.100g K2
961. 0.200g E2 + 0.210g K9 + 0.200g E8 + 0.210g K13 + 0.210g K1 + 1.811g K16
962. 0.200gE3+ 1.811gK16+0.210gK9+0.200gE8+0.210gK13+0.210gK11
963. 1.000g E4 + 1.050g K9 + 1.811g K16 + 1.000g E8 + 1.050g K13 + 1.050g K14
964. 2.000g E1 + 2. l00g K9 + 2.000g E8 + 1.811g K16 + 2.100g K13 + 2.100g K24
965. 1.000g E2 + 1.050g K9 + 1.000g E8 + 1.050g K13 + 1.811g K16 + 1.050g K2
966. 2.000g E3 + 2.100g K9 + 2.000g E8 + 2.100g K1 + 2.100g K11 + 1.811g K16
967. 2.000g E4 + 1.811g K16 + 2.100g K9 + 2.000g E8 + 2.100g Kl + 2.100g K14
968. 0.200g El + 0.210g K9 + 1.81 lg K16 + 0.200g E8 + 0.210g Kl + 0.210g K24
969. 0.200g E2 + 0.210g K9 + 0.200g E8 + 1.811g K16 + 0.210g K1 + 0.210g K2
970. 1.000g E3 + 1.050g K9 + 1.000g E8 + 1.050g K11 + 1.81 lg K16 + 1.050g K14
CA 02646867 2008-12-16
W245FQ/JC 82
971. 1.000g E4 + 1.050g K9 + 1.000g E8 + 1.050g K11 + 1.050g K24 + 1.811g K16
972. 2.000g El + 1.811g K16 + 2.100g K9 + 2.000g E8 + 2.100g K1 l+ 2.100g K2
973. 2.000g E2 + 2.100g K9 + 1.811 g K16 + 2.000g E8 + 2.100g K14 + 2.100g K24
974. 2.000g E3 + 2.100g K9 + 2.000g E8 + 1.811g K16 + 2.100g K14 + 2.100g K2
975. 0.200g E4 + 0.210g K9 + 0.200g E8 + 0.210g K24 + 1.811g K16 + 0.210g K2
976. 2.500g E1 + 2.625g K9 + 2.500g E6 + 2.625g K12 + 1.811g K16
977. 0.250g E2 + 1.811g K16 + 0.263g K9 + 0.250g E6 + 0.263g K6
978. 2.500g E3 + 2.625g K9 + 1.811gK16+2.500gE6+2.625gK7
979. 0.250g E4 + 0.263g K9 + 0.250g E6 + 1.81 lg K16 + 0.263g K13
980. 2.500g E1 + 2.625g K9 + 2.500g E6 + 2.625g Kl + 1.81 lg K16
981. 0.250g E2 + 1.811g K16 + 0.263g K9 + 0.250g E6 + 0.263g K11 + 0.050g K23
982. 2.500g E3 + 2.625g K9 + 1.811g K16 + 2.500g E6 + 2.625g K14
983. 1.250g E4 + 1.313g K9 + 1.250g E6 + 1.811g K16 + 1.313g K24
984. 1.250gE1 + 1.313gK9+ 1.250gE6+ 1.313gK2+ 1.811gK16
985. 0.200g E2 + 1.811 g K16 + 0.210g K9 + 0.200g E6 + 0.210g K12 + 0.210g K6
986. 1.000g E3 + 1.050g K9 + 1.811g K16 + 1.000g E6 + 1.050g K12 + 1.050g K7
987. 0.200gE4+0.210gK9+0.200gE6+ 1.811gK16+0.210gK12+0.210gK13
988. 0.200gE1 + 0.210g K9 + 0.200g E6 + 0.210g K12 + 1.811gK16+0.210gK1
989. 2.000g E2 + 2.100g K9 + 2.000g E6 + 2.100g K12 + 2.100g K11 + 1.811g K16
990. 1.000g E3 + 1.811g K16 + 1.050g K9 + 1.000g E6 + 1.050g K12 + 1.050g K14
991. 1.000g E4 + 1.050g K9 + 1.811g K16 + 1.000g E6 + 1.050g K12 + 1.050g K24
992. 0.200gE1 +0.210gK9+0.200gE6+ 1.811gK16+0.210gK12+0.210gK2
993. 1.000g E2 + 1.050g K9 + 1.000g E6 + 1.050g K6 + 1.811g K16 + 1.050g K7
994. 0.200g E3 + 0.210g K9 + 0.200g E6 + 0.210g K6 + 0.210g K13 + 1.811g K16
995. 2.000g E4 + 1.811g K16 + 2.100g K9 + 2.000g E6 + 2.100g K6 + 0.100g K18
996. 0.200gE1+0.210gK9+1.811gK16+0.200gE6+0.210gK6+0.2lOgK11
997. 0.200g E2 + 0.210g K9 + 0.200g E6 + 1.811g K16 + 0.210g K6 + 0.210g K14
998. 0.200g E3 + 0.210g K9 + 0.200g E6 + 0.210g K6 + 1.811g K16 + 0.210g K24
999. 1.000g E4 + 1.050g K9 + 1.000g E6 + 1.050g K6 + 1.050g K2 + 1.811g K16
1000 0.200g E1 + 1.811g K16 + 0.210g K9 + 0.200g E6 + 0.2l Og K7 + 0.210g K13
1001 0.200g E2 + 0.210g K9 + 1.811g K16 + 0.200g E6 + 0.210g K7 + 0.210g K1
1002 2.000g E3 + 2.100g K9 + 2.000g E6 + 1.811 g K16 + 2.100g K7 + 2.100g K11
CA 02646867 2008-12-16
W245FQ/JC 83
1003 1.000g E4 + 1.050g K9 + 1.000g E6 + 1.050g K7 + 1.811g K16 + 1.050g K14
1004 2.000g E 1+ 2.100g K9 + 2.000g E6 + 2. l 00g K7 + 2.100g K24 + 1.811 g K
16
1005 0.200g E2 + 1.811g K16 + 0.210g K9 + 0.200g E6 + 0.210g K7 + 0.210g K2
1006 0.200gE3+0.210gK9+1.811gK16+0.200gE6+0.210gK13+0.210gK1
1007 1.000g E4 + 1.050g K9 + 1.000g E6 + 1.811g K16 + 1.050g K13 + 1.050g K11
1008 2.000gE1 +2.100gK9+2.000gE6+2.100gK13+1.811gK16+2.100gK14
1009 1.000g E2 + 1.050g K9 + 1.000g E6 + 1.050g K13 + 1.050g K24 + 1.81 lg K16
1010 2.000g E3 + 1.811g K16 + 2.100g K9 + 2.000g E6 + 2.100g K13 + 2.100g K2
1011 0.200g E4 + 0.210g K9 + 1.811 g K16 + 0.200g E6 + 0.210g K1 + 0.210g K11
1012 2.000g E1 + 2.100g K9 + 2.000g E6 + 1.811g K16 + 2.100g Kl + 2.100g K14
1013 2.000g E2 + 2.100g K9 + 2.000g E6 + 2.100g K1 + 1.811g K16 + 2.100g K24
1014 1.000g E3 + 1.050g K9 + 1.000g E6 + 1.050g K1 + 1.050g K2 + 1.81 lg K16
1015 1.000g E4 + 1.81 lg K16 + 1.050g K9 + 1.000g E6 + 1.050g K11 + l.050g K14
1016 1.000g El + 1.050g K9 + 1.81 lg K16 + 1.000g E6 + 1.050g K11 + 1.050g K24
1017 0.200gE2+0.210gK9+0.200gE6+ 1.811gK16+0.210gK11 +0.210gK2
1018 0.200gE3+0.210gK9+0.200gE6+0.210gK14+1.811gK16+0.210gK24
1019 2.000g E4 + 2.100g K9 + 2.000g E6 + 2.100g K14 + 2.100g K2 + 1.811 g K16
1020 2.000g E 1+ 1.811 g K16 + 2. l 00g K9 + 2.000g E6 + 2.100g K24 + 2.100g
K2
1021 0.250g E2 + 0.263g K9 + 1.811g K16 + 0.250g E5 + 0.263g K12
1022 0.250g E3 + 0.263g K9 + 0.250g E5 + 0.013g K16 + 0.263g K6
1023 2.500g E4 + 2.625g K9 + 2.500g E5 + 2.625g K7 + 0.013g K16
1024 0.250g El + 0.013g K16 + 0.263g K9 + 0.250g E5 + 0.263g K13
1025 0.250g E2 + 0.263g K9 + 0.013g K16 + 0.250g E5 + 0.263g K1
1026 1.250g E3 + 1.313g K9 + 1.250g E5 + 0.013g K16 + 1.313g K11
1027 1.250g E4 + 1.313g K9 + 1.250g E5 + 1.313g K14 + 0.013g K16
1028 1.250g E1 + 0.013g K16 + 1.313g K9 + 1.250g E5 + 1.313g K24
1029 1.250g E2 + 1.313g K9 + 0.013g K16 + 1.250g E5 + 1.313g K2
1030 1.000g E3 + 1.050g K9 + 1.000g E5 + 0.013g K16 + 1.050g K12 + 1.050g K6
1031 1.000g E4 + 1.050g K9 + 1.000g E5 + 1.050g K12 + 0.013g K16 + 1.050g K21
1032 0.200gE1 + 0.210g K9 + 0.200g E5 + 0.210g K12 + 0.210g K13 + 0.013g K16
1033 2.000g E2 + 0.013g K16 + 2.l00g K9 + 2.000g E5 + 2.l00g K12 + 2.100g K1
1 1034 2.000g E3 + 2.100g K9 + 0.013g K16 + 2.000g E5 + 2.100g K12 + 2.100g
K11
CA 02646867 2008-12-16
W245FQ/JC 84
1035 0.200gE4+0.210gK9+0.200gE5+0.013gK16+0.210gK12+0.210gK14
1036 2.000g E1 + 2.100g K9 + 2.000g E5 + 2.100g K12 + 0.013g K16 + 2.100g K24
1037 2.000g E2 + 2.100g K9 + 2.000g E5 + 2.100g K12 + 2.100g K2 + 0.013g K16
1038 2.000g E3 + 0.013g K16 + 2.100g K9 + 2.000g E5 + 2.100g K6 + 2.100g K8
1039 2.000g E4 + 2.100g K9 + 0.013g K16 + 2.000g E5 + 2.100g K6 + 2.100g K13
1040 2.000g E1 + 2.100g K9 + 2.000g E5 + 0.013g K16 + 2.100g K6 + 2.100g Kl
1041 1.000g E2 + 1.050g K9 + 1.000g E5 + 1.050g K6 + 0.013g K16 + 1.050g K11
1042 0.200g E3 + 0.210g K9 + 0.200g E5 + 0.210g K6 + 0.210g K14 + 0.013g K16
1043 1.000g E4 + 0.013g K16 + 1.050g K9 + 1.000g E5 + 1.050g K6 + 1.050g K24
1044 2.000g El + 2.100g K9 + 0.013g K16 + 2.000g E5 + 2.100g K6 + 2.100g K2
1045 0.200g E2 + 0.210g K9 + 0.200g E5 + 0.013g K16 + 0.210g K7 + 0.210g K13
1046 2.000g E3 + 2.l00g K9 + 2.000g E5 + 2.100g K7 + 0.013g K16 + 2.100g K1
1047 0.200g E4 + 0.210g K9 + 0.200g E5 + 0.210g K7 + 0.210g K11 + 0.013g K16
1048 2.000g El + 0.013g Kl6 + 2.l00g K9 + 2.000g E5 + 2.l00g K7 + 2.l00g K14
1049 2.000g E2 + 2.100g K9 + 0.013g K16 + 2.000g E5 + 2.100g K7 + 2.100g K24
1050 0.200g E3 + 0.210g K9 + 0.200g E5 + 0.013g K16 + 0.210g K7 + 0.210g K2
1051 2.000gE4+2.100gK9+2.000gE5+2.100gK13+0.013gK16+2.100gK1
1052 0.200g El + 0.210g K9 + 0.200g E5 + 0.210g K13 + 0.210g K11 + 0.013g K16
1053 0.200gE2+0.013gK16+0.210gK9+0.200gE5+0.210gK13+0.210gK14
1054 1.000g E3 + 1.050g K9 + 0.013g K16 + 1.000g E5 + 1.050g K13 + 1.050g K24
1055 1.000g E4 + 1.050g K9 + 1.000g E5 + 0.013g K16 + 1.050g K13 + 1.050g K2
1056 1.000g El + 1.050g K9 + 1.000g E5 + 1.050g Kl + 0.013g K16 + 1.050g K11
1057 0.200g E2 + 0.210g K9 + 0.200g E5 + 0.210g Kl + 0.210g K14 + 0.013g K16
1058 2.000g E3 + 0.013g K16 + 2.100g K9 + 2.000g E5 + 2.100g K1 + 2.l00g K24
1059 0.200gE4+0.210gK9+0.013gK16+0.200gE5+0.210gK1 +0.210gK2
1060 0.200g E1 + 0.210g K9 + 0.200g E5 + 0.013g K16 + 0.210g K11 + 0.210g K14
1061 1.000g E2 + 1.050g K9 + 1.000g E5 + 1.050g Kl l+ 0.013g K16 + 1.050g K24
1062 2.000g E3 + 2.100g K9 + 2.000g E5 + 2.100g K1 l+ 2.100g K2 + 0.013g K16
1063 2.000g E4 + 0.013g Kl6 + 2.100g K9 + 2.000g E5 + 2.100g K14 + 2.100g K24
1064 2.000g E1 + 2.100g K9 + 0.013g K16 + 2.000g E5 + 2.100g K14 + 2.100g K2
1065 0.200g E2 + 0.210g K9 + 0.200g E5 + 0.013g K16 + 0.210g K24 + 0.210g K2
1066 2.500g E3 + 2.625g K9 + 2.500g E7 + 2.625g K12 + 0.013g K16
CA 02646867 2008-12-16
W245FQ/JC 85
1067 2.500g E4 + 0.013g K16 + 2.625g K9 + 2.500g E7 + 2.625g K6
1068 0.250g El + 0.263g K9 + 0.013g K16 + 0.250g E7 + 0.263g K7
1069 2.500g E2 + 2.625g K9 + 2.500g E7 + 0.013g K16 + 2.625g K13
1070 2.500g E3 + 2.625g K9 + 2.500g E7 + 2.625g K1 + 0.013g K16
1071 2.500g E4 + 0.013g K16 + 2.625g K9 + 2.500g E7 + 2.625g K11
1072 2.500g El + 2.625g K9 + 0.013g K16 + 2.500g E7 + 2.625g K14
1073 1.250g E2 + 1.313g K9 + 1.250g E7 + 0.013g K16 + 1.313g K24
1074 0.250g E3 + 0.263g K9 + 0.250g E7 + 0.263g K2 + 0.013g K16
1075 2.000g E4 + 0.013g K16 + 2.100g K9 + 2.000g E7 + 2.100g K12 + 2.100g K6
1076 0.200gE1 + 0.210g K9 + 0.013g K16 + 0.200g E7 + 0.210g K12 + 0.210g K7
1077 2.000g E2 + 2.100g K9 + 2.000g E7 + 0.013g K16 + 2.100g K12 + 2.100g K13
1078 1.000g E3 + 1.050g K9 + 1.000g E7 + 1.050g K12 + 0.013g K16 + 1.050g K5
1079 0.200g E4 + 0.210g K9 + 0.200g E7 + 0.210g K12 + 0.210g K11 + 0.013g K16
1080 0.200gE1 + 0.013g K16 + 0.210g K9 + 0.200g E7 + 0.210g K12 + 0.210g K14
1081 1.000g E2 + 1.050g K9 + 0.013g K16 + 1.000g E7 + 1.050g K12 + 1.050g K24
1082 0.200gE3 + 0.210g K9 + 0.200g E7 + 0.013g K16 + 0.210g K12 + 0.210g K2
1083 2.000g E4 + 2.100g K9 + 2.000g E7 + 2.100g K6 + 0.013g K16 + 2.100g K7
1084 0.200g El + 0.210g K9 + 0.200g E7 + 0.210g K6 + 0.210g K13 + 0.013g K16
1085 2.000g E2 + 0.013g K16 + 2.100g K9 + 2.000g E7 + 2.100g K6 + 2.100g K1
1086 2.000g E3 + 2.100g K9 + 0.013g K16 + 2.000g E7 + 2.100g K6 + 2.100g K11
1087 2.000g E4 + 2.100g K9 + 2.000g E7 + 0.013g K16 + 2.100g K6 + 2.100g K14
1088 1.000g E1 + 1.050g K9 + 1.000g E7 + 1.050g K6 + 0.013g K16 + 1.050g K24
1089 2.000g E2 + 2.100g K9 + 2.000g E7 + 2.100g K6 + 2.100g K2 + 0.216g K16
1090 0.200gE3+0.216gK16+0.210gK9+0.200gE7+0.210gK7+0.210gK13
1091 2.000g E4 + 2.100g K9 + 0.216g K16 + 2.000g E7 + 2.100g K7 + 2.100g Kl
1092 1.000g E1 + 1.050g K9 + 1.000g E7 + 0.216g K16 + 1.050g K7 + 1.050g Kl 1
1093 0.200g E2 + 0.210g K9 + 0.200g E7 + 0.210g K7 + 0.216g K16 + 0.210g K14
1094 1.000g E3 + 1.050g K9 + 1.000g E7 + 1.050g K7 + 1.050g K24 + 0.216g K16
1095 0.200g E4 + 0.216g K16 + 0.210g K9 + 0.200g E7 + 0.210g K7 + 0.210g K2
1096 1.000g El + 1.050g K9 + 0.216g K16 + 1.000g E7 + 1.050g K13 + 1.050g Ki
1097 0.200gE2+0.210gK9+0.200gE7+0.216gK16+0.210gK13+0.210gK11
1098 0.200g E3 + 0.210g K9 + 0.200g E7 + 0.210g K13 + 0.216g K16 + 0.210g K14
CA 02646867 2008-12-16
W245FQ/JC 86
1099 2.000g E4 + 2.l00g K9 + 2.000g E7 + 2.100g K13 + 2.100g K24 + 0.216g K16
1100 2.000g E1 + 0.216g K16 + 2.100g K9 + 2.000g E7 + 2.100g K13 + 2.100g K2
1101 1.000g E2 + 1.050g K9 + 0.216g K16 + 1.000g E7 + 1.050g K1 + 1.050g K11
1102 0.200g E3 + 0.210g K9 + 0.200g E7 + 0.216g K16 + 0.210g K1 + 0.210g K14
1103 0.200g E4 + 0.210g K9 + 0.200g E7 + 0.210g K1 + 0.216g K16 + 0.210g K24
1104 1.000g El + 1.050g K9 + 1.000g E7 + 1.050g K1 + 1.050g K2 + 0.216g K16
1105 1.000g E2 + 0.216g K16 + 1.050g K9 + 1.000g E7 + l.050g K11 + 1.050g K14
1106 2.000g E3 + 2.100g K9 + 0.216g K16 + 2.000g E7 + 2.100g K11 + 2.100g K24
1107 0.200g E4 + 0.210g K9 + 0.200g E7 + 0.216g K16 + 0.210g K11 + 0.210g K2
1108 2.000g El + 2.100g K9 + 2.000g E7 + 2.100g K14 + 0.216g K16 + 2.100g K24
1109 0.200g E2 + 0.210g K9 + 0.200g E7 + 0.210g K14 + 0.210g K2 + 0.216g K16
1110 1.000g E3 + 0.216g K16 + 1.050g K9 + 1.000g E7 + 1.050g K24 + 1.050g K2
1111 3.333g E4 + 3.500g K9 + 0.216g K16 + 3.500g K12
1112 0.250g El + 0.263g K9 + 0.263g K12 + 0.216g K16 + 0.263g K6
1113 0.250g E2 + 0.263g K9 + 0.263g K12 + 0.263g K7 + 0.216g K16
1114 1.250g E3 + 0.216g K16 + 1.313gK9+ 1.313gK12+ 1.313gK13
1115 2.500g E4 + 2.625g K9 + 0.216g K16 + 2.625g K12 + 2.625g K1
1116 1.250gE1+1.313gK9+1.313gK12+0.216gK16+1.313gK11
1117 2.500g E2 + 2.625g K9 + 2.625g K12 + 2.625g K14 + 0.216g K16
1118 1.250g E3 + 0.216g K16 + 1.313g K9 + 1.313g K12 + 1.313g K24
1119 0.250g E4 + 0.263g K9 + 0.216g K16 + 0.263g K12 + 0.263g K2 + 0.070g K23
1120 1.000g E1 + 1.050g K9 + 1.050g K12 + 0.216g K16 + 1.050g K6 + 1.050g K7
1121 2.000g E2 + 2.100g K9 + 2.100g K12 + 2.100g K6 + 0.216g K16 + 2.100g K13
1122 1.000g E3 + 1.050g K9 + 1.050g K12 + 1.050g K6 + 1.050g K1 + 0.216g K16
1123 1.000g E4 + 0.216g K16 + 1.050g K9 + 1.050g K12 + 1.050g K6 + 1.050g K11
1124 0.200gE1 + 0.210g K9 + 0.216g K16 + 0.210g K12 + 0.210g K6 + 0.210g K14
1125 2.000g E2 + 2.100g K9 + 2.100g K12 + 0.216g K16 + 2.100g K6 + 2.100g K24
1126 2.000g E3 + 2.100g K9 + 2.100g K12 + 2.100g K6 + 0.216g K16 + 2.100g K2
1127 1.000g E4 + 1.050g K9 + 1.050g K12 + 1.050g K7 + 1.050g K13 + 0.216g K16
1128 1.000g E1 + 0.216g K16 + 1.050g K9 + 1.050g K12 + 1.050g K7 + 1.050g K1
1129 1.000g E2 + 1.050g K9 + 0.216g K16 + 1.050g K12 + 1.050g K21 + 1.050g K11
1130 1.000g E3 + 1.050g K9 + 1.050g K12 + 0.216g K16 + 1.050g K7 + 1.050g K14
CA 02646867 2008-12-16
W245FQ/JC 87
1131 1.000g E4 + 1.050g K9 + 1.050g K12 + 1.050g K8 + 0.216g K16 + 1.050g K24
1132 2.000g E1 + 2.l00g K9 + 2.100g K12 + 2.100g K7 + 2.100g K2 + 0.216g K16
1133 0.200gE2+0.216gK16+0.210gK9+0.210gK12+0.210gK13+0.210gK5
1134 0.200gE3+0.210gK9+0.216gK16+0.210gK12+0.210gK13+0.210gK11
1135 0.200g E4 + 0.210g K9 + 0.210g K12 + 0.216g K16 + 0.210g K13 + 0.210g K14
1136 0.200gE1 + 0.210g K9 + 0.210g K12 + 0.210g K13 + 0.216g K16 + 0.210g K24
1137 2.000g E2 + 2.100g K9 + 2.100g K12 + 2.100g K13 + 2.100g K2 + 0.216g K16
1138 2.000g E3 + 0.216g K16 + 2.100g K9 + 2.100g K12 + 2.100g K1 + 2.100g K11
1139 0.200gE4+0.210gK9+0.216gK16+0.210gK12+0.210gK1 +0.210gK14
1140 2.000g E1 + 2.100g K9 + 2.100g K12 + 0.216g K16 + 2.100g K1 + 2.100g K24
1141 0.200gE2+0.210gK9+0.210gK12+0.210gK1 + 0.216g K16 + 0.210g K2
1142 0.200gE3+0.210gK9+0.210gK12+0.210gK11+0.210gK14+0.216gK16
1143 0.200gE4+0.216gK16+0.2lOgK9+0.210gK12+0.210gK1l+0.210gK24
1144 0.200gE1 +0.210gK9+0.216gK16+0.2lOgK12+0.210gK11 +0.2lOgK2
1145 2.000g E2 + 2.100g K9 + 2.100g K12 + 0.216g K16 + 2.100g K14 + 2.100g K24
1146 0.200g E3 + 0.210g K9 + 0.210g K12 + 0.210g K14 + 0.216g K16 + 0.210g K2
1147 2.000g E4 + 2.100g K9 + 2.100g K12 + 2.100g K24 + 2.100g K2 + 0.216g K16
1148 0.333g El + 0.216g K16 + 0.350g K9 + 0.350g K6
1149 0.250g E2 + 0.263g K9 + 0.216g K16 + 0.263g K6 + 0.263g K7
1150 0.250g E3 + 0.263g K9 + 0.263g K6 + 0.216g K16 + 0.263g K13
1151 1.250gE4+1.313gK9+1.313gK6+1.313gK1+0.216gK16
1152 0.250g El + 0.216g K16 + 0.263g K9 + 0.263g K6 + 0.263g Kl 1
1153 2.500g E2 + 2.625g K9 + 0.216g K16 + 2.625g K6 + 2.625g K14
1154 1.250g E3 + 1.313g K9 + 1.313g K6 + 0.216g K16 + 1.313g K24
1155 1.250g E4 + 1.313g K9 + 1.313g K6 + 1.313g K2 + 0.216g K16
1156 1.000g E1 + 0.216g K16 + 1.050g K9 + 1.050g K6 + 1.050g K7 + 1.050g K13
1157 2.000g E2 + 2.100g K9 + 0.419g K16 + 2.100g K6 + 2.100g K7 + 2.100g K1
1158 1.000g E3 + 1.050g K9 + 1.050g K6 + 0.419g K16 + 1.050g K7 + 1.050g Kl 1
1159 0.200g E4 + 0.210g K9 + 0.210g K6 + 0.210g K7 + 0.419g K16 + 0.210g K14
1160 2.000g E1 + 2.100g K9 + 2.100g K6 + 2.100g K7 + 2.100g K24 + 0.419g K16
1161 2.000g E2 + 0.419g K16 + 2.100g K9 + 2.100g K6 + 2.100g K7 + 2.100g K2
1162 2.000g E3 + 2.100g K9 + 0.419g K16 + 2.100g K6 + 2.100g K13 + 2.100g K1
CA 02646867 2008-12-16
W245FQ/JC 88
1163 0.200gE4+0.210gK9+0.210gK6+0.419gK16+0.210gK13+0.210gK11
1164 2.000g E1 + 2.100g K9 + 2.100g K6 + 2.100g K13 + 0.419g K16 + 2.100g K14
1165 0.200gE2+0.210gK9+0.210gK6+0.210gK13+0.210gK24+0.419gK16
1166 0.200g E3 + 0.419g K16 + 0.210g K9 + 0.210g K6 + 0.210g K13 + 0.210g K2
1167 0.200g E4 + 0.210g K9 + 0.419g K16 + 0.210g K6 + 0.210g K1 + 0.210g K11
1168 1.000g E1 + 1.050g K9 + 1.050g K6 + 0.419g K16 + 1.050g K1 + 1.050g K14
1169 0.200gE2+0.210gK9+0.210gK6+0.210gK1 + 0.419g K16 + 0.210g K24
1170 2.000g E3 + 2.100g K9 + 2.100g K6 + 2.100g K1 + 2.100g K2 + 0.419g K16
1171 2.000g E4 + 0.419g K16 + 2.100g K9 + 2.100g K6 + 2.100g K11 + 2.100g K14
1172 1.000g E1 + 1.050g K9 + 0.419g K16 + 1.050g K6 + 1.050g K11 + 1.050g K24
1173 2.000g E2 + 2.100g K9 + 2. l00g K6 + 0.419g K16 + 2.100g K11 + 2.100g K2
1174 1.000g E3 + 1.050g K9 + 1.050g K6 + 1.050g K14 + 0.419g K16 + 1.050g K24
1175 2.000g E4 + 2.100g K9 + 2.100g K6 + 2.100g K14 + 2.100g K2 + 0.419g K16
1176 1.000g E1 + 0.419g K16 + 1.050g K9 + 1.050g K6 + 1.050g K24 + 1.050g K2
1177 1.667g E2 + 1.750g K9 + 0.419g K16 + 1.750g K7
1178 0.250g E3 + 0.263g K9 + 0.263g K7 + 0.419g K16 + 0.263g K13
1179 1.250gE4+1.313gK9+1.313gK7+1.313gK1+0.419gK16
1180 1.250g E1 + 0.419g K16 + 1.313g K9 + 1.313g K7 + 1.313g K11
1181 1.250gE2+ 1.313g K9 + 0.419g K16 + 1.313gK7+ 1.313gK14
1182 0.250g E3 + 0.263g K9 + 0.263g K7 + 0.419g K16 + 0.263g K24
1183 0.250g E4 + 0.263g K9 + 0.263g K7 + 0.263g K2 + 0.419g K16
1184 2.000g E1 + 0.419g K16 + 2.100g K9 + 2. l00g K7 + 2.100g K13 + 2.100g Kl
1185 1.000g E2 + 1.050g K9 + 0.419g K16 + 1.050g K7 + 1.050g K13 + 1.050g K11
1186 2.000g E3 + 2.100g K9 + 2.l00g K7 + 0.419g K16 + 2.l00g K13 + 2.100g K14
1187 1.000g E4 + 1.050g K9 + 1.050g K21 + 1.050g K13 + 0.419g K16 + 1.050g K24
1188 2.000g E1 + 2.100g K9 + 2.100g K7 + 2.100g K13 + 2.100g K2 + 0.419g K16
1189 1.000g E2 + 0.419g K16 + 1.050g K9 + 1.050g K7 + 1.050g K1 + 1.050g K11
1190 1.000g E3 + 1.050g K9 + 0.419g K16 + 1.050g K8 + 1.050g K1 + 1.050g K14
1191 0.200gE4+0.210gK9+0.210gK7+0.419gK16+0.210gK1 +0.210gK24
1192 1.000g E1 + 1.050g K9 + 1.050g K7 + 1.050g Kl + 0.419g K16 + 1.050g K2
1193 0.200gE2+0.210gK9+0.210gK7+0.210gK11 + 0.210g K14 + 0.419g K16
1194 2.000g E3 + 0.419g K16 + 2.100g K9 + 2. l00g K7 + 2.100g K11 + 2.100g K24
CA 02646867 2008-12-16
W245FQ/JC 89
1195 0.200gE4+0.210gK9+0.419gK16+0.210gK7+0.210gK11 +0.210gK2
1196 0.200gE1+0.210gK9+0.2lOgK7+0.419gK16+0.210gK14+0.210gK24
1197 2.000g E2 + 2.100g K9 + 2.100g K7 + 2.100g K14 + 0.419g K16 + 2.100g K2
1198 0.200g E3 + 0.210g K9 + 0.210g K7 + 0.210g K24 + 0.210g K2 + 0.419g K16
1199 2.500g El + 0.419g K16 + 2.625g K9
1200 3.333g El + 3.500g K9 + 0.419g K16 + 3.500g K13
1201 0.333g E2 + 0.350g K9 + 0.350g K1 + 0.419g K16
1202 1.667g E3 + 0.419g K16 + 1.750g K9 + 1.750g K11
1203 0.333g E4 + 0.350g K9 + 0.419g K16 + 0.350g K14
1204 3.333g El + 3.500g K9 + 3.500g K24 + 0.419g K16 + 0.139g K19
1205 0.333g E2 + 0.419g K16 + 0.350g K9 + 0.350g K2
1206 0.250g E3 + 0.263g K9 + 0.419g K16 + 0.263g K13 + 0.263g K1
1207 2.500g E4 + 2.625g K9 + 2.625g K13 + 0.419g K16 + 2.625g K11
1208 2.500g El + 2.625g K9 + 2.625g K13 + 2.625g K14 + 0.419g K16
1209 1.250g E2 + 0.419g K16 + 1.313gK9+ 1.313gK13+ 1.313gK24
1210 0.250g E3 + 0.263g K9 + 0.419g K16 + 0.263g K13 + 0.263g K2
1211 2.500g E4 + 2.625g K9 + 2.625g K1 + 0.419g K16 + 2.625g K11
1212 0.250g El + 0.263g K9 + 0.263g Kl + 0.263g K14 + 0.419g K16
1213 2.500g E2 + 0.419g K16 + 2.625g K9 + 2.625g Kl + 2.625g K24
1214 1.250gE3+1.313gK9+0.419gK16+1.313gK1+1.313gK2
1215 2.500g E4 + 2.625g K9 + 2.625g Kl 1+ 0.419g K16 + 2.625g K14
1216 0.250g El + 0.263g K9 + 0.263g K11 + 0.263g K24 + 0.419g K16
1217 2.500g E2 + 0.419g K16 + 2.625g K9 + 2.625g Kl 1+ 2.625g K2
1218 1.250g E3 + 1.313g K9 + 0.419g K16 + 1.313g K14 + 1.313g K24
1219 1.250g E4 + 1.313g K9 + 1.313g K14 + 0.419g K16 + 1.313g K2
1220 2.500g El + 2.625g K9 + 2.625g K24 + 2.625g K2 + 0.419g K16
1221 2.000g E2 + 0.419g K16 + 2.100g K9 + 2.100g K13 + 2.100g Kl + 2.100g K11
1222 1.000g E3 + 1.050g K9 + 0.419g K16 + 1.050g K13 + 1.050g K1 + 1.050g K14
1223 2.000g E4 + 2.100g K9 + 2.100g K13 + 0.419g K16 + 2.100g K1 + 2.100g K24
1224 0.200gE1+0.210gK9+0.210gK13+0.210gK1+0.419gK16+0.210gK2
1225 0.200g E2 + 0.210g K9 + 0.2lOg K13 + 0.210g K11 + 0.210g K14 + 0.419g K16
1226 1.000g E3 + 0.419g K16 + 1.050g K9 + 1.050g K13 + 1.050g K11 + 1.050g K24
CA 02646867 2008-12-16
W245 FQ/J C 90
1227 2.000g E4 + 2.100g K9 + 0.419g K16 + 2.100g K13 + 2.100g K11 + 2.100g K2
1228 1.000g El + 1.050g K9 + 1.050g K13 + 0.419g K16 + 1.050g K14 + 1.050g K24
1229 0.200g E2 + 0.210g K9 + 0.210g K13 + 0.210g K14 + 0.419g K16 + 0.210g K2
1230 1.000g E3 + 1.050g K9 + 1.050g K13 + 1.050g K24 + 1.050g K2 + 0.419g K16
1231 1.000g E4 + 0.419g K16 + 1.050g K9 + 1.050g K1 + 1.050g Kl 1+ 1.050g K14
1232 2.000g E1 + 2.l00g K9 + 0.419g K16 + 2.l00g K1 + 2.l00g K11 + 2.100g K24
1233 0.200gE2+0.210gK9+0.210gK1 +0.419gK16+0.210gK11 +0.210gK2
1234 2.000gE3+2.100gK9+2.100gK1 + 2.100g K14 + 0.419g K16 + 2.100g K24
1235 1.000g E4 + 1.050g K9 + 1.050g K1 + 1.050g K14 + 1.050g K2 + 0.419g K16
1236 0.200gEl +0.419gK16+0.210gK9+0.210gK1 + 0.210g K24 + 0.210g K2
1237 1.000g E2 + 1.050g K9 + 1.622g K16 + 1.050g Kl 1+ 1.050g K14 + 1.050g K24
1238 0.200g E3 + 0.210g K9 + 0.210g K11 + 1.622g K16 + 0.210g K14 + 0.210g K2
1239 1.000g E4 + 1.050g K9 + 1.050g K11 + 1.050g K24 + 1.622g K16 + 1.050g K2
1240 1.000g E1 + 1.050g K9 + 1.050g K14 + 1.050g K24 + 1.050g K2 + 1.622g K16
1241 2.500g E2 + 1.622g K16 + 2.625g K13 + 2.500g E8 + 2.625g K12 + 2.625g K10
1242 0.250g E3 + 0.263g K13 + 1.622g K16 + 0.250g E8 + 0.263g K6
1243 0.250g E4 + 0.263g K13 + 0.250g E8 + 1.622g K16 + 0.263g K7
1244 0.250g El + 0.263g K13 + 0.250g E8 + 0.263g K9 + 1.622g K16 + 0.622g K15
1245 1.250g E2 + 1.622g K16 + 1.313g K13 + 1.250g E8 + 1.313g K1
1246 1.250g E3 + 1.313g K13 + 1.622g K16 + 1.250g E8 + 1.313g K11
1247 2.500g E4 + 2.625g K22 + 2.500g E8 + 1.622g K16 + 2.625g K14
1248 1.250g E1 + 1.313g K13 + 1.250g E8 + 1.313g K24 + 1.622g K16
1249 1.250g E2 + 1.622g K16 + 1.313g K13 + 1.250g E8 + 1.313g K2
1250 2.000g E3 + 2.100g K13 + 1.622g K16 + 2.000g E8 + 2.100g K12 + 2.100g K6
1251 2.000g E4 + 2.100g K13 + 2.000g E8 + 1.622g K16 + 2.100g K12 + 2.100g K7
1252 0.200g E1 + 0.210g K13 + 0.200g E8 + 0.210g K12 + 1.622g K16 + 0.210g K9
1253 2.000g E2 + 2.100g K13 + 2.000g E8 + 2.100g K12 + 2.100g K1 + 1.622g K16
1254 0.200g E3 + 1.622g K16 + 0.210g K13 + 0.200g E8 + 0.210g K12 + 0.210g K11
1255 1.000g E4 + 1.050g K13 + 1.622g K16 + 1.000g E8 + 1.050g K12 + 1.050g K14
1256 2.000g El + 2.100g K13 + 2.000g E8 + 1.622g K16 + 2.100g K12 + 2.100g K24
1257 0.200g E2 + 0.210g K13 + 0.200g E8 + 0.210g K12 + 1.622g K16 + 0.210g K2
1258 2.000g E3 + 2.100g K 13 + 2.000g E8 + 2. 1 00g K6 + 2.100g K7 + 1.622g
K16
CA 02646867 2008-12-16
W245FQ/JC 91
1259 2.000g E4 + 1.622g K16 + 2.100g K13 + 2.000g E8 + 2.100g K6 + 2.100g K9
1260 2.000g El + 2.100g K13 + 1.622g K16 + 2.000g E8 + 2.100g K6 + 2.100g K1
1261 1.000g E2 + 1.050g K13 + 1.000g E8 + 1.622g K16 + 1.050g K6 + 1.050g K11
1262 2.000g E3 + 2.100g K13 + 2.000g E8 + 2.100g K6 + 1.622g K16 + 2.100g K14
1263 1.000g E4 + 1.050g K13 + 1.000g E8 + 1.050g K6 + 1.050g K24 + 1.622g K16
1264 1.000g El + 1.622g K16 + 1.050g K13 + 1.000g E8 + 1.050g K6 + 1.050g K2
1265 0.200g E2 + 0.210g Kl3 + 1.622g K16 + 0.200g E8 + 0.210g K7 + 0.210g K9
1266 0.200g E3 + 0.210g K13 + 0.200g E8 + 1.622g K16 + 0.210g K7 + 0.210g Kl
1267 2.000g E4 + 2.100g K13 + 2.000g E8 + 2.100g K7 + 1.622g K16 + 2.100g K11
1268 1.000g El + 1.050g K22 + 1.000g E8 + 1.050g K7 + 1.050g K14 + 1.622g K16
1269 1.000g E2 + 1.622g K16 + 1.050g K13 + 1.000g E8 + 1.050g K7 + 1.050g K24
1270 1.000g E3 + 1.050g K13 + 1.622g K16 + 1.000g E8 + 1.050g K7 + 1.050g K2
1271 2.000g E4 + 2.l00g K13 + 2.000g E8 + 1.622g K16 + 2.l00g K9 + 2.l00g K1
1272 0.200g El + 0.210g K13 + 0.200g E8 + 0.210g K9 + 1.622g K16 + 0.210g Kl 1
1273 1.000g E2 + 1.050g K13 + 1.000g E8 + 1.050g K9 + l.050g K14 + 1.622g K16
1274 2.000g E3 + 1.622g K16 + 2.100g K13 + 2.000g E8 + 2.100g K9 + 2.100g K24
1275 0.200g E4 + 0.210g K13 + 1.622g K16 + 0.200g E8 + 0.210g K9 + 0.210g K2
1276 0.200g El + 0.210g K13 + 0.200g E8 + 1.622g K16 + 0.210g K1 + 0.210g K11
1277 1.000g E2 + 1.050g K13 + 1.000g E8 + 1.050g Kl + 1.622g K16 + 1.050g K14
1278 1.000g E3 + 1.050g K13 + 1.000g E8 + 1.050g K1 + 1.050g K24 + 1.622g K16
1279 2.000g E4 + 1.622g K16 + 2.100g K13 + 2.000g E8 + 2.100g K1 + 2.100g K2
1280 0.200g E1 + 0.210g K13 + 1.622g K16 + 0.200g E8 + 0.210g K11 + 0.210g K14
1281 2.000g E2 + 2.100g K13 + 2.000g E8 + 1.622g K16 + 2.100g K11 + 2.100g K24
1282 2.000g E3 + 2.100g K13 + 2.000g E8 + 2.100g K11 + 1.622g K16 + 2.100g K2
1283 0.200g E4 + 0.210g K13 + 0.200g E8 + 0.210g K14 + 0.210g K24 + 1.622g K16
1284 2.000g E1 + 1.622g K16 + 2.100g K13 + 2.000g E8 + 2.100g K14 + 2.100g K2
1285 1.000g E2 + 1.050g K13 + 1.622g K16 + 1.000g E8 + 1.050g K24 + 1.050g K2
1286 0.250g E3 + 0.263g K13 + 0.250g E6 + 1.622g K16 + 0.263g K12
1287 2.500g E4 + 2.625g K13 + 2.500g E6 + 2.625g K6 + 1.622g K16
1288 1.250g E1 + 1.622g K16 + 1.313g K13 + 1.250g E6 + 1.313g K21
1289 2.500g E2 + 2.625g K13 + 1.622g K16 + 2.500g E6 + 2.625g K9
1290 1.250g E3 + 1.313g K13 + 1.250g E6 + 1.622g K16 + 1.313g KI
CA 02646867 2008-12-16
W245FQ/JC 92
1291 0.250g E4 + 0.263g K13 + 0.250g E6 + 0.263g K11 + 1.622g K16
1292 1.250g E1 + 1.622g K16 + 1.313g K13 + 1.250g E6 + 1.313g K14
1293 0.250g E2 + 0.263g K13 + 1.622g K16 + 0.250g E6 + 0.263g K24
1294 1.250g E3 + 1.313g K13 + 1.250g E6 + 1.622g K16 + 1.313g K2
1295 2.000g E4 + 2.1 OOg K 13 + 2.000g E6 + 2.100g K 12 + 1.622g K 16 + 2.100g
K6
1296 0.200g E1 + 0.210g K13 + 0.200g E6 + 0.210g K12 + 0.210g K7 + 1.622g K16
1297 1.000g E2 + 1.622g K16 + 1.050g K13 + 1.000g E6 + 1.050g K12 + 1.050g K9
1298 2.000g E3 + 2.100g K13 + 1.622g K16 + 2.000g E6 + 2.100g K12 + 2.100g K1
1299 1.000g E4 + 1.050g K13 + 1.000g E6 + 1.622g K16 + 1.050g K12 + 1.050g K11
1300 2.000g E1 + 2.l00g K13 + 2.000g E6 + 2.l00g K12 + 1.622g K16 + 2.l00g K14
1301 0.200g E2 + 0.210g K13 + 0.200g E6 + 0.210g K12 + 0.210g K24 + 1.622g K16
1302 1.000g E3 + 1.622g K16 + 1.050g K13 + 1.000g E6 + 1.050g K12 + 1.050g K2
1303 1.000g E4 + 1.050g K13 + 1.622g K16 + 1.000g E6 + 1.050g K6 + 1.050g K7
1304 2.000g El + 2.100g K13 + 2.000g E6 + 1.622g K16 + 2.100g K6 + 2.100g K9
1305 2.000g E2 + 2.100g K13 + 2.000g E6 + 2.100g K6 + 1.622g K16 + 2.100g K1
1306 1.000g E3 + 1.050g K13 + 1.000g E6 + 1.050g K6 + 1.050g K11 + 1.622g K16
1307 2.000g E4 + 1.622g K16 + 2.100g K13 + 2.000g E6 + 2.100g K6 + 2.100g K14
1308 0.200g El + 0.210g K13 + 1.622g K16 + 0.200g E6 + 0.210g K6 + 0.210g K24
1309 0.200g E2 + 0.210g K13 + 0.200g E6 + 1.622g K16 + 0.210g K6 + 0.21 Qg K2
1310 0.200g E3 + 0.210g K13 + 0.200g E6 + 0.210g K7 + 1.622g K16 + 0.210g K9
1311 0.200g E4 + 0.210g K13 + 0.200g E6 + 0.210g K8 + 0.210g K1 + 1.622g K16
1312 0.200gE1 +1.622gK16+0.210gK13+0.200gE6+0.210gK7+0.210gK11
1313 1.000g E2 + 1.050g K13 + 1.622g K16 + 1.000g E6 + 1.050g K7 + 1.050g K14
1314 0.200g E3 + 0.210g K13 + 0.200g E6 + 1.622g K16 + 0.210g K7 + 0.210g K24
1315 1.000g E4 + 1.050g K13 + 1.000g E6 + 1.050g K7 + 1.622g K16 + 1.050g K2
1316 1.000g El + 1.050g K13 + 1.000g E6 + 1.050g K9 + 1.050g K1 + 1.622g K16
1317 0.200gE2+1.622gK16+0.210gK13+0.200gE6+0.210gK9+0.210gKil
1318 0.200g E3 + 0.210g K13 + 1.622g K16 + 0.200g E6 + 0.210g K9 + 0.210g K14
1319 1.000g E4 + 1.050g K13 + 1.000g E6 + 1.622g K16 + 1.050g K9 + 1.050g K24
1320 1.000g E1 + 1.050g K13 + 1.000g E6 + 1.050g K9 + 1.622g K16 + 1.050g K2
1321 2.000g E2 + 2.l00g K13 + 2.000g E6 + 2.100g Kl + 2.100g K11 + 1.622g K16
1322 0.200g E3 + 1.622g K16 + 0.210g K13 + 0.200g E6 + 0.210g K1 + 0.210g K14
CA 02646867 2008-12-16
W245FQ/JC 93
1323 2.000g E4 + 2.100g K13 + 1.622g K16 + 2.000g E6 + 2.100g Kl + 2.100g K24
1324 2.000g E1 + 2.100g K13 + 2.000g E6 + 1.622g K16 + 2.100g K1 + 2.100g K2
1325 2.000g E2 + 2.100g K13 + 2.000g E6 + 2.100g K11 + 1.622g K16 + 2.100g K14
1326 1.000g E3 + 1.050g K13 + 1.000g E6 + 1.050g K11 + 1.050g K24 + 1.622g K16
1327 1.000g E4 + 1.622g K16 + 1.050g K13 + 1.000g E6 + 1.050g K11 + 1.050g K2
1328 0.200g E1 + 0.210g K13 + 1.825g K16 + 0.200g E6 + 0.210g K14 + 0.210g K24
1329 1.000g E2 + 1.050g K13 + 1.000g E6 + 1.825g K16 + 1.050g K14 + 1.050g K2
1330 2.000g E3 + 2.100g K13 + 2.000g E6 + 2.100g K24 + 1.825g K16 + 2.100g K2
1331 2.500g E4 + 2.625g K13 + 2.500g E5 + 2.625g K12 + 1.825g K16
1332 1.250g E1 + 1.825g K16 + 1.313g K13 + 1.250g E5 + 1.313g K6
1333 1.250g E2 + 1.313g K13 + 1.825g K16 + 1.250g E5 + 1.313g K7
1334 1.250g E3 + 1.313g K13 + 1.250g E5 + 1.825g K16 + 1.313g K9
1335 1.250g E4 + 1.313g K13 + 1.250g E5 + 1.313g K1 + 1.825g K16
1336 1.250g El + 1.825g K16 + 1.313g K13 + 1.250g E5 + 1.313g K11
1337 2.500g E2 + 2.625g K13 + 1.825g K16 + 0.020g K3 + 2.500g E5 + 2.625g K14
1338 0.250g E3 + 0.263g K13 + 0.250g E5 + 1.825g K16 + 0.263g K24
1339 2.500g E4 + 2.625g K13 + 2.500g E5 + 2.625g K2 + 1.825g K16
1340 2.000g El + 1.825g K16 + 2.100g K13 + 2.000g E5 + 2.100g K12 + 2.100g K6
1341 2.000g E2 + 2.100g K13 + 1.825g K16 + 2.000g E5 + 2.100g K12 + 2.100g K7
1342 1.000g E3 + 1.050g K13 + 1.000g E5 + 1.825g K16 + 1.050g K12 + 1.050g K9
1343 1.000g E4 + 1.050g K13 + 1.000g E5 + 1.050g K12 + 1.825g K16 + 1.050g Kl
1344 0.200g E1 + 0.210g K13 + 0.200g E5 + 0.210g K12 + 0.210g K11 + 1.825g K16
1345 1.000g E2 + 1.825g K16 + 1.050g K13 + 1.000g E5 + 1.050g K12 + 1.050g K14
1346 1.000g E3 + 1.050g K13 + 1.825g K16 + 1.000g E5 + 1.050g K12 + 1.050g K24
1347 2.000g E4 + 2.100g K13 + 2.000g E5 + 1.825g K16 + 2.100g K12 + 2.100g K2
1348 2.000g El + 2.100g K13 + 2.000g E5 + 2.100g K6 + 1.825g K16 + 2.100g K7
1349 2.000g E2 + 2.100g K13 + 2.000g E5 + 2.100g K6 + 2.100g K9 + 1.825g K16
1350 0.200g E3 + 1.825g K16 + 0.210g K13 + 0.200g E5 + 0.210g K6 + 0.210g K1
1351 1.000g E4 + 1.050g K13 + 1.825g K16 + 1.000g E5 + 1.050g K6 + 1.050g Kl 1
1352 1.000g E1 + 1.050g K13 + 1.000g E5 + 1.825g K16 + 1.050g K6 + 1.050g K14
1353 1.000g E2 + 1.050g K13 + 1.000g E5 + 1.050g K6 + 1.825g K16 + 1.050g K24
1354 2.000g E3 + 2.100g K13 + 2.000g E5 + 2.100g K6 + 2.100g K2 + 1.825g K16
CA 02646867 2008-12-16
W245FQ/JC 94
1355 0.200g E4 + 1.825g K16 + 0.210g K13 + 0.200g E5 + 0.210g K7 + 0.210g K9
1356 1.000g El + 1.050g K13 + 1.825g K16 + 1.000g E5 + 1.050g K7 + 1.050g Kl
1357 2.000g E2 + 2.100g K13 + 2.000g E5 + 1.825g K16 + 2.100g K7 + 2.100g K11
1358 1.000g E3 + 1.050g K13 + 1.000g E5 + 1.050g K7 + 1.825g K16 + 1.050g K14
1359 1.000g E4 + 1.050g K13 + 1.000g E5 + 1.050g K7 + 1.050g K24 + 1.825g K16
1360 0.200g El + 1.825g K16 + 0.210g K13 + 0.200g E5 + 0.210g K7 + 0.210g K2
1361 0.200g E2 + 0.210g K13 + 1.825g K16 + 0.200g E5 + 0.210g K9 + 0.210g K1
1362 0.200g E3 + 0.210g K13 + 0.200g E5 + 1.825g K16 + 0.210g K9 + 0.210g K11
1363 2.000g E4 + 2.100g K13 + 2.000g E5 + 2.100g K9 + 1.825g K16 + 2.100g K14
1364 2.000g El + 2.100g K13 + 2.000g E5 + 2.100g K9 + 2.100g K24 + 1.825g K16
1365 1.000g E2 + 1.825g K16 + 1.050g K13 + 1.000g E5 + 1.050g K9 + 1.050g K2
1366 2.000g E3 + 2.100g K13 + 1.825g K16 + 2.000g E5 + 2.100g K1 + 2.100g K11
1367 2.000g E4 + 2.100g K13 + 2.000g E5 + 1.825g K16 + 2.100g K1 + 2.100g K14
1368 1.000g El + 1.050g K13 + 1.000g E5 + 1.050g Kl + 1.825g K16 + 1.050g K24
1369 1.000g E2 + 1.050g K13 + 1.000g E5 + 1.050g K1 + 1.050g K2 + 1.825g K16
1370 0.200g E3 + 1.825g K16 + 0.210g K13 + 0.200g E5 + 0.210g K11 + 0.210g K14
1371 0.200g E4 + 0.210g K13 + 1.825g K16 + 0.200g E5 + 0.210g K11 + 0.210g K24
1372 2.000g E1 + 2.100g K13 + 2.000g E5 + 1.825g K16 + 2.100g K11 + 2.100g K2
1373 2.000g E2 + 2.100g K13 + 2.000g E5 + 2.100g K14 + 1.825g K16 + 2.100g K24
1374 1.000g E3 + 1.050g K13 + 1.000g E5 + 1.050g K14 + 1.050g K2 + 1.825g K16
1375 0.200g E4 + 1.825g K16 + 0.210g K13 + 0.200g E5 + 0.210g K24 + 0.210g K2
1376 0.250g El + 0.263g K13 + 1.825g K16 + 0.250g E7 + 0.263g K12
1377 2.500g E2 + 2.625g K13 + 2.500g E7 + 1.825g K16 + 2.625g K6
1378 1.250g E3 + 1.313g K13 + 1.250g E7 + 1.313g K7 + 1.825g K16
1379 1.250g E4 + 1.825g K16 + 1.313g K13 + 1.250g E7 + 1.313g K9
1380 0.250g El + 0.263g K13 + 1.825g K16 + 0.250g E7 + 0.263g K1
1381 1.250g E2 + 1.313g K13 + 1.250g E7 + 1.825g K16 + 1.313g K11
1382 1.250g E3 + 1.313g K13 + 1.250g E7 + 1.313g K14 + 1.825g K16
1383 1.250g E4 + 1.825g K16 + 1.313g K13 + 1.250g E7 + 1.313g K24
1384 1.250g E1 + 1.313g K13 + 1.825g K16 + 1.250g E7 + 1.313g K2
1385 0.200g E2 + 0.210g K13 + 0.200g E7 + 1.825g K16 + 0.210g K12 + 0.210g K6
1386 0.200g E3 + 0.210g K13 + 0.200g E7 + 0.210g K12 + 1.825g K16 + 0.210g K7
CA 02646867 2008-12-16
W245FQ/JC 95
1387 1.000g E4 + 1.050g K13 + 1.000g E7 + 1.050g K12 + 1.050g K9 + 1.825g K16
1388 0.200g E1 + 1.825g K16 + 0.210g K13 + 0.200g E7 + 0.210g K12 + 0.210g K1
1389 2.000g E2 + 2.100g K13 + 1.825g K16 + 2.000g E7 + 2.100g K12 + 2.100g K11
1390 0.200g E3 + 0.210g K13 + 0.200g E7 + 1.825g K16 + 0.210g K12 + 0.210g K14
1391 0.200g E4 + 0.210g K13 + 0.200g E7 + 0.210g K12 + 1.825g K16 + 0.210g K24
1392 1.000g E1 + 1.050g K13 + 1.000g E7 + 1.050g K12 + 1.050g K2 + 1.825g K16
1393 0.200g E2 + 1.825g K16 + 0.210g K13 + 0.200g E7 + 0.210g K6 + 0.210g K7
1394 1.000g E3 + 1.050g K13 + 1.825g K16 + 1.000g E7 + l.050g K6 + 1.050g K9
1395 0.200g E4 + 0.210g K13 + 0.200g E7 + 1.825g K16 + 0.210g K6 + 0.210g K1
1396 1.000g El + l.050g K13 + 1.000g E7 + 1.050g K6 + 1.825g K16 + l.050g Kl 1
1397 1.000g E2 + 1.050g K13 + 1.000g E7 + 1.050g K6 + 1.050g K14 + 1.825g K16
1398 1.000g E3 + 1.825g K16 + 1.050g K13 + 1.000g E7 + 1.050g K6 + 1.050g K24
1399 0.200g E4 + 0.210g K13 + 1.825g K16 + 0.200g E7 + 0.210g K6 + 0.210g K2
1400 0.200g E1 + 0.210g K13 + 0.200g E7 + 1.825g K16 + 0.210g K21 + 0.210g K9
1401 1.000g E2 + 1.050g K13 + 1.000g E7 + 1.050g K7 + 1.825g K16 + 1.050g K1
1402 2.000g E3 + 2.100g K13 + 2.000g E7 + 2.100g K7 + 2.100g K11 + 1.825g K16
1403 1.000g E4 + 1.825g K16 + 1.050g K13 + 1.000g E7 + 1.050g K7 + 1.050g K14
1404 0.200g El + 0.210g K13 + 1.825g K16 + 0.200g E7 + 0.210g K7 + 0.210g K24
1405 2.000g E2 + 2.100g K13 + 2.000g E7 + 1.825g K16 + 2.100g K8 + 2.100g K2
1406 1.000g E3 + 1.050g K13 + 1.000g E7 + 1.050g K9 + 1.825g K16 + 1.050g K1
1407 0.200g E4 + 0.210g K13 + 0.200g E7 + 0.210g K9 + 0.210g K11 + 1.825g K16
1408 1.000g El + 1.825g K16 + 1.050g K13 + 1.000g E7 + 1.050g K9 + 1.050g K14
1409 1.000g E2 + 1.050g K13 + 1.825g K16 + 1.000g E7 + 1.050g K9 + 1.050g K24
1410 2.000g E3 + 2.100g K13 + 2.000g E7 + 1.825g K16 + 2.l00g K9 + 2.100g K2
1411 1.000g E4 + 1.050g K13 + 1.000g E7 + 1.050g Kl + 1.825g K16 + 1.050g Kl l
1412 2.000g El + 2.100g K13 + 2.000g E7 + 2.100g K1 + 2.l00g K14 + 1.825g K16
1413 1.000g E2 + 1.825g K16 + 1.050g K13 + 1.000g E7 + 1.050g K1 + 1.050g K24
1414 0.200g E3 + 0.210g K13 + 1.825g K16 + 0.200g E7 + 0.210g Kl + 0.210g K2
1415 2.000g E4 + 2.100g K13 + 2.000g E7 + 1.825g K16 + 2.100g K11 + 2.100g K14
1416 1.000g El + 1.050g K13 + 1.000g E7 + 1.050g K11 + 1.825g K16 + 1.050g K24
1417 1.000g E2 + 1.050g K13 + 1.000g E7 + 1.050g K1 l+ 1.050g K2 + 1.825g K16
1418 1.000g E3 + 0.028g K16 + 1.050g K13 + 1.000g E7 + 1.050g K14 + 1.050g K24
CA 02646867 2008-12-16
W245FQ/JC 96
1419 2.000g E4 + 2.100g K13 + 0.028g K16 + 2.000g E7 + 2.100g K14 + 2.100g K2
1420 1.000g E1 + 1.050g K13 + 1.000g E7 + 0.028g K16 + 1.050g K24 + 1.050g K2
1421 3.333g E2 + 3.500g K13 + 3.500g K12 + 0.028g K16
1422 1.250g E3 + 0.028g K16 + 1.313g K13 + 1.313g K12 + 1.313g K6
1423 0.250g E4 + 0.263g K13 + 0.028g K16 + 0.263g K12 + 0.263g K7
1424 1.250g El + 1.313g K13 + 1.313g K12 + 0.028g K16 + 1.313g K9
1425 2.500g E2 + 2.625g K13 + 2.625g K12 + 2.625g K1 + 0.028g K16
1426 2.500g E3 + 0.028g K16 + 2.625g K13 + 2.625g K12 + 2.625g K11
1427 0.250g E4 + 0.263g K13 + 0.028g K16 + 0.263g K12 + 0.263g K14
1428 1.250g El + 1.313g K13 + 1.313g K12 + 0.028g K16 + 1.313g K24
1429 1.250g E2 + 1.313g K13 + 1.313g K12 + 1.313g K2 + 0.028g K16
1430 2.000g E3 + 0.028g K16 + 2.100g K13 + 2.100g K12 + 2.100g K6 + 2.100g K7
1431 1.000g E4 + 1.050g K13 + 0.028g K16 + 1.050g K12 + 1.050g K6 + 1.050g K9
1432 0.200g E1 + 0.210g K13 + 0.210g K12 + 0.028g K16 + 0.210g K6 + 0.210g K1
1433 2.000g E2 + 2.l00g K13 + 2.l00g K12 + 2. l00g K6 + 0.028g K16 + 2.l00g
K11
1434 2.000g E3 + 2.100g K13 + 2.l00g K12 + 2. l00g K6 + 2.l00g K14 + 0.028g
K16
1435 2.000g E4 + 0.028g K16 + 2.100g K13 + 2.100g K12 + 2.100g K6 + 2.100g K24
1436 2.000g E1 + 2.100g K13 + 0.028g K16 + 2.100g K12 + 2.100g K6 + 2.100g K2
1437 0.200g E2 + 0.210g K13 + 0.2lOg K12 + 0.028g K16 + 0.210g K7 + 0.210g K9
1438 2.000g E3 + 2.100g K13 + 2.100g K12 + 2.100g K7 + 0.028g K16 + 2.100g K1
1439 0.200g E4 + 0.210g K13 + 0.210g K12 + 0.210g K7 + 0.210g K11 + 0.028g K16
1440 2.000g E1 + 0.028g K16 + 2.100g K13 + 2.100g K12 + 2.100g K7 + 2.100g K14
1441 2.000g E2 + 2.100g K13 + 0.028g K16 + 2.100g K12 + 2.100g K7 + 2.100g K24
1442 1.000g E3 + 1.050g K13 + 1.050g K12 + 0.028g K16 + 1.050g K7 + 1.050g K2
1443 2.000g E4 + 2.100g K13 + 2.100g K12 + 2.100g K9 + 0.028g K16 + 2.100g K1
1444 1.000g E1 + 1.050g K13 + 1.050g K12 + 1.050g K9 + 1.050g Kl l+ 0.028g K16
1445 1.000g E2 + 0.028g K16 + 1.050g K13 + 1.050g K12 + 1.050g K9 + 1.050g K14
1446 2.000g E3 + 2.100g K13 + 0.028g K16 + 2.100g K12 + 2.100g K9 + 2.100g K24
1447 2.000g E4 + 2.100g K13 + 2.100g K12 + 0.028g K16 + 2.100g K9 + 2.100g K2
1448 0.200g El + 0.210g K13 + 0.210g K12 + 0.210g K1 + 0.028g K16 + 0.210g K11
1449 2.000g E2 + 2.100g K13 + 2.l00g K12 + 2.100g Kl + 2.100g K14 + 0.028g K16
1450 2.000g E3 + 0.028g K16 + 2. l00g K13 + 2. l00g K12 + 2.l00g K1 + 2.100g
K24
CA 02646867 2008-12-16
W245FQ/JC 97
1451 2.000g E4 + 2.100g K13 + 0.028g K16 + 2.100g K12 + 2.100g K1 + 2.100g K2
1452 2.000g E1 + 2.100g K13 + 2.100g K12 + 0.028g K16 + 2.100g K11 + 2.100g
K14
1453 2.000g E2 + 2.100g K13 + 2.100g K12 + 2.100g K11 + 0.028g K16 + 2.100g
K24
1454 1.000g E3 + 1.050g K13 + 1.050g K12 + 1.050g K11 + 1.050g K2 + 0.028g K16
1455 1.000g E4 + 0.028g K16 + 1.050g K13 + 1.050g K12 + 1.050g K14 + 1.050g
K24
1456 0.200g E1 + 0.210g K13 + 0.028g K16 + 0.210g K12 + 0.210g K14 + 0.210g K2
1457 1.000g E2 + 1.050g K13 + 1.050g K12 + 0.028g K16 + 1.050g K24 + 1.050g K2
1458 3.333g E3 + 3.500g K13 + 3.500g K6 + 0.028g K16
1459 0.250g E4 + 0.028g K16 + 0.263g K13 + 0.263g K6 + 0.263g K7
1460 0.250g El + 0.263g K13 + 0.028g K16 + 0.263g K6 + 0.263g K9
1461 1.250g E2 + 1.313g K13 + 1.313g K6 + 0.028g K16 + 1.313g K1
1462 2.500g E3 + 2.625g K13 + 2.625g K6 + 2.625g K11 + 0.028g K16
1463 0.250g E4 + 0.028g K16 + 0.263g K13 + 0.263g K6 + 0.263g K14
1464 2.500g El + 2.625g K13 + 0.028g K16 + 0.068g K3 + 2.625g K6 + 2.625g K24
1465 2.500g E2 + 2.625g K13 + 2.625g K6 + 0.028g K16 + 2.625g K2
1466 1.000g E3 + 1.050g K13 + 1.050g K6 + 1.050g K7 + 0.028g K16 + 1.050g K9
1467 2.000g E4 + 2.100g K13 + 2.100g K6 + 2.100g K7 + 2.100g K1 + 0.028g K16
1468 0.200g El + 0.028g K16 + 0.210g K13 + 0.210g K6 + 0.210g K7 + 0.210g K11
1469 1.000g E2 + 1.050g K13 + 0.028g K16 + 1.050g K6 + 1.050g K7 + 1.050g K14
1470 2.000g E3 + 2.100g K13 + 2.100g K6 + 0.028g K16 + 2.100g K7 + 2.100g K24
1471 0.200g E4 + 0.210g K13 + 0.210g K6 + 0.210g K7 + 0.028g K16 + 0.210g K2
1472 0.200g E1 + 0.210g K13 + 0.210g K6 + 0.210g K9 + 0.210g K1 + 0.028g K16
1473 1.000g E2 + 0.028g K16 + 1.050g K13 + 1.050g K6 + 1.050g K9 + 1.050g K11
1474 2.000g E3 + 2.100g K13 + 0.028g K16 + 2.l00g K6 + 2.l00g K9 + 2.l00g K14
1475 0.200g E4 + 0.210g K13 + 0.210g K6 + 0.028g K16 + 0.210g K9 + 0.210g K24
1476 1.000g El + 1.050g K13 + 1.050g K6 + 1.050g K9 + 0.028g K16 + 1.050g K2
1477 0.200g E2 + 0.210g K13 + 0.210g K6 + 0.210g K1 + 0.210g K11 + 0.028g K16
1478 0.200g E3 + 0.028g K16 + 0.210g K13 + 0.210g K6 + 0.210g K1 + 0.210g K14
1479 2.000g E4 + 2.100g K13 + 0.028g K16 + 2.100g K6 + 2.100g K1 + 2.100g K24
1480 0.200g E1 + 0.210g K13 + 0.210g K6 + 0.028g K16 + 0.210g K1 + 0.210g K2
1481 0.200g E2 + 0.210g K13 + 0.210g K6 + 0.210g K11 + 0.028g K16 + 0.210g K14
1482 2.000g E3 + 2.100g K13 + 2. l00g K6 + 2. l00g Kl 1+ 2.100g K24 + 0.028g
K16
CA 02646867 2008-12-16
W245FQ/JC 98
1483 2.000g E4 + 0.028g K16 + 2.100g K13 + 2.100g K6 + 2.100g K11 + 2.100g K2
1484 2.000g E1 + 2.100g K13 + 0.028g K16 + 2.100g K6 + 2.100g K14 + 2.100g K24
1485 2.000g E2 + 2.l00g K13 + 2.100g K6 + 0.028g K16 + 2.100g K14 + 2.100g K2
1486 2.000g E3 + 2.100g K13 + 2.100g K6 + 2.100g K24 + 0.028g K16 + 2.100g K2
1487 3.333g E4 + 3.500g K13 + 3.500g K21 + 0.028g K16
1488 1.250g E1 + 0.028g K16 + 1.313g K13 + 1.313g K7 + 1.313g K9
1489 1.250g E2 + 1.313g K13 + 0.028g K16 + 1.313g K7 + 1.313g K1
1490 2.500g E3 + 2.625g K13 + 2.625g K7 + 0.028g K16 + 2.625g K11
1491 1.250gE4+ 1.313gK13+ 1.313gK7+ 1.313gK14+0.028gK16
1492 2.500g E1 + 0.028g K16 + 2.625g K13 + 2.625g K7 + 2.625g K24
1493 1.250gE2+1.313gK13+0.028gK16+1.313gK8+1.313gK2
1494 2.000g E3 + 2.100g K13 + 2.100g K7 + 0.028g K16 + 2.100g K9 + 2.100g K1
1495 1.000g E4 + 1.050g K13 + 1.050g K7 + 1.050g K9 + 0.028g K16 + 1.050g K11
1496 1.000g El + 1.050g K13 + 1.050g K7 + 1.050g K9 + 1.050g K14 + 0.028g K16
1497 0.200g E2 + 0.028g K16 + 0.210g K13 + 0.210g K7 + 0.210g K9 + 0.210g K24
1498 1.000g E3 + 1.050g K13 + 0.028g K16 + 1.050g K7 + 1.050g K9 + 1.050g K2
1499 2.000g E4 + 2.100g K13 + 2.100g K7 + 0.028g K16 + 2.100g K1 + 2.100g K11
1500 0.200gE1+0.210gK13+0.210gK7+0.210gK1+0.028gK16+0.210gK14
1501 2.000g E2 + 2.100g K13 + 2.100g K7 + 2.100g K1 + 2.100g K24 + 0.028g K16
1502 1.000g E3 + 0.028g K16 + 1.050g K13 + 1.050g K7 + 1.050g K1 + 1.050g K2
1503 0.200gE4+0.210gK13+0.028gK16+0.210gK7+0.210gK11 +0.210gK14
1504 1.000g El + 1.050g K13 + 1.050g K7 + 0.028g K16 + 1.050g Kl l+ 1.050g K24
1505 0.200g E2 + 0.210g K13 + 0.210g K7 + 0.210g K11 + 0.028g K16 + 0.210g K2
1506 2.000g E3 + 2.100g K13 + 2.100g K7 + 2.100g K14 + 2.100g K24 + 0.028g K16
1507 2.000g E4 + 0.028g K16 + 2.100g K13 + 2.100g K7 + 2.100g K14 + 2.100g K2
1508 0.200g E1 + 0.210g K13 + 0.231g K16 + 0.210g K21 + 0.210g K24 + 0.210g K2
1509 3.333g E2 + 3.500g K13 + 3.500g K9 + 0.231g K16
1510 2.500g E3 + 0.231g K16 + 2.625g K13 + 2.625g K9 + 2.625g K1
1511 2.500g E4 + 2.625g K13 + 0.231g K16 + 2.625g K9 + 2.625g K11
1512 2.500g E1 + 2.625g K13 + 2.625g K9 + 0.231g K16 + 2.625g K14
1513 1.250gE2+1.313gK13+1.313gK9+1.313gK24+0.231gK16
1514 0.250gE3+0.231gK16+0.263gK13+0.263gK9+0.263gK2
CA 02646867 2008-12-16
W245FQ/JC 99
1515 1.000g E4 + 1.050g K13 + 0.231g K16 + 1.050g K9 + 1.050g Kl + 1.050g Kl 1
1516 0.200gEl +0.210gK13+0.210gK9+0.231gK16+0.210gK1 +0.210gK14
1517 0.200gE2+0.210gK13+0.210gK9+0.210gK1 +0.231gK16+0.210gK24
1518 1.000g E3 + 1.050g K13 + 1.050g K9 + 1.050g K1 + 1.050g K2 + 0.231g K16
1519 0.200gE4+0.231gK16+0.210gK13+0.210gK9+0.210gK11 +0.210gK14
1520 0.200g E1 + 0.210g K13 + 0.231g K16 + 0.210g K9 + 0.210g K11 + 0.210g K24
1521 2.000g E2 + 2.100g K13 + 2.100g K9 + 0.231g K16 + 2.100g K11 + 2.100g K2
1522 2.000g E3 + 2.100g K13 + 2.100g K9 + 2.100g K14 + 0.231g K16 + 2.100g K24
1523 1.000g E4 + 1.050g K13 + 1.050g K9 + 1.050g K14 + 1.050g K2 + 0.231g K16
1524 0.200gE1+0.231gK16+0.210gK13+0.210gK9+0.210gK24+0.210gK2
1525 2.500g E1 + 2.625g K13 + 0.231g K16
1526 1.667g E3 + 0.231g K16 + 1.750g K13 + 1.750g K1
1527 1.667g E4 + 1.750g K13 + 0.231g K16 + 1.750g K11
1528 3.333g E1 + 3.500g K13 + 3.500g K14 + 0.231g K16
1529 1.667g E2 + 0.231g K16 + 1.750g K13 + 1.750g K24
1530 3.333g E3 + 3.500g K13 + 0.231g K16 + 3.500g K2
1531 2.500g E4 + 2.625g K13 + 2.625g K5 + 0.231g K16 + 2.625g K11
1532 2.500g El + 2.625g K13 + 1.625g Kl + 1.025g K5 + 2.625g K14 + 0.231g K16
1533 0.250g E2 + 0.231g K16 + 0.263g K13 + 0.263g K1 + 0.263g K24
1534 1.250g E3 + 1.313g K13 + 0.231g K16 + 1.313g K1 + 1.313g K2
1535 2.500g E4 + 2.625g K13 + 2.625g K11 + 0.231g K16 + 2.625g K14
1536 2.500g El + 2.625g K13 + 2.625g K11 + 2.625g K24 + 0.231g K16
1537 1.250gE2+0.231gK16+1.313gK13+1.313gK11+1.313gK2
1538 0.250g E3 + 0.263g K13 + 0.231g K16 + 0.263g K14 + 0.263g K24
1539 1.250gE4+1.313gK13+1.313gK14+0.231gK16+1.313gK2
1540 1.250gE1+1.313gK13+1.313gK24+1.313gK2+0.231gK16
1541 1.000g E2 + 0.231g K16 + 1.050g K13 + 1.050g K1 + 1.050g K11 + 1.050g K14
1542 2.000g E3 + 2.100g K13 + 0.23lg K16 + 2.100g K1 + 2.100g K11 + 2.100g K24
1543 2.000g E4 + 2.100g K13 + 2.100g K1 + 0.231g K16 + 2.100g K11 + 2.100g K2
1544 0.200g E1 + 0.210g K13 + 0.210g K1 + 0.210g K14 + 0.231g K16 + 0.210g K24
1545 1.000g E2 + 1.050g K13 + 1.050g K1 + 1.050g K14 + 1.050g K2 + 0.231g K16
1546 2.000g E3 + 0.23lg K16 + 2.100g K13 + 2.100g K1 + 2.100g K24 + 2.100g K2
CA 02646867 2008-12-16
W245FQ/JC 100
1547 0.200g E4 + 0.210g K13 + 0.23lg K16 + 0.210g K11 + 0.210g K14 + 0.210g
K24
1548 2.000g E1 + 2.100g K13 + 2.100g K11 + 0.231g K16 + 2.100g K14 + 2.100g K2
1549 2.000g E2 + 2.100g K13 + 2.100g K11 + 2.100g K24 + 0.231g K16 + 2.100g K2
1550 1.000g E3 + 1.050g K13 + 1.050g K14 + 1.050g K24 + 1.050g K2 + 0.231g K16
1551 2.500g E4 + 0.231g K16 + 2.625g Ki + 2.500g E8 + 2.625g K12
1552 0.250g El + 0.263g Kl + 0.231g K16 + 0.250g E8 + 0.263g K6
1553 0.250g E2 + 0.263g K1 + 0.250g E8 + 0.231g K16 + 0.263g K7
1554 1.250g E3 + 1.313g K1 + 1.250g E8 + 1.313g K9 + 0.231g K16
1555 1.250g E4 + 0.231g K16 + 1.313g Kl + 1.250g E8 + 1.313g K13
1556 2.500g El + 2.625g K1 + 0.231g K16 + 2.500g E8 + 2.625g K11
1557 2.500g E2 + 2.625g Kl + 2.500g E8 + 0.231g K16 + 2.625g K14
1558 0.250g E3 + 0.263g Kl + 0.250g E8 + 0.263g K24 + 0.231g K16
1559 1.250g E4 + 0.23lg K16 + 1.313g K1 + 1.250g E8 + 1.313g K2
1560 0.200g El + 0.210g Kl + 0.231g K16 + 0.200g E8 + 0.210g K12 + 0.210g K6
1561 0.200gE2+0.210gK1 +0.200gE8+0.231gK16+0.210gK12+0.210gK7
1562 0.200g E3 + 0.210g K1 + 0.200g E8 + 0.210g K12 + 0.231g K16 + 0.210g K9
1563 1.000g E4 + 1.050g K1 + 1.000g E8 + 1.050g K12 + 1.050g K13 + 0.231g K16
1564 1.000g El + 0.231g K16 + 1.050g Kl + 1.000g E8 + 1.050g K12 + 1.050g Kl 1
1565 1.000g E2 + 1.050g Kl + 0.231g K16 + 1.000g E8 + 1.050g K12 + 1.050g K14
1566 2.000g E3 + 2.100g K1 + 2.000g E8 + 0.231g K16 + 2.100g K12 + 2.100g K24
1567 2.000g E4 + 2.100g K1 + 2.000g E8 + 2.100g K12 + 0.231g K16 + 2.100g K2
1568 0.200g El + 0.210g K1 + 0.200g E8 + 0.210g K6 + 0.210g K7 + 0.231g K16
1569 2.000g E2 + 0.231 g K16 + 2.100g K1 + 2.000g E8 + 2.100g K6 + 2.100g K9
1570 1.000g E3 + 1.050g Kl + 0.231g K16 + 1.000g E8 + 1.050g K6 + 1.050g K13
1571 2.000g E4 + 2.100g K1 + 2.000g E8 + 0.231g K16 + 2.100g K6 + 2.100g K11
1572 0.200gEl +0.210gK1 +0.200gE8+0.210gK6+0.231gK16+0.210gK14
1573 1.000g E2 + 1.050g Kl + 1.000g E8 + 1.050g K6 + 1.050g K24 + 0.231g K16
1574 0.200g E3 + 0.231g K16 + 0.210g Kl + 0.200g E8 + 0.210g K6 + 0.210g K2
1575 1.000g E4 + 1.050g Kl + 0.231g K16 + 1.000g E8 + 1.050g K7 + l.050g K9
1576 1.000g El + l.050g K1 + 1.000g E8 + 0.231g K16 + 1.050g K7 + l.050g K22
1577 0.200gE2+0.210gK1+0.200gE8+0.210gK7+0.231gK16+0.210gK11
1 1578 0.200g E3 + 0.210g Kl + 0.200g E8 + 0.210g K8 + 0.210g K14 + 0.231g K16
CA 02646867 2008-12-16
W245FQ/JC 101
1579 1.000g E4 + 0.231g K16 + 1.050g K1 + 1.000g E8 + 1.050g K7 + 1.050g K24
1580 1.000g El + 1.050g Kl + 0.231g K16 + 1.000g E8 + 1.050g K7 + 1.050g K2
1581 2.000gE2+2.100gK1 +2.000gE8+0.231gK16+2.100gK9+2.100gK13
1582 1.000g E3 + 1.050g K1 + 1.000g E8 + 1.050g K9 + 0.231g K16 + 1.050g K11
1583 1.000g E4 + 1.050g K1 + 1.000g E8 + 1.050g K9 + 1.050g K14 + 0.231g K16
1584 1.000g El + 0.231g K16 + 1.050g K1 + 1.000g E8 + 1.050g K9 + 1.050g K24
1585 1.000g E2 + 1.050g Kl + 0.231g K16 + 1.000g E8 + 1.050g K9 + 1.050g K2
1586 1.000g E3 + 1.050g Kl + 1.000g E8 + 0.434g K16 + 1.050g K13 + 1.050g K11
1587 1.000g E4 + 1.050g K1 + 1.000g E8 + 1.050g K13 + 0.434g K16 + 1.050g K14
1588 0.200g El + 0.210g K1 + 0.200g E8 + 0.210g K13 + 0.210g K24 + 0.434g K16
1589 2.000g E2 + 0.434g K16 + 2.100g K1 + 2.000g E8 + 2. l00g K13 + 2.100g K2
1590 2.000g E3 + 2.100g Kl + 0.434g K16 + 2.000g E8 + 2.100g K11 + 2.100g K14
1591 0.200g E4 + 0.210g K1 + 0.200g E8 + 0.434g K16 + 0.210g K11 + 0.210g K24
1592 0.200g El + 0.210g K1 + 0.200g E8 + 0.210g K11 + 0.434g K16 + 0.210g K2
1593 0.200g E2 + 0.210g K1 + 0.200g E8 + 0.210g K14 + 0.210g K24 + 0.434g K16
1594 1.000g E3 + 0.434g K16 + 1.050g K1 + 1.000g E8 + 1.050g K14 + 1.050g K2
1595 2.000g E4 + 2.100g K1 + 0.434g K16 + 2.000g E8 + 2.100g K24 + 2.100g K2
1596 0.250g El + 0.263g K1 + 0.250g E6 + 0.434g K16 + 0.263g K12
1597 0.250g E2 + 0.263g Kl + 0.250g E6 + 0.263g K6 + 0.434g K16
1598 0.250g E3 + 0.434g K16 + 0.263g K1 + 0.250g E6 + 0.263g K7
1599 1.250g E4 + 1.313g Kl + 0.434g K16 + 1.250g E6 + 1.313g K9
1600 1.250g El + 1.313g Kl + 1.250g E6 + 0.434g K16 + 1.313g K13
1601 0.250g E2 + 0.263g K1 + 0.250g E6 + 0.263g Kl 1+ 0.434g K16
1602 2.500g E3 + 0.434g K16 + 2.625g KI + 2.500g E6 + 2.625g K14
1603 1.250g E4 + 1.313g K1 + 0.434g K16 + 1.250g E6 + 1.313g K24
1604 1.250g El + 1.313g K1 + 1.250g E6 + 0.434g K16 + 1.313g K2
1605 1.000g E2 + 0.750g K1 + 0.500g K4 + 1.000g E6 + 1.050g K12 + 0.434g K16 +
1.050g K6
1606 1.000g E3 + 1.050g K1 + 1.000g E6 + 1.050g K12 + 1.050g K7 + 0.434g K16
1607 1.000g E4 + 0.434g K16 + 1.050g K1 + 1.000g E6 + 1.050g K12 + 1.050g K9
1608 2.000g E1 + 2.100g K1 + 0.434g K16 + 2.000g E6 + 2.100g K12 + 2.100g K13
1609 1.000g E2 + 1.050g K1 + 1.000g E6 + 0.434g K16 + 1.050g K12 + 1.050g Kl 1
CA 02646867 2008-12-16
W245FQ/JC 102
1610 0.200g E3 + 0.210g K1 + 0.200g E6 + 0.210g K12 + 0.434g K16 + 0.210g K14
1611 1.000g E4 + 1.050g K1 + 1.000g E6 + 1.050g K12 + 1.050g K24 + 0.434g K16
1612 2.000g El + 0.434g K16 + 2.100g K1 + 2.000g E6 + 2.100g K12 + 2.100g K2
1613 1.000g E2 + 1.050g K1 + 0.434g K16 + 1.000g E6 + 1.050g K6 + 1.050g K7
1614 1.000g E3 + 1.050g Kl + 1.000g E6 + 0.434g K16 + 1.050g K6 + 1.050g K9
1615 0.200g E4 + 0.210g K1 + 0.200g E6 + 0.210g K6 + 0.434g K16 + 0.210g K13
1616 1.000g E1 + 1.050g Kl + 1.000g E6 + 1.050g K6 + 1.050g K11 + 0.434g K16
1617 2.000g E2 + 0.434g K16 + 2.100g K1 + 2.000g E6 + 2.100g K6 + 2.100g K14
1618 1.000g E3 + 1.050g K1 + 0.434g K16 + 1.000g E6 + 1.050g K6 + 1.050g K24
1619 0.200g E4 + 0.210g K1 + 0.200g E6 + 0.434g K16 + 0.210g K6 + 0.210g K2
1620 1.000g El + 1.050g Kl + 1.000g E6 + 1.050g K7 + 0.434g K16 + 1.050g K9
1621 1.000g E2 + 1.050g K1 + 1.000g E6 + 1.050g K7 + 1.050g K13 + 0.434g K16
1622 0.200g E3 + 0.434g K16 + 0.210g K1 + 0.200g E6 + 0.210g K7 + 0.210g K11
1623 1.000g E4 + 1.050g K1 + 0.434g K16 + 1.000g E6 + 1.050g K7 + 1.050g K14
1624 0.200g El + 0.210g K1 + 0.200g E6 + 0.434g K16 + 0.210g K7 + 0.210g K24
1625 1.000g E2 + 1.050g K1 + 1.000g E6 + 1.050g K7 + 0.434g K16 + 1.050g K2
1626 2.000g E3 + 2.100g K1 + 2.000g E6 + 2.100g K9 + 2.100g K13 + 0.434g K16
1627 2.000g E4 + 0.434g K16 + 2.100g K1 + 2.000g E6 + 2.100g K9 + 2.100g K11
1628 0.200g El + 0.210g K1 + 0.434g K16 + 0.200g E6 + 0.210g K9 + 0.210g K14
1629 2.000g E2 + 2.100g K1 + 2.000g E6 + 0.434g K16 + 2.100g K9 + 2.100g K24
1630 2.000g E3 + 2.100g K1 + 2.000g E6 + 2.100g K9 + 0.434g K16 + 2.100g K2
1631 2.000g E4 + 2.100g Kl + 2.000g E6 + 2.100g K13 + 2.100g K11 + 0.434g K16
1632 1.000g El + 0.434g K16 + 1.050g K1 + 1.000g E6 + 1.050g K13 + 1.050g K14
1633 1.000g E2 + 1.050g Kl + 0.434g K16 + 1.000g E6 + 1.050g K13 + 1.050g K24
1634 1.000g E3 + 1.050g Kl + 1.000g E6 + 0.434g K16 + 1.050g K13 + 1.050g K2
1635 0.200g E4 + 0.210g K1 + 0.200g E6 + 0.210g K11 + 0.434g K16 + 0.210g K14
1636 1.000g El + 1.050g Ki + 1.000g E6 + 1.050g K11 + 1.050g K24 + 0.434g K16
1637 0.200g E2 + 0.434g K16 + 0.210g K1 + 0.200g E6 + 0.210g K11 + 0.210g K2
1638 0.200g E3 + 0.210g Kl + 0.434g K16 + 0.200g E6 + 0.210g K14 + 0.210g K24
1639 1.000g E4 + 1.050g K1 + 1.000g E6 + 0.434g K16 + 1.050g K14 + 1.050g K2
1640 1.000g El + 1.050g Kl + 1.000g E6 + 1.050g K24 + 0.434g K16 + 1.050g K2
1641 1.250g E2 + 1.313g K1 + 1.250g E5 + 1.313g K12 + 0.434g K16
CA 02646867 2008-12-16
W245FQ/JC 103
1642 1.250g E3 + 0.434g K16 + 1.313g K1 + 1.250g E5 + 1.313g K6
1643 2.500g E4 + 2.625g K1 + 0.434g K16 + 2.500g E5 + 2.625g K7
1644 0.250g El + 0.263g K1 + 0.250g E5 + 0.434g K16 + 0.263g K9
1645 2.500g E2 + 2.625g Kl + 2.500g E5 + 2.625g K13 + 0.434g K16
1646 1.250g E3 + 0.434g K16 + 1.313g K1 + 1.250g E5 + 1.313g K11
1647 2.500g E4 + 2.625g K1 + 0.434g K16 + 2.500g E5 + 2.625g K14
1648 2.500g El + 2.625g Kl + 2.500g E5 + 0.434g K16 + 2.625g K24
1649 1.250g E2 + 1.313g Kl + 1.250g E5 + 1.313g K2 + 0.434g K16
1650 1.000g E3 + 0.434g K16 + 1.050g K1 + 1.000g E5 + 1.050g K12 + 1.050g K6
1651 0.200g E4 + 0.210g K1 + 0.434g K16 + 0.200g E5 + 0.210g K12 + 0.210g K7
1652 1.000g El + 1.050g K1 + 1.000g E5 + 0.434g K16 + 1.050g K12 + 1.050g K9
1653 2.000g E2 + 2.100g K1 + 2.000g E5 + 2.100g K12 + 0.434g K16 + 2.100g K13
1654 2.000g E3 + 2.100g K1 + 2.000g E5 + 2.100g K12 + 2.100g K11 + 0.434g K16
1655 2.000g E4 + 0.434g K16 + 2.100g K1 + 2.000g E5 + 2.100g K12 + 2.100g K14
1656 2.000g El + 2.100g Kl + 0.434g K16 + 2.000g E5 + 2.100g K12 + 2.100g K24
1657 1.000g E2 + 1.050g K1 + 1.000g E5 + 0.434g K16 + 1.050g K12 + 1.050g K2
1658 1.000g E3 + 1.050g K1 + 1.000g E5 + 1.050g K6 + 0.434g K16 + 1.050g K21
1659 0.200g E4 + 0.210g Kl + 0.200g E5 + 0.210g K6 + 0.210g K9 + 0.434g K16
1660 2.000g El + 0.434g K16 + 2.100g K1 + 2.000g E5 + 2.100g K6 + 2.100g K13
1661 0.200g E2 + 0.210g K1 + 0.434g K16 + 0.200g E5 + 0.210g K6 + 0.210g Kl 1
1662 0.200g E3 + 0.210g K1 + 0.200g E5 + 0.434g K16 + 0.210g K6 + 0.210g K14
1663 2.000g E4 + 2.100g K1 + 2.000g E5 + 2.100g K6 + 0.434g K16 + 2.100g K24
1664 1.000g El + 1.050g K1 + 1.000g E5 + 1.050g K6 + 1.050g K2 + 0.434g K16
1665 0.200g E2 + 0.434g K16 + 0.210g Kl + 0.200g E5 + 0.210g K7 + 0.210g K9
1666 0.200g E3 + 0.210g K1 + 0.434g K16 + 0.200g E5 + 0.210g K7 + 0.210g K13
1667 0.200g E4 + 0.210g K1 + 0.200g E5 + 0.434g K16 + 0.210g K7 + 0.210g K11
1668 1.000g El + 1.050g K1 + 1.000g E5 + 1.050g K7 + 0.434g K16 + 1.050g K14
1669 2.000g E2 + 2.100g K1 + 2.000g E5 + 2.100g K7 + 2.100g K24 + 0.434g K16
1670 1.000g E3 + 0.434g K16 + 1.050g K1 + 1.000g E5 + 1.050g K7 + 1.050g K2
1671 0.200g E4 + 0.210g K1 + 0.434g K16 + 0.200g E5 + 0.210g K9 + 0.210g K13
1672 0.200g El + 0.2lOg K1 + 0.200g E5 + 0.434g K16 + 0.2lOg K9 + 0.210g Kl 1
1673 2.000g E2 + 2.100g Kl + 2.000g E5 + 2.100g K9 + 0.434g K16 + 2.100g K14
CA 02646867 2008-12-16
W245FQ/JC 104
1674 1.000g E3 + 1.050g KI + 1.000g E5 + 1.050g K9 + 1.050g K24 + 0.434g K16
1675 2.000g E4 + 0.434g K16 + 2.100g K1 + 2.000g E5 + 2.100g K9 + 2.100g K2
1676 2.000g E1 + 2.100g K1 + 1.636g K16 + 2.000g E5 + 2.100g K13 + 2.100g K11
1677 1.000g E2 + 1.050g K1 + 1.000g E5 + 1.636g K16 + 1.050g K13 + 1.050g K14
1678 2.000g E3 + 2.100g K1 + 2.000g E5 + 2.100g K13 + 1.636g K16 + 2.100g K24
1679 1.000g E4 + 1.050g Kl + 1.000g E5 + 1.050g K13 + 1.050g K2 + 1.636g K16
1680 1.000g El + 1.636g K16 + 1.050g K1 + 1.000g E5 + 1.050g K11 + 1.050g K14
1681 0.200gE2+0.210gK1 + 1.636gK16+0.200gE5+0.210gK11 +0.210gK24
1682 0.200g E3 + 0.210g K1 + 0.200g E5 + 1.636g K16 + 0.210g K11 + 0.210g K2
1683 0.200g E4 + 0.210g K1 + 0.200g E5 + 0.210g K14 + 1.636g K16 + 0.210g K24
1684 1.000g E1 + 1.050g Kl + 1.000g E5 + 1.050g K14 + 1.050g K2 + 1.636g K16
1685 2.000g E2 + 1.636g K16 + 2.100g K1 + 2.000g E5 + 2.100g K24 + 2.100g K2
1686 2.500g E3 + 2.625g K1 + 1.636g K16 + 2.500g E7 + 2.625g K12
1687 0.250g E4 + 0.263g K1 + 0.250g E7 + 1.636g K16 + 0.263g K6
1688 0.250g El + 0.263g K1 + 0.250g E7 + 0.263g K7 + 1.636g K16
1689 0.250g E2 + 1.636g K16 + 0.263g K1 + 0.250g E7 + 0.263g K9
1690 2.500g E3 + 2.625g K1 + 1.636g K16 + 2.500g E7 + 2.625g K13
1691 1.250g E4 + 1.313g K1 + 1.250g E7 + 1.636g K16 + 1.313g K11
1692 2.500g El + 2.625g K1 + 2.500g E7 + 2.625g K14 + 1.636g K16
1693 2.500g E2 + 1.636g K16 + 2.625g Kl + 2.500g E7 + 2.625g K24
1694 2.500g E3 + 2.625g KI + 1.636g K16 + 2.500g E7 + 2.625g K2
1695 0.200g E4 + 0.210g Kl + 0.200g E7 + 1.636g K16 + 0.210g K12 + 0.210g K6
1696 0.200g E1 + 0.210g K1 + 0.200g E7 + 0.210g K12 + 1.636g K16 + 0.210g K8
1697 0.200g E2 + 0.210g K1 + 0.200g E7 + 0.210g K12 + 0.210g K9 + 1.636g K16
1698 2.000g E3 + 1.636g K16 + 2.100g K1 + 2.000g E7 + 2.100g K12 + 2.100g K13
1699 0.200g E4 + 0.210g K1 + 1.636g K16 + 0.200g E7 + 0.210g K12 + 0.210g K11
1700 0.200g E1 + 0.210g K1 + 0.200g E7 + 1.636g K16 + 0.210g K12 + 0.210g K14
1701 0.200g E2 + 0.210g K1 + 0.200g E7 + 0.210g K12 + 1.636g K16 + 0.210g K24
1702 2.000g E3 + 2.100g K1 + 2.000g E7 + 2.100g K12 + 2.100g K2 + 1.636g K16
1703 1.000g E4 + 1.636g K16 + 1.050g K1 + 1.000g E7 + 1.050g K6 + 1.050g K7
1704 1.000g El + 1.050g K1 + 1.636g K16 + 1.000g E7 + 1.050g K6 + 1.050g K9
1705 2.000g E2 + 2.100g K1 + 2.000g E7 + 1.636g K16 + 2.100g K6 + 2.100g K13
CA 02646867 2008-12-16
W245FQ/JC 105
1706 1.000g E3 + 1.050g Kl + 1.000g E7 + 1.050g K6 + 1.636g K16 + 1.050g Kl l
1707 0.200g E4 + 0.210g Kl + 0.200g E7 + 0.210g K6 + 0.210g K14 + 1.636g K16
1708 1.000g El + 1.636g K16 + 1.050g Kl + 1.000g E7 + 1.050g K6 + 1.050g K24
1709 0.200g E2 + 0.210g K1 + 1.636g K16 + 0.200g E7 + 0.210g K6 + 0.210g K2
1710 0.200g E3 + 0.210g K1 + 0.200g E7 + 1.636g K16 + 0.210g K7 + 0.210g K9
1711 0.200g E4 + 0.2lOg K1 + 0.200g E7 + 0.2lOg K7 + 1.636g K16 + 0.210g K13
1712 1.000g E1 + 1.050g K1 + 1.000g E7 + 1.050g K7 + 1.050g K11 + 1.636g K16
1713 2.000g E2 + 1.636g K16 + 2.100g K1 + 2.000g E7 + 2.100g K7 + 2.100g K14
1714 2.000g E3 + 2.100g Kl + 1.636g K16 + 2.000g E7 + 2.100g K7 + 2.100g K24
1715 1.000g E4 + 1.050g K1 + 1.000g E7 + 1.636g K16 + 1.050g K7 + 1.050g K2
1716 1.000g E1 + 1.050g K1 + 1.000g E7 + 1.050g K9 + 1.636g K16 + 1.050g K13
1717 2.000g E2 + 2. l00g Kl + 2.000g E7 + 2.100g K9 + 2.100g K11 + 1.636g K16
1718 0.200g E3 + 1.636g K16 + 0.210g K1 + 0.200g E7 + 0.210g K9 + 0.210g K14
1719 1.000g E4 + 1.050g K1 + 1.636g K16 + 1.000g E7 + 1.050g K9 + 1.050g K24
1720 0.200g El + 0.210g Kl + 0.200g E7 + 1.636g K16 + 0.210g K9 + 0.210g K2
1721 1.000g E2 + 1.050g K1 + 1.000g E7 + 1.050g K13 + 1.636g K16 + 1.050g K11
1722 2.000g E3 + 2.100g Kl + 2.000g E7 + 2.100g K13 + 2.100g K14 + 1.636g K16
1723 0.200g E4 + 1.636g K16 + 0.210g Kl + 0.200g E7 + 0.210g K13 + 0.210g K24
1724 0.200g E1 + 0.2lOg K1 + 1.636g K16 + 0.200g E7 + 0.210g K13 + 0.210g K2
1725 1.000g E2 + 1.050g K1 + 1.000g E7 + 1.636g K16 + 1.050g K11 + 1.050g K14
1726 2.000g E3 + 2.100g Kl + 2.000g E7 + 2.100g K11 + 1.636g K16 + 2.100g K24
1727 2.000g E4 + 2.100g Kl + 2.000g E7 + 2.100g K11 + 2.100g K2 + 1.636g K16
1728 2.000g E1 + 1.636g K16 + 2.100g K1 + 2.000g E7 + 2.100g K14 + 2.100g K24
1729 0.200g E2 + 0.210g Kl + 1.636g K16 + 0.200g E7 + 0.210g K14 + 0.210g K2
1730 0.200g E3 + 0.210g K1 + 0.200g E7 + 1.636g K16 + 0.210g K24 + 0.210g K2
1731 3.333g E4 + 3.500g Kl + 3.500g K12 + 1.636g K16
1732 0.250g El + 1.636g K16 + 0.263g Ki + 0.263g K12 + 0.263g K6
1733 0.250g E2 + 0.263g Kl + 1.636g K16 + 0.263g K12 + 0.263g K7
1734 1.250g E3 + 1.313g K1 + 1.313g K12 + 1.636g K16 + 1.313g K9
1735 0.250g E4 + 0.263g K1 + 0.263g K12 + 0.263g K13 + 1.636g K16
1736 1.250g E1 + 1.636g K16 + 1.313g K1 + 1.313g K12 + 1.313g K11
1737 2.500g E2 + 2.625g Ki + 1.636g K16 + 2.625g K12 + 2.625g K14
CA 02646867 2008-12-16
W245FQ/JC 106
1738 2.500g E3 + 2.625g K1 + 2.625g K12 + 1.636g K16 + 2.625g K24
1739 0.250g E4 + 0.263g Kl + 0.263g K12 + 0.263g K2 + 1.636g K16
1740 1.000g E1 + 1.636g K16 + 1.050g K1 + 1.050g K12 + 1.050g K6 + 1.050g K7
1741 1.000g E2 + 1.050g K1 + 1.636g K16 + 1.050g K12 + 1.050g K6 + 1.050g K9
1742 0.200g E3 + 0.210g K1 + 0.210g K12 + 1.636g K16 + 0.210g K6 + 0.210g K13
1743 1.000g E4 + 1.050g Kl + 1.050g K12 + 1.050g K6 + 1.636g K16 + 1.050g K11
1744 1.000g El + 1.050g K1 + 1.050g K12 + 1.050g K6 + 1.050g K14 + 1.636g K16
1745 1.000g E2 + 1.636g K16 + 1.050g Ki + 1.050g K12 + 1.050g K6 + 1.050g K24
1746 2.000g E3 + 2.l00g K1 + 1.636g K16 + 2.l00g K12 + 2.l00g K6 + 2.l00g K2
1747 0.200g E4 + 0.210g K1 + 0.210g K12 + 1.636g K16 + 0.210g K7 + 0.210g K9
1748 0.200g E1 + 0.210g K1 + 0.210g K12 + 0.210g K7 + 1.636g K16 + 0.210g K13
1749 1.000g E2 + 1.050g Kl + 1.050g K12 + 1.050g K7 + 1.050g K11 + 1.636g K16
1750 1.000g E3 + 1.636g K16 + 1.050g Kl + 1.050g K12 + 1.050g K21 + 1.050g K14
1751 2.000g E4 + 2.100g Kl + 1.636g K16 + 2.100g K12 + 2.100g K7 + 2.100g K24
1752 1.000g E1 + 1.050g Kl + 1.050g K12 + 1.636g K16 + 1.050g K7 + 1.050g K2
1753 2.000g E2 + 2.100g K1 + 2.100g K12 + 2.100g K9 + 1.636g K16 + 2.100g K13
1754 0.200g E3 + 0.210g K1 + 0.210g K12 + 0.210g K9 + 0.210g K11 + 1.636g K16
1755 1.000g E4 + 1.636g K16 + 1.050g K1 + 1.050g K12 + l.050g K9 + 1.050g K14
1756 2.000g E1 + 2.100g K1 + 1.636g K16 + 2.100g K12 + 2.100g K9 + 2.100g K24
1757 1.000g E2 + 1.050g K1 + 1.050g K12 + 1.636g K16 + 1.050g K9 + 1.050g K2
1758 0.200g E3 + 0.210g K1 + 0.210g K12 + 0.210g K13 + 1.636g K16 + 0.210g K11
1759 1.000g E4 + 1.050g Kl + 1.050g K12 + 1.050g K13 + 1.050g K14 + 1.636g K16
1760 0.200g E1 + 1.636g K16 + 0.210g K1 + 0.210g K12 + 0.210g K13 + 0.210g K24
1761 0.200gE2+0.210gK1 + 1.636g K16 + 0.210g K12 + 0.210g K13 +0.210gK2
1762 2.000g E3 + 2.100g Kl + 2.100g K12 + 1.839g K16 + 2.100g Kl l+ 2.100g K14
1763 1.000g E4 + l.050g Kl + 1.050g K12 + 1.050g K11 + 1.839g K16 + 1.050g K24
1764 2.000g E1 + 2.100g Kl + 2.100g K12 + 2.100g K11 + 2.100g K2 + 1.839g K16
1765 2.000g E2 + 1.839g K16 + 2.100g Kl + 2.100g K12 + 2.100g K14 + 2.100g K24
1766 0.200gE3+0.210gK1 + 1.839g K16 + 0.210g K12 + 0.210g K14 + 0.210g K2
1767 0.200gE4+0.210gK1 +0.210gK12+ 1.839g K16 + 0.210g K24 + 0.210g K2
1768 3.333g El + 3.500g Ki + 3.500g K6 + 1.839g K16
1 1769 1.250g E2 + 1.839g K16 + 1.313g K1 + 1.313g K6 + 1.313g K7
CA 02646867 2008-12-16
W245FQ/JC 107
1770 1.250g E3 + 1.313g K1 + 1.839g K16 + 1.313g K6 + 1.313g K9
1771 1.250gE4+1.313gK1+1.313gK6+1.839gK16+1.313gK13
1772 0.250g E1 + 0.263g K1 + 0.263g K6 + 0.263g K11 + 1.839g K16
1773 0.250g E2 + 1.839g K16 + 0.263g K1 + 0.263g K6 + 0.263g K14
1774 1.250g E3 + 1.313g K1 + 1.839g K16 + 1.313g K6 + 1.313g K24
1775 0.250g E4 + 0.263g KI + 0.263g K6 + 1.839g K16 + 0.263g K2
1776 0.200gE1 +0.210gK1 + 0.210g K6 + 0.210g K7 + 1.839g K16 + 0.210g K9
1777 1.000g E2 + 0.850g K1 + 1.050g K6 + 1.050g K7 + 1.050g K4 + 1.050g K13 +
1.839g K16
1778 0.200g E3 + 1.839g K16 + 0.210g K1 + 0.210g K6 + 0.210g K7 + 0.210g K11
1779 2.000g E4 + 2.100g K1 + 1.839g K16 + 2.100g K6 + 2.100g K7 + 2.100g K14
1780 2.000g E1 + 2.100g Kl + 2.100g K6 + 1.839g K16 + 2.100g K7 + 2.100g K24
1781 0.200g E2 + 0.210g K1 + 0.210g K6 + 0.210g K8 + 1.839g K16 + 0.210g K2
1782 2.000g E3 + 2.100g Kl + 2. l00g K6 + 2.100g K9 + 2.100g K13 + 1.839g K16
1783 0.200g E4 + 1.839g K16 + 0.210g K1 + 0.210g K6 + 0.210g K9 + 0.210g K11
1784 2.000g E1 + 2.100g K1 + 1.839g K16 + 2.100g K6 + 2.100g K9 + 2.100g K14
1785 2.000g E2 + 2.100g Kl + 2.100g K6 + 1.839g K16 + 2.100g K9 + 2.100g K24
1786 1.000g E3 + 1.050g K1 + 1.050g K6 + 1.050g K9 + 1.839g K16 + 1.050g K2
1787 2.000g E4 + 2.100g Kl + 2. l00g K6 + 2.100g K13 + 2.100g K11 + 1.839g K16
1788 2.000g E1 + 1.839g K16 + 2.100g K1 + 2.100g K6 + 2.100g K13 + 2.100g K14
1789 0.200g E2 + 0.210g Kl + 1.839g K16 + 0.210g K6 + 0.210g K13 + 0.210g K24
1790 0.200g E3 + 0.210g K1 + 0.210g K6 + 1.839g K16 + 0.210g K13 + 0.210g K2
1791 0.200g E4 + 0.210g K1 + 0.210g K6 + 0.210g K1 l+ 1.839g K16 + 0.210g K14
1792 0.200g El + 0.210g K1 + 0.210g K6 + 0.210g Kl 1+ 0.210g K24 + 1.839g K16
1793 0.200g E2 + 1.839g K16 + 0.210g K1 + 0.210g K6 + 0.210g K11 + 0.210g K2
1794 1.000g E3 + 1.050g Kl + 1.839g K16 + 1.050g K6 + 1.050g K14 + 1.050g K24
1795 1.000g E4 + 1.050g K1 + 1.050g K6 + 1.839g K16 + 1.050g K14 + 1.050g K2
1796 1.000g E1 + 1.050g K1 + 1.050g K6 + 1.050g K24 + 1.839g K16 + 1.050g K2
1797 0.333g E2 + 0.350g K1 + 0.350g K7 + 1.839g K16
1798 0.250g E3 + 1.839g K16 + 0.263g K5 + 0.263g K7 + 0.263g K9
1799 1.250gE4+1.313gK1+1.839gK16+1.313gK7+1.313gK13
1800 0.250g El + 0.263g K1 + 0.263g K7 + 1.839g K16 + 0.263g K11
CA 02646867 2008-12-16
W245FQ/JC 108
1801 0.250g E2 + 0.263g Kl + 0.263g K7 + 0.263g K14 + 1.839g K16
1802 2.500g E3 + 1.839g K16 + 2.625g K1 + 2.625g K7 + 2.625g K24
1803 2.500g E4 + 2.625g Kl + 1.839g K16 + 2.625g K7 + 2.625g K2
1804 0.200g E1 + 0.210g K1 + 0.210g K7 + 1.839g K16 + 0.210g K9 + 0.210g K13
1805 1.000g E2 + 1.050g K1 + 1.050g K7 + 1.050g K9 + 1.839g K16 + 1.050g K11
1806 2.000g E3 + 2.100g K1 + 2.100g K7 + 2.100g K9 + 2.100g K14 + 1.839g K16
1807 2.000g E4 + 1.839g K16 + 2.100g K1 + 2.100g K7 + 2.100g K9 + 2.100g K24
1808 2.000g E1 + 2.100g Kl + 1.839g K16 + 2.100g K21 + 2.100g K9 + 2.100g K2
1809 0.200g E2 + 0.210g K1 + 0.210g K7 + 1.839g K16 + 0.210g K13 + 0.210g K11
1810 0.200g E3 + 0.210g K1 + 0.210g K7 + 0.210g K13 + 1.839g K16 + 0.210g K14
1811 2.000g E4 + 2.100g K1 + 2.100g K7 + 2.100g K13 + 2.100g K24 + 1.839g K16
1812 2.000g El + 1.839g K16 + 2.l00g K1 + 2.100g K7 + 2.100g K13 + 2.100g K2
1813 2.000g E2 + 2.100g K1 + 1.839g K16 + 2.100g K7 + 2.100g K11 + 2.100g K14
1814 1.000g E3 + 1.050g K1 + 1.050g K7 + 1.839g K16 + 1.050g Kl l+ 1.050g K24
1815 1.000g E4 + 1.050g K1 + 1.050g K7 + 1.050g K11 + 1.839g K16 + 1.050g K2
1816 2.000g E1 + 2.100g K1 + 2.100g K7 + 2.100g Kl4 + 2.100g K24 + 1.839g K16
1817 2.000g E2 + 1.839g K16 + 2.100g Kl + 2.100g K7 + 2.100g K14 + 2.100g K2
1818 2.000g E3 + 2.100g K1 + 1.839g K16 + 2.100g K8 + 2.100g K24 + 2.100g K2
1819 1.667g E4 + 1.750g Kl + 1.750g K9 + 1.839g K16
1820 0.250g El + 1.839g K16 + 0.263g K1 + 0.263g K9 + 0.263g K13
1821 2.500g E2 + 2.625g K1 + 1.839g K16 + 2.625g K9 + 2.625g K11
1822 2.500g E3 + 2.625g Kl + 2.625g K9 + 1.839g K16 + 2.625g K14
1823 1.250g E4 + 1.313g K1 + 1.313g K9 + 1.313g K24 + 1.839g K16
1824 0.250g El + 1.839g K16 + 0.263g K1 + 0.263g K9 + 0.263g K2
1825 0.200g E2 + 0.210g K1 + 1.839g K16 + 0.210g K9 + 0.210g K13 + 0.210g K11
1826 0.200g E3 + 0.210g K1 + 0.210g K9 + 1.839g K16 + 0.210g K13 + 0.210g K14
1827 0.200g E4 + 0.210g K1 + 0.210g K9 + 0.210g K13 + 1.839g K16 + 0.210g K24
1828 1.000g El + 1.050g K1 + 1.050g K9 + 1.050g K13 + 1.050g K2 + 1.839g K16
1829 1.000g E2 + 1.839g K16 + 1.050g K1 + l.050g K9 + 1.050g Kl l+ 1.050g Kl4
1830 0.200g E3 + 0.210g Kl + 1.839g K16 + 0.210g K9 + 0.210g Kl l+ 0.210g K24
1831 1.000g E4 + 1.050g K1 + 1.050g K9 + 1.839g K16 + 1.050g K11 + 1.050g K2
1832 2.000g E1 + 2.100g Kl + 2.100g K9 + 2.100g K14 + 1.839g K16 + 2.100g K24
CA 02646867 2008-12-16
W245FQ/JC 109
1833 0.200gE2+0.210gK1 + 0.210g K9 + 0.210g K14 + 0.210g K2 + 1.839gK16
1834 1.000g E3 + 1.839g K16 + 1.050g K1 + 1.050g K9 + 1.050g K24 + 1.050g K2
1835 1.667g E4 + 1.750g K1 + 1.839g K16 + 1.750g K13
1836 0.250g El + 0.263g Kl + 0.263g K13 + 1.839g K16 + 0.263g Kl 1
1837 1.250g E2 + 1.313g K1 + 1.313g K13 + 1.313g K14 + 1.839g K16
1838 2.500g E3 + 1.839g K16 + 2.625g K1 + 2.625g K13 + 2.625g K24
1839 2.500g E4 + 2.625g Kl + 1.839g K16 + 2.625g K13 + 2.625g K2
1840 1.000g E1 + 1.050g Kl + 1.050g K13 + 1.839g K16 + 1.050g Kl l+ 1.050g K14
1841 0.200g E2 + 0.210g Kl + 0.210g K13 + 0.210g K11 + 1.839g K16 + 0.210g K24
1842 0.200g E3 + 0.210g K1 + 0.210g K13 + 0.210g K11 + 0.210g K2 + 1.839g K16
1843 0.200g E4 + 1.839g K16 + 0.210g Kl + 0.210g K13 + 0.210g K14 + 0.210g K24
1844 1.000g El + 1.050g Kl + 1.839g K16 + 1.050g K13 + 1.050g K14 + 1.050g K2
1845 0.200g E2 + 0.210g Kl + 0.210g K13 + 1.839g K16 + 0.210g K24 + 0.210g K2
1846 5.000g El + 5.250g K1 + 1.839g K16 + O.OlOg D1
1847 0.333g E4 + 1.839g K16 + 0.350g K1 + 0.350g K11
1848 1.667g E1 + 1.750g Kl + 1.839g K16 + 1.750g K14
1849 0.333g E2 + 0.350g KI + 0.350g K24 + 1.839g K16
1850 1.667g E3 + 1.839g K16 + 0.750g K18 + 1.750g K2
1851 1.250gE4+1.313gK1+1.839gK16+1.313gK11+1.313gK14
1852 2.500g El + 2.625g K1 + 2.625g K11 + 0.042g K16 + 2.625g K24
1853 1.250gE2+ 1.313gK1 +0.313gK4+ 1.313gK11 + 1.313gK2+0.042gK16
1854 0.250g E3 + 0.042g K16 + 0.263g Kl + 0.263g K14 + 0.263g K24
1855 1.250gE4+1.313gK1 + 0.042g K16 + 1.313g K14 + 1.313g K2
1856 1.250g El + 1.313g K1 + 1.313g K24 + 0.042g K16 + 1.313g K2
1857 2.000g E2 + 2.100g K1 + 2.100g K11 + 2.100g K14 + 0.042g K16 + 2.100g K24
1858 0.200g E3 + 0.210g K1 + 0.210g K11 + 0.210g K14 + 0.210g K2 + 0.042g K16
1859 2.000g E4 + 0.042g K16 + 2.100g K1 + 2.100g K11 + 2.100g K24 + 2.100g K2
1860 1.000g El + 1.050g Kl + 0.042g K16 + 1.050g K14 + 1.050g K24 + 1.050g K2
1861 2.500g E2 + 2.625g Kl 1 + 2.500g E8 + 0.042g K16 + 2.625g K12
1862 2.500g E3 + 2.625g Kl 1+ 2.500g E8 + 2.625g K6 + 0.042g K16
1863 1.250g E4 + 0.042g K16 + 1.313g K11 + 1.250g E8 + 1.313g K7
1864 0.250g El + 0.263g K11 + 0.042g K16 + 0.250g E8 + 0.263g K9
CA 02646867 2008-12-16
W245FQ/JC 110
1865 2.500g E2 + 2.625g K11 + 2.500g E8 + 0.042g K16 + 2.625g K13
1866 2.500g E3 + 2.625g K11 + 2.500g E8 + 2.625g K1 + 0.042g K16
1867 1.250g E4 + 0.042g K16 + 1.313g K11 + 1.250g E8 + 1.313g K14
1868 0.250g El + 0.263g K11 + 0.042g K16 + 0.250g E8 + 0.263g K24
1869 0.250g E2 + 0.263g K11 + 0.250g E8 + 0.042g K16 + 0.263g K2
1870 1.000g E3 + 1.050g Kl 1+ 1.000g E8 + 1.050g K12 + 0.042g K16 + 1.050g K6
1871 2.000g E4 + 2.100g K11 + 2.000g E8 + 2.100g K12 + 2.100g K7 + 0.042g K16
1872 1.000g E1 + 0.042g K16 + 1.050g K11 + 1.000g E8 + 1.050g K12 + 1.050g K9
1873 1.000g E2 + 1.050g K11 + 0.042g K16 + 1.000g E8 + 1.050g K12 + 1.050g K13
1874 0.200g E3 + 0.210g K11 + 0.200g E8 + 0.042g K16 + 0.210g K12 + 0.210g K1
1875 1.000g E4 + 1.050g K11 + 1.000g E8 + 1.050g K12 + 0.042g K16 + 1.050g K14
1876 1.000g El + 1.050g K11 + 1.000g E8 + 1.050g K12 + 1.050g K24 + 0.042g K16
1877 0.200g E2 + 0.042g K16 + 0.210g K11 + 0.200g E8 + 0.210g K12 + 0.210g K2
1878 0.200g E3 + 0.210g Kl 1+ 0.042g K16 + 0.200g E8 + 0.210g K6 + 0.210g K7
1879 2.000g E4 + 2.100g K11 + 2.000g E8 + 0.042g K16 + 2.l00g K6 + 2.l00g K9
1880 2.000g E1 + 2.100g K11 + 2.000g E8 + 2.100g K6 + 0.042g K16 + 2.100g K13
1881 1.000g E2 + 1.050g Kl 1 + 1.000g E8 + 1.050g K6 + 1.050g KI + 0.042g K16
1882 2.000g E3 + 0.042g K16 + 2.100g K11 + 2.000g E8 + 2.100g K6 + 2.100g K14
1883 2.000g E4 + 2.100g Kl l+ 0.042g K16 + 2.000g E8 + 2.100g K6 + 2.100g K24
1884 1.000g E1 + 1.050g K11 + 1.000g E8 + 0.042g K16 + 1.050g K6 + 1.050g K2
1885 0.200g E2 + 0.210g K11 + 0.200g E8 + 0.210g K7 + 0.042g K16 + 0.210g K9
1886 1.000g E3 + 1.050g Kl l+ 1.000g E8 + 1.050g K7 + 1.050g K13 + 0.042g K16
1887 2.000g E4 + 0.042g K16 + 2.100g K11 + 2.000g E8 + 2.100g K7 + 2.100g Kl
1888 1.000g E1 + 1.050g Kl l+ 0.042g K16 + 1.000g E8 + 1.050g K7 + 1.050g K14
1889 1.000g E2 + 1.050g K11 + 1.000g E8 + 0.042g K16 + 1.050g K7 + 1.050g K24
1890 1.000g E3 + 1.050g Kl l+ 1.000g E8 + 1.050g K7 + 0.042g K16 + 1.050g K2
1891 2.000g E4 + 2. l00g K11 + 2.000g E8 + 2.100g K9 + 2. l00g K13 + 0.042g
K16
1892 0.200g El + 0.042g K16 + 0.210g Kl 1+ 0.200g E8 + 0.210g K9 + 0.210g Kl
1893 0.200g E2 + 0.210g K11 + 0.042g K16 + 0.200g E8 + 0.210g K9 + 0.210g K14
1894 1.000g E3 + 1.050g K11 + 1.000g E8 + 0.042g K16 + 1.050g K9 + 1.050g K24
1895 2.000g E4 + 2.100g K11 + 2.000g E8 + 2.100g K9 + 0.042g K16 + 2.100g K2
1896 2.000g E1 + 2.100g K11 + 2.000g E8 + 2.100g K13 + 0. l00g K5 + 1.900g K1
+
CA 02646867 2008-12-16
W245FQ/JC 111
0.042g K16
1897 0.200gE2+0.042gK16+0.210gK11+0.200gE8+0.210gK13+0.210gK14
1898 0.200g E3 + 0.210g K11 + 0.042g K16 + 0.200g E8 + 0.210g K13 + 0.210g K24
1899 1.000g E4 + 1.050g K11 + 1.000g E8 + 0.042g K16 + 1.050g K13 + 1.050g K2
1900 0.200g El + 0.210g Kl 1 + 0.200g E8 + 0.210g K1 + 0.042g K16 + 0.210g K14
1901 1.000g E2 + 1.050g K11 + 1.000g E8 + 1.050g K1 + 1.050g K24 + 0.042g K16
1902 0.200g E3 + 0.042g K16 + 0.210g K11 + 0.200g E8 + 0.210g K1 + 0.210g K2
1903 0.200g E4 + 0.210g Kl 1 + 0.042g K16 + 0.200g E8 + 0.210g K14 + 0.210g
K24
1904 2.000g El + 2.100g K11 + 2.000g E8 + 0.042g K16 + 2.100g K14 + 2.100g K2
1905 0.200g E2 + 0.210g K11 + 0.200g E8 + 0.210g K24 + 0.042g K16 + 0.210g K2
1906 1.250g E3 + 1.313g K11 + 1.250g E6 + 1.313g K12 + 0.042g K16
1907 2.500g E4 + 0.042g K16 + 2.625g K11 + 2.500g E6 + 2.625g K6
1908 0.250g El + 0.263g KI 1 + 0.042g K16 + 0.250g E6 + 0.263g K7
1909 2.500g E2 + 2.625g Kl 1 + 2.500g E6 + 0.042g K16 + 2.625g K9
1910 2.500g E3 + 2.625g K11 + 2.500g E6 + 2.625g K13 + 0.042g K16
1911 0.250g E4 + 0.042g K16 + 0.263g K11 + 0.250g E6 + 0.263g Kl
1912 0.250g El + 0.263g Ki 1+ 0.042g K16 + 0.250g E6 + 0.263g K14 + 0.090g D2
1913 0.250g E2 + 0.263g Kl 1+ 0.250g E6 + 0.042g K16 + 0.263g K24
1914 1.250g E3 + 1.313g K11 + 1.250g E6 + 1.313g K2 + 0.042g K16
1915 1.000g E4 + 0.042g K16 + 1.050g Kl 1+ 1.000g E6 + 1.050g K12 + 1.050g K6
1916 2.000g El + 2.100g K11 + 0.042g K16 + 2.000g E6 + 2.100g K12 + 2.100g K21
1917 0.200gE2+0.210gK11 + 0.200g E6 + 0.042g K16 + 0.210g K12 + 0.210g K9
1918 1.000g E3 + 1.050g Kl l+ 1.000g E6 + 1.050g K12 + 0.042g K16 + 1.050g K13
1919 1.000g E4 + 1.050g K11 + 1.000g E6 + 1.050g K12 + 1.050g K1 + 0.042g K16
1920 0.200gE1 +0.042gK16+0.210gK11 + 0.200g E6 + 0.210g K12 + 0.210g K14
1921 2.000g E2 + 2.100g Kl l+ 0.042g K16 + 2.000g E6 + 2.100g K12 + 2.100g K24
1922 1.000g E3 + 1.050g Kl l+ 1.000g E6 + 0.042g K16 + 1.050g K12 + 1.050g K2
1923 1.000g E4 + 1.050g K11 + 1.000g E6 + 1.050g K6 + 0.042g K16 + 1.050g K7
1924 2.000g El + 2.100g K11 + 2.000g E6 + 2.100g K6 + 2.100g K9 + 0.042g K16
1925 2.000g E2 + 0.042g K16 + 2.100g K11 + 2.000g E6 + 2.100g K6 + 2.100g K13
1926 2.000g E3 + 2.100g Kl 1+ 0.042g K16 + 2.000g E6 + 2.100g K6 + 2.100g K1
1927 0.200g E4 + 0.210g K11 + 0.200g E6 + 0.042g K16 + 0.210g K6 + 0.210g K14
CA 02646867 2008-12-16
W245FQ/JC 112
1928 0.200g El + 0.210g Kl 1+ 0.200g E6 + 0.210g K6 + 0.042g K16 + 0.210g K24
1929 1.000g E2 + 1.050g K11 + 1.000g E6 + 1.050g K6 + 1.050g K2 + 0.042g K16
1930 0.200g E3 + 0.042g K16 + 0.210g K11 + 0.200g E6 + 0.214g K7 + 0.210g K9
1931 2.000g E4 + 2.100g K1 l+ 0.042g K16 + 2.000g E6 + 2.100g K7 + 2.100g K13
1932 0.200g El + 0.210g K11 + 0.200g E6 + 0.042g K16 + 0.210g K7 + 0.210g K1
1933 0.200g E2 + 0.210g K11 + 0.200g E6 + 0.210g K7 + 0.042g K16 + 0.210g K14
1934 2.000g E3 + 2.100g K11 + 2.000g E6 + 2.100g K7 + 2.100g K24 + 0.042g K16
1935 1.000g E4 + 0.042g K16 + 1.050g K11 + 1.000g E6 + 1.050g K7 + 1.050g K2
1936 2.000g El + 2.100g Kl 1 + 0.042g K16 + 2.000g E6 + 2.100g K9 + 2.100g K13
1937 1.000g E2 + 1.050g Kl l+ 1.000g E6 + 0.042g K16 + 1.050g K9 + 1.050g K1
1938 0.200gE3+0.210gK11 + 0.200g E6 + 0.210g K9 + 0.042g K16 + 0.210g K14
1939 0.200g E4 + 0.210g K11 + 0.200g E6 + 0.210g K9 + 0.210g K24 + 0.042g K16
1940 2.000g El + 0.042g K16 + 2.100g K11 + 2.000g E6 + 2.100g K9 + 2.100g K2
1941 2.000g E2 + 2.100g K11 + 0.042g K16 + 2.000g E6 + 2.100g K13 + 2.100g K1
1942 1.000g E3 + 1.050g K11 + 1.000g E6 + 0.245g K16 + 1.050g K13 + 1.050g K14
1943 0.200g E4 + 0.210g K11 + 0.200g E6 + 0.210g K13 + 0.245g K16 + 0.210g K24
1944 0.200g El + 0.210g KI 1+ 0.200g E6 + 0.210g K13 + 0.210g K2 + 0.245g K16
1945 0.200g E2 + 0.245g K16 + 0.210g K11 + 0.200g E6 + 0.210g K1 + 0.210g K14
1946 1.000g E3 + 1.050g Kl l+ 0.245g K16 + 1.000g E6 + 1.050g K1 + 1.050g K24
1947 2.000g E4 + 2.100g Kl l+ 2.000g E6 + 0.245g K16 + 2.100g K1 + 2.100g K2
1948 2.000g E1 + 2.100g K11 + 2.000g E6 + 2.100g K14 + 0.245g K16 + 2.100g K24
1949 0.200g E2 + 0.210g K11 + 0.200g E6 + 0.210g K14 + 0.210g K2 + 0.245g K16
1950 0.200g E3 + 0.245g K16 + 0.210g K11 + 0.200g E6 + 0.210g K24 + 0.210g K2
1951 1.250g E4 + 1.313g K11 + 0.245g K16 + 1.250g E5 + 1.313g K12
1952 1.250g E1 + 1.313g Kl 1+ 1.250g E5 + 0.245g K16 + 1.313g K6
1953 1.250g E2 + 1.313g K11 + 1.250g E5 + 1.313g K7 + 0.245g K16
1954 1.250g E3 + 0.245g K16 + 1.313g K11 + 1.250g E5 + 1.313g K9
1955 0.250g E4 + 0.263g Kl 1+ 0.245g K16 + 0.250g E5 + 0.263g K13
1956 2.500g El + 2.625g KI 1+ 2.500g E5 + 0.245g K16 + 2.625g K1
1957 2.500g E2 + 2.625g K11 + 2.500g E5 + 2.625g K14 + 0.245g K16
1958 1.250g E3 + 0.245g K16 + 1.313g K11 + 1.250g E5 + 1.313g K24
1959 1.250g E4 + 1.313g K11 + 0.245g K16 + 1.250g E5 + 1.313g K2
CA 02646867 2008-12-16
W245FQ/JC 113
1960 2.000g E1 + 2.100g K11 + 2.000g E5 + 0.245g K16 + 2.100g K12 + 2.100g K6
1961 1.000g E2 + 1.050g K11 + 1.000g E5 + 1.050g K15 + 0.245g K16 + 1.050g K7
1962 2.000g E3 + 2.100g K11 + 2.000g E5 + 2.100g K12 + 2.100g K9 + 0.245g K16
1963 2.000g E4 + 0.245g K16 + 2.100g K11 + 2.000g E5 + 2.000g K15 + 2.l00g K12
+
2.100g K13
1964 2.000g El + 2.100g K11 + 0.245g K16 + 2.000g E5 + 2.100g K12 + 2.100g Kl
1965 2.000g E2 + 2.100g Kl 1+ 2.000g E5 + 0.245g K16 + 2.100g K12 + 2.100g K14
1966 0.200g E3 + 0.210g K11 + 0.200g E5 + 0.210g K12 + 0.245g K16 + 0.210g K24
1967 1.000g E4 + 1.050g K11 + 1.000g E5 + 1.050g K12 + 1.050g K2 + 0.245g K16
1968 0.200g E1 + 0.245g K16 + 0.210g K11 + 0.200g E5 + 0.210g K6 + 0.210g K7
1969 0.200g E2 + 0.210g K11 + 0.245g K16 + 0.200g E5 + 0.210g K6 + 0.210g K9
1970 0.200g E3 + 0.210g K11 + 0.200g E5 + 0.245g K16 + 0.210g K6 + 0.210g K13
1971 1.000g E4 + 1.050g K11 + 1.000g E5 + 1.050g K6 + 0.245g K16 + 1.050g Kl
1972 1.000g El + 1.050g K11 + 1.000g E5 + 1.050g K6 + 1.050g K14 + 0.245g K16
1973 2.000g E2 + 0.245g K16 + 2.l00g K11 + 2.000g E5 + 2.l00g K6 + 2.100g K24
1974 1.000g E3 + 1.050g Kl 1 + 0.245g K16 + 1.000g E5 + 1.050g K6 + 1.050g K2
1975 0.200g E4 + 0.210g K11 + 0.200g E5 + 0.245g K16 + 0.210g K8 + 0.210g K9
1976 1.000g E1 + 1.050g Kl 1+ 1.000g E5 + 1.050g K7 + 0.245g K16 + 1.050g K13
1977 2.000g E2 + 2.100g K11 + 2.000g E5 + 2.100g K7 + 2.100g K1 + 0.245g K16
1978 0.200g E3 + 0.245g K16 + 0.210g K11 + 0.200g E5 + 0.210g K7 + 0.210g K14
1979 2.000g E4 + 2.100g Kl l+ 0.245g K16 + 2.000g E5 + 2.100g K7 + 2.100g K24
1980 0.200g E1 + 0.210g K11 + 0.200g E5 + 0.245g K16 + 0.210g K7 + 0.210g K2
1981 1.000g E2 + 1.050g Kl 1 + 1.000g E5 + 1.050g K9 + 0.245g K16 + 1.050g K13
1982 2.000g E3 + 2.100g KI l+ 2.000g E5 + 2.100g K9 + 2.100g Kl + 0.245g K16
1983 0.200g E4 + 0.245g K16 + 0.210g K11 + 0.200g E5 + 0.210g K9 + 0.210g K14
1984 0.200g El + 0.210g Kl 1 + 0.245g K16 + 0.200g E5 + 0.210g K9 + 0.210g K24
1985 0.200g E2 + 0.210g K11 + 0.200g E5 + 0.245g K16 + 0.210g K9 + 0.210g K2
1986 1.000g E3 + 1.050g Kl l+ 1.000g E5 + 1.050g K13 + 0.245g K16 + 1.050g K1
1987 1.000g E4 + 1.050g K11 + 1.000g E5 + 1.050g K13 + 1.050g K14 + 0.245g K16
1988 1.000g E1 + 0.245g K16 + 1.050g Kl l+ 1.000g E5 + 1.050g K13 + 1.050g K24
1989 2.000g E2 + 2.l00g K11 + 0.245g K16 + 2.000g E5 + 2.l00g K13 + 2.l00g K2
1990 2.000g E3 + 2.l00g K11 + 2.000g E5 + 0.245g K16 + 2.l00g K1 + 2.l00g K14
CA 02646867 2008-12-16
W245 FQ/J C 114
1991 0.200g E4 + 0.210g K11 + 0.200g E5 + 0.210g K1 + 0.245g K16 + 0.210g K24
1992 2.000g El + 2.100g K11 + 2.000g E5 + 2.100g K1 + 2.100g K2 + 0.245g K16
1993 2.000g E2 + 0.245g K16 + 2.100g K11 + 2.000g E5 + 2.100g K14 + 2.100g K24
1994 1.000g E3 + 1.050g K11 + 0.245g K16 + 1.000g E5 + 1.050g K14 + 1.050g K2
1995 2.000g E4 + 2.100g K11 + 2.000g E5 + 0.245g K16 + 2.100g K24 + 2.100g K2
1996 2.500g El + 2.625g K11 + 2.500g E7 + 2.625g K12 + 0.245g K16
1997 1.250g E2 + 0.245g K16 + 1.313g K11 + 1.250g E7 + 1.313g K6
1998 2.500g E3 + 2.625g K11 + 0.245g K16 + 2.500g E7 + 2.625g K7
1999 0.250g E4 + 0.263g K11 + 0.250g E7 + 0.245g K16 + 0.263g K9
2000 1.250g El + 1.313g Kl 1+ 1.250g E7 + 1.313g K13 + 0.245g K16
2001 2.500g E2 + 0.245g K16 + 2.625g Kl 1+ 2.500g E7 + 2.625g K1
2002 2.500g E3 + 2.625g Kl 1+ 0.245g K16 + 2.500g E7 + 2.625g K14
2003 2.500g E4 + 2.625g K11 + 2.500g E7 + 0.245g K16 + 2.625g K24
2004 2.500g El + 2.625g K11 + 2.500g E7 + 2.625g K2 + 0.245g K16
2005 2.000g E2 + 0.245g K16 + 2.100g K11 + 2.000g E7 + 2.100g K15 + 2.100g K6
2006 0.200g E3 + 0.210g K11 + 0.245g K16 + 0.200g E7 + 0.210g K12 + 0.210g K7
2007 2.000g E4 + 2.100g K11 + 2.000g E7 + 0.245g K16 + 2.100g K12 + 2.100g K9
2008 0.200g E1 + 0.210g K11 + 0.200g E7 + 0.210g K15 + 0.245g K16 + 0.210g K13
2009 2.000g E2 + 2.100g K11 + 2.000g E7 + 2.100g K12 + 2.100g Kl + 0.245g K16
2010 1.000g E3 + 0.245g K16 + 1.050g K11 + 1.000g E7 + 1.050g K12 + 1.050g K14
2011 2.000g E4 + 2.100g K11 + 0.245g K16 + 2.000g E7 + 2.100g K12 + 2.100g K24
2012 1.000g E1 + 1.050g K11 + 1.000g E7 + 0.245g K16 + 1.050g K12 + 1.050g K2
2013 1.000g E2 + 1.050g Kl 1+ 1.000g E7 + 1.050g K6 + 0.245g K16 + 1.050g K7
2014 2.000g E3 + 2.100g K11 + 2.000g E7 + 2.100g K6 + 2.100g K9 + 0.245g K16
2015 0.200gE4+0.245gK16+0.210gK11 + 0.200g E7 + 0.210g K6 + 0.210g K13
2016 1.000g E1 + 1.050g K11 + 0.245g K16 + 1.000g E7 + 1.050g K6 + 1.050g K1
2017 2.000g E2 + 2.100g K11 + 2.000g E7 + 0.245g K16 + 2.100g K6 + 2.l00g K14
2018 2.000g E3 + 2.100g Kl 1+ 2.000g E7 + 2.100g K6 + 0.245g K16 + 2.100g K24
2019 0.200g E4 + 0.210g K11 + 0.200g E7 + 0.210g K6 + 0.210g K2 + 0.245g K16
2020 2.000g E1 + 0.245g K16 + 2.100g K11 + 2.000g E7 + 2.100g K7 + 2.100g K9
2021 1.000g E2 + 1.050g K11 + 0.245g K16 + 1.000g E7 + 1.050g K21 + 1.050g K13
2022 1.000g E3 + 1.050g K11 + 1.000g E7 + 0.245g K16 + 1.050g K7 + 1.050g Kl
CA 02646867 2008-12-16
W245FQ/JC 115
2023 2.000g E4 + 2.100g K11 + 2.000g E7 + 2.100g K7 + 0.245g K16 + 2.100g K14
2024 0.200g El + 0.210g K11 + 0.200g E7 + 0.210g K7 + 0.210g K24 + 0.245g K16
2025 0.200g E2 + 0.245g K16 + 0.210g K11 + 0.200g E7 + 0.210g K7 + 0.210g K2
2026 2.000g E3 + 2.100g Kl 1 + 0.245g K16 + 2.000g E7 + 2.100g K9 + 2.100g K13
2027 2.000g E4 + 2.100g K11 + 2.000g E7 + 0.245g K16 + 2.100g K9 + 2.100g K1
2028 0.200g El + 0.210g K11 + 0.200g E7 + 0.210g K9 + 0.245g K16 + 0.210g K14
2029 0.200g E2 + 0.210g K11 + 0.200g E7 + 0.210g K9 + 0.210g K24 + 0.245g K16
2030 1.000g E3 + 0.245g K16 + 1.050g K11 + 1.000g E7 + 1.050g K9 + 1.050g K2
2031 1.000g E4 + 1.050g K11 + 0.245g K16 + 1.000g E7 + 1.050g K13 + l.050g K1
2032 2.000g El + 2.100g Kl 1+ 2.000g E7 + 0.245g K16 + 2.100g K13 + 2.100g K14
2033 0.200g E2 + 0.210g K11 + 0.200g E7 + 0.210g K13 + 0.448g K16 + 0.210g K24
2034 2.000g E3 + 2.100g K11 + 2.000g E7 + 2.100g K13 + 2.100g K15 + 0.048g K16
2035 2.000g E4 + 0.448g K16 + 2.100g Kl l+ 2.000g E7 + 2.100g Kl + 2.100g K14
2036 0.200g El + 0.210g K11 + 0.448g K16 + 0.200g E7 + 0.210g Kl + 0.210g K24
2037 0.200g E2 + 0.210g Kl 1 + 0.200g E7 + 0.448g K16 + 0.210g K1 + 0.210g K2
2038 1.000g E3 + 1.050g K11 + 1.000g E7 + 1.050g K14 + 0.448g K16 + 1.050g K24
2039 0.200g E4 + 0.210g Kl 1+ 0.200g E7 + 0.210g K14 + 0.210g K2 + 0.448g K16
2040 0.200g El + 0.448g K16 + 0.210g K11 + 0.200g E7 + 0.210g K24 + 0.210g K2
2041 3.333g E2 + 3.500g K11 + 0.448g K16 + 3.500g K12 + 0.100g D3
2042 2.500g E3 + 2.625g K11 + 2.625g K12 + 0.448g K16 + 2.625g K6
2043 0.250g E4 + 0.263g K11 + 0.263g K12 + 0.263g K7 + 0.448g K16
2044 0.250g El + 0.448g K16 + 0.263g K11 + 0.263g K12 + 0.263g K9
2045 2.500g E2 + 2.625g Kl 1 + 0.448g K16 + 2.625g K12 + 2.625g K15
2046 0.250g E3 + 0.263g Kl 1 + 0.263g K12 + 0.448g K16 + 0.263g K1
2047 0.250g E4 + 0.263g Kl 1 + 0.263g K12 + 0.263g K14 + 0.448g K16
2048 1.250g E1 + 0.448g K16 + 1.313g K11 + 1.313g K12 + 1.313g K24
2049 2.500g E2 + 2.625g K11 + 0.448g K16 + 2.625g K12 + 2.625g K2
2050 0.200g E3 + 0.210g K11 + 0.210g K12 + 0.448g K16 + 0.210g K6 + 0.210g K7
2051 0.200g E4 + 0.210g K11 + 0.210g K12 + 0.210g K6 + 0.448g K16 + 0.210g K9
2052 2.000g El + 2.100g Kl 1 + 2.100g K12 + 2.100g K6 + 2.100g K13 + 0.448g
K16
2053 1.000g E2 + 0.448g K16 + 1.050g K11 + 1.050g K12 + 1.050g K6 + 1.050g Kl
2054 0.200gE3+0.210gK11 + 0.448g K16 + 0.210g K12 + 0.210g K6 + 0.210g K14
CA 02646867 2008-12-16
W245FQ/JC 116
2055 1.000g E4 + 1.050g K11 + 1.050g K12 + 0.448g K16 + 1.050g K6 + 1.050g K24
2056 0.200g E1 + 0.210g K11 + 0.210g K12 + 0.210g K6 + 0.448g K16 + 0.210g K2
2057 2.000g E2 + 2.100g Kl l+ 2.100g K12 + 2.100g K7 + 2.100g K9 + 0.448g K16
2058 0.200g E3 + 0.448g K16 + 0.210g K11 + 0.210g K12 + 0.210g K7 + 0.210g K13
2059 2.000g E4 + 2.100g K11 + 0.448g K16 + 2.100g K12 + 2.100g K7 + 2.100g K1
2060 1.000g E1 + 1.050g K11 + 1.050g K12 + 0.448g K16 + 1.050g K7 + 1.050g K14
2061 1.000g E2 + 1.050g K11 + 1.050g K12 + 1.050g K7 + 0.448g K16 + 1.050g K24
2062 1.000g E3 + 1.050g Kl 1+ 1.050g K12 + 1.050g K8 + 1.050g K2 + 0.448g K16
2063 0.200gE4+0.448gK16+0.210gK11 + 0.210g K12 + 0.210g K9 + 0.210g K13
2064 0.200g E1 + 0.210g K11 + 0.448g K16 + 0.210g K12 + 0.210g K9 + 0.210g K1
2065 0.200g E2 + 0.210g K11 + 0.210g K12 + 0.448g K16 + 0.210g K9 + 0.210g K14
2066 2.000g E3 + 2.100g Kl l+ 2.100g K12 + 2.l00g K9 + 0.448g K16 + 2.l00g K24
2067 0.200g E4 + 0.210g K11 + 0.210g K12 + 0.210g K9 + 0.210g K2 + 0.448g K16
2068 0.200g E1 + 0.448g K16 + 0.210g K11 + 0.210g K12 + 0.210g K13 + 0.210g K1
2069 2.000g E2 + 2.l00g Kl 1+ 0.448g K16 + 2.l00g K12 + 2.l00g K13 + 2.100g
K14
2070 2.000g E3 + 2.100g K1 l+ 2.l00g K12 + 0.448g K16 + 2.100g K13 + 2.100g
K24
2071 1.000g E4 + 1.050g Kl l+ 1.050g K12 + 1.050g K13 + 0.448g K16 + 1.050g K2
2072 1.000g E1 + 1.050g K11 + 1.050g K12 + 1.050g K1 + 1.050g K14 + 0.448g K16
2073 0.200g E2 + 0.448g K16 + 0.210g K11 + 0.210g K12 + 0.210g K1 + 0.210g K24
2074 2.000g E3 + 2.l00g K11 + 0.448g K16 + 2.100g K12 + 2.l00g K1 + 2.l00g K2
2075 2.000g E4 + 2.100g Kl l+ 2.l00g K12 + 0.448g K16 + 2.100g K14 + 2.100g
K24
2076 1.000g E1 + 1.050g Kl l+ 1.050g K12 + 1.050g K14 + 0.448g K16 + 1.050g K2
2077 1.000g E2 + 1.050g K11 + 1.050g K12 + 1.050g K24 + 1.050g K2 + 0.448g K16
2078 1.667g E3 + 0.448g K16 + 1.750g Kl 1+ 1.750g K6
2079 1.250g E4 + 1.313g K11 + 0.448g K16 + 1.313g K6 + 1.313g K7
2080 1.250g E1 + 1.313g K11 + 1.313g K6 + 0.448g K16 + 1.313g K9
2081 1.250g E2 + 1.313g K11 + 1.313g K6 + 1.313g K13 + 0.448g K16
2082 2.500g E3 + 0.448g K16 + 2.625g K11 + 2.625g K6 + 2.625g K1
2083 0.250g E4 + 0.263g K11 + 0.448g K16 + 0.263g K6 + 0.263g K14
2084 0.250g El + 0.263g K11 + 0.263g K6 + 0.448g K16 + 0.263g K24
2085 1.250g E2 + 1.313g K11 + 1.313g K6 + 1.313g K2 + 0.448g K16
1 2086 2.000g E3 + 0.448g K16 + 2.100g K11 + 2.100g K6 + 2.100g K7 + 2.100g K9
CA 02646867 2008-12-16
W245FQ/JC 117
2087 2.000g E4 + 2.100g K11 + 0.448g K16 + 2.100g K6 + 2.100g K7 + 2.100g K13
2088 0.200g E1 + 0.210g K11 + 0.210g K6 + 0.448g K16 + 0.210g K7 + 0.210g K1
2089 1.000g E2 + 1.050g Kl 1 + 1.050g K6 + 1.050g K7 + 0.448g K16 + 1.050g K14
2090 1.000g E3 + 1.050g Kl 1+ 1.050g K6 + 1.050g K7 + 1.050g K24 + 0.448g K16
2091 1.000g E4 + 0.448g K16 + 1.050g K11 + 1.050g K6 + 1.050g K7 + 1.050g K2
2092 1.000g E1 + 1.050g K11 + 0.448g K16 + 1.050g K6 + 1.050g K9 + 1.050g K13
2093 0.200g E2 + 0.210g K11 + 0.210g K6 + 0.448g K16 + 0.210g K9 + 0.210g K1
2094 1.000g E3 + 1.050g K11 + 1.050g K6 + 1.050g K9 + 0.448g K16 + 1.050g K14
2095 2.000g E4 + 2.l00g K11 + 2.l00g K6 + 2. l00g K9 + 2.100g K24 + 0.448g K16
2096 0.200g E1 + 0.448g K16 + 0.210g K11 + 0.210g K6 + 0.210g K9 + 0.210g K2
2097 0.200g E2 + 0.210g K11 + 0.448g K16 + 0.210g K6 + 0.210g K13 + 0.210g K1
2098 2.000g E3 + 2.100g Kl l+ 2.100g K6 + 0.448g K16 + 2.100g K13 + 2.100g K14
2099 1.000g E4 + 1.050g Kl 1+ 1.050g K6 + 1.050g K13 + 0.448g K16 + 1.050g K24
2100 0.200gE1+0.210gK11+0.210gK6+0.210gK13+0.210gK2+0.448gK16
2101 2.000g E2 + 0.448g K16 + 2.l00g K11 + 2.l00g K6 + 2.l00g K1 + 2.l00g K14
2102 0.200g E3 + 0.210g K11 + 0.448g K16 + 0.210g K6 + 0.210g K1 + 0.210g K24
2103 2.000g E4 + 2.100g Kl l+ 2.100g K6 + 0.448g K16 + 2.100g K1 + 2.100g K2
2104 0.200g E1 + 0.210g K11 + 0.210g K6 + 0.210g K14 + 0.448g K16 + 0.210g K24
2105 2.000gE2+2.100gK11 + 2.100g K6 + 2.100g K14 + 2.100g K2 + 0.448g K16
2106 2.000g E3 + 0.448g K16 + 2.100g K11 + 2.100g K6 + 2.100g K24 + 2.100g K2
2107 1.667g E4 + 1.750g K11 + 0.448g K16 + 1.750g K7
2108 0.250g El + 0.263g K11 + 0.263g K21 + 0.448g K16 + 0.263g K9
2109 1.250g E2 + 1.313g K11 + 1.313g K7 + 1.313g K13 + 0.448g K16 + 1.013g K3
2110 0.250g E3 + 0.448g K16 + 0.263g K11 + 0.263g K7 + 0.263g K1
2111 1.250g E4 + 1.313g K11 + 0.448g K16 + 1.313g K7 + 1.313g K14
2112 0.250g El + 0.263g Kl 1+ 0.263g K7 + 0.448g K16 + 0.263g K24
2113 1.250g E2 + 1.313g K11 + 1.313g K7 + 1.313g K2 + 0.448g Kl6
2114 1.000g E3 + 0.448g Kl6 + 1.050g K1 l+ 1.050g K7 + 1.050g K9 + 1.050g K13
2115 1.000g E4 + 1.050g Kl l+ 0.448g K16 + 1.050g K7 + 1.050g K9 + 1.050g Kl
2116 0.200gE1+0.2lOgK11+0.210gK7+0.448gK16+0.210gK9+0.210gK14
2117 2.000g E2 + 2.100g K1 l+ 2.100g K7 + 2.100g K9 + 0.448g K16 + 2.100g K24
2118 2.000g E3 + 2.100g K11 + 2.100g K7 + 2.100g K9 + 2.100g K2 + 0.448g K16
CA 02646867 2008-12-16
W245FQ/JC 118
2119 2.000g E4 + 0.448g K16 + 2.100g Kl 1+ 2.100g K7 + 2.100g K13 + 2.100g K1
2120 1.000g E1 + 1.050g K11 + 0.448g K16 + 1.050g K7 + 1.050g K13 + 1.050g K14
2121 2.000g E2 + 2.100g Kl l+ 2.100g K8 + 0.448g K16 + 2.100g K13 + 2.100g K24
2122 0.200g E3 + 0.210g K11 + 0.210g K7 + 0.210g K13 + 0.448g K16 + 0.210g K2
2123 2.000g E4 + 2.100g K11 + 2.100g K7 + 2.100g K1 + 2.100g K14 + 1.651g K16
2124 1.000g E1 + 1.651g K16 + 1.050g K11 + 1.050g K7 + 1.050g K1 + 1.050g K24
2125 0.200g E2 + 0.210g K11 + 1.651g K16 + 0.210g K7 + 0.210g Kl + 0.210g K2
2126 2.000g E3 + 2.100g Kl 1+ 2.100g K7 + 1.651g K16 + 2.100g K14 + 2.100g K24
2127 1.000g E4 + 1.050g K11 + 1.050g K7 + 1.050g K14 + 1.651g K16 + 1.050g K2
2128 1.000g E1 + 1.050g K11 + 1.050g K7 + 1.050g K24 + 1.050g K2 + 1.651g K16
2129 0.333g E2 + 1.651g K16 + 0.350g K11 + 0.350g K9
2130 1.250gE3+1.313gK11+1.651gK16+1.313gK9+1.313gK13
2131 1.250gE4+1.313gK11+1.313gK9+1.651gK16+1.313gK1
2132 2.500g El + 2.625g K11 + 2.625g K9 + 2.625g K14 + 1.651g K16
2133 1.250g E2 + 1.651g K16 + 1.313g K11 + 1.313g K9 + 1.313g K24
2134 0.250g E3 + 1.863g K11 + 1.651g K16 + 0.263g K9 + 0.263g K2 + 0.410g K23
2135 1.000g E4 + 1.050g Kl l+ 1.050g K9 + 1.651g K16 + 1.050g K13 + 1.050g K1
2136 2.000g E1 + 2.100g K11 + 2.100g K9 + 2.100g K13 + 1.651g K16 + 2.100g K14
2137 0.200g E2 + 0.210g K11 + 0.210g K9 + 0.210g K13 + 0.210g K24 + 1.651g K16
2138 1.000g E3 + 1.651g K16 + 1.050g K11 + 1.050g K9 + 1.050g K13 + 1.050g K2
2139 0.200gE4+0.210gK11+1.651gK16+0.210gK9+0.210gK1+0.210gK14
2140 2.000g E1 + 2.100g Kl l+ 2.100g K9 + 1.651g K16 + 2.100g K1 + 2.100g K24
2141 2.000g E2 + 2.100g Kl 1+ 2.100g K9 + 2.100g K1 + 1.651g K16 + 2.100g K2
2142 1.000g E3 + 1.050g K11 + 1.050g K9 + 1.050g K14 + 1.050g K24 + 1.651g K16
2143 0.200gE4+1.651gK16+0.2lOgK11+0.210gK9+0.210gK14+0.210gK2
2144 0.200g E1 + 0.2lOg Kl l+ 1.651g K16 + 0.210g K9 + 0.210g K24 + 0.210g K2
2145 0.333g E2 + 0.350g Kl 1+ 0.350g K13 + 1.651g K16
2146 1.250g E3 + 1.651g K16 + 1.313g K11 + 1.313g K13 + 1.313g K1
2147 1.250gE4+1.313gK11+1.651gK16+1.313gK13+1.313gK14
2148 1.250gE1+1.313gK11+1.313gK13+1.651gK16+1.313gK24
2149 0.250g E2 + 0.263g K11 + 0.263g K13 + 0.263g K2 + 1.651g K16
2150 1.000g E3 + 1.651g K16 + 1.050g K11 + 1.050g K13 + 1.050g Kl + 1.050g K14
CA 02646867 2008-12-16
W245FQ/JC 119
2151 2.000g E4 + 2.l00g Kl 1+ 1.65lg K16 + 2.100g K13 + 2.l00g K1 + 2.100g K24
2152 0.200g El + 0.210g K11 + 0.210g K13 + 1.651g K16 + 0.210g K1 + 0.210g K2
2153 0.200gE2+0.210gK11+0.210gK13+0.210gK14+1.651gK16+0.214gK24
2154 1.000g E3 + 1.050g K11 + 1.050g K13 + 1.050g K14 + 1.050g K2 + 1.651g K16
2155 1.000g E4 + 1.651g K16 + 1.050g K11 + 1.050g K13 + l.050g K24 + 1.050g K2
2156 0.333g E1 + 0.350g K11 + 1.651g K16 + 0.350g K1
2157 2.500g E2 + 2.625g K11 + 2.625g K1 + 1.651g K16 + 2.625g K14
2158 0.250g E3 + 0.263g K11 + 0.263g K1 + 0.263g K24 + 1.651g K16
2159 0.250g E4 + 1.651g K16 + 0.263g K11 + 0.263g K1 + 0.263g K2
2160 1.000g E1 + 1.050g K11 + 1.651g K16 + 1.050g K1 + 1.050g K14 + 1.050g K24
2161 1.000g E2 + 1.050g K11 + 1.050g K1 + 1.651g K16 + 1.050g K14 + 1.050g K2
2162 1.000g E3 + 1.050g K11 + 1.050g K1 + 1.050g K24 + 1.651g K16 + 1.050g K2
2163 2.500g E1 + 2.625g K11 + 1.651g K16
2164 3.333g El + 1.651g K16 + 3.500g K11 + 3.500g K14
2165 3.333g E2 + 3.500g K11 + 1.651g K16 + 3.500g K24
2166 3.333g E3 + 3.500g K11 + 3.500g K2 + 1.651g K16
2167 0.250g E4 + 1.651g K16 + 0.263g K11 + 0.263g K14 + 0.263g K24
2168 0.250g El + 0.263g K11 + 1.651g K16 + 0.263g K14 + 0.263g K2
2169 1.250gE2+ 1.313gK11 + 1.313gK24+ 1.651gK16+ 1.313gK2
2170 0.200gE3 +0.210gK11 +0.210gK14+0.210gK24+ 1.651gK16+0.210gK2
2171 2.500g E4 + 2.625g K14 + 2.500g E8 + 2.625g K12 + 1.651g K16
2172 1.250g E1 + 1.651g K16 + 1.313g K14 + 1.250g E8 + 1.313g K6
2173 0.250g E2 + 0.263g K14 + 1.651g K16 + 0.250g E8 + 0.263g K21
2174 2.500g E3 + 2.625g K14 + 2.500g E8 + 1.651g K16 + 2.625g K9
2175 1.250g E4 + 1.313g K14 + 1.250g E8 + 1.313g K13 + 1.65lg K16
2176 2.500g El + 1.651g K16 + 2.625g K14 + 2.500g E8 + 2.625g Kl
2177 1.250g E2 + 1.313g K14 + 1.651g K16 + 1.250g E8 + 1.313g K11
2178 0.250g E3 + 0.263g K14 + 0.250g E8 + 1.651g K16 + 0.050g K3 + 0.263g K24
2179 1.250g E4 + 1.313g K14 + 1.250g E8 + 1.313g K2 + 1.651g K16
2180 1.000g E1 + 1.651g K16 + 1.050g K14 + 1.000g E8 + 1.050g K12 + 1.050g K6
2181 1.000g E2 + 1.050g K14 + 1.651g K16 + 1.000g E8 + 1.050g K12 + 1.050g K7
2182 2.000g E3 + 2.100g K14 + 2.000g E8 + 1.651g K16 + 2.100g K12 + 2.100g K9
CA 02646867 2008-12-16
W245FQ/JC 120
2183 1.000g E4 + 1.050g K14 + 1.000g E8 + 0.050g K3 + 1.050g K12 + 1.651g K16
+
1.050g K13
2184 0.200g El + 0.210g K14 + 0.200g E8 + 0.210g K12 + 0.210g K1 + 1.651g K16
2185 2.000g E2 + 1.651g K16 + 2.100g K14 + 2.000g E8 + 2.100g K12 + 2.100g K11
2186 1.000g E3 + 1.050g K14 + 1.651g K16 + 1.000g E8 + 1.050g K12 + 1.050g K24
2187 1.000g E4 + 1.050g K14 + 1.000g E8 + 1.651g K16 + 1.050g K12 + 1.050g K2
2188 1.000g E1 + 1.050g K14 + 1.000g E8 + 1.050g K6 + 1.651g K16 + 1.050g K7
2189 1.000g E2 + 1.050g K14 + 1.000g E8 + 1.050g K6 + 1.050g K9 + 1.651g K16
2190 0.200gE3+1.651gK16+0.210gK14+0.200gE8+0.210gK6+0.210gK13
2191 2.000g E4 + 2.100g K14 + 1.651gK16+2.000gE8+2.100gK6+2.100gK1
2192 0.200g E 1+ 0.210g K 14 + 0.200g E8 + 0.050g K3 + 1.651 g K 16 + 0.210g
K6 +
0.210g K11
2193 2.000g E2 + 2.100g K14 + 2.000g E8 + 2.100g K6 + 1.651gK16+2.100gK24
2194 1.000g E3 + 1.050g K14 + 1.000g E8 + 1.050g K6 + 1.050g K2 + 1.651g K16
2195 0.200g E4 + 1.651g K16 + 0.210g K14 + 0.200g E8 + 0.210g K7 + 0.210g K9
2196 0.200g E1 + 0.210g K14 + 1.651g K16 + 0.200g E8 + 0.210g K7 + 0.210g K13
2197 2.000g E2 + 2.100g K14 + 2.000g E8 + 1.651g K16 + 2.100g K7 + 2.100g Kl
2198 0.200g E3 + 0.210g K14 + 0.200g E8 + 0.210g K7 + 1.651g K16 + 0.210g K11
2199 0.200g E4 + 0.210g K14 + 0.200g E8 + 0.210g K7 + 0.210g K24 + 1.651 g K16
2200 1.000g El + 1.651g K16 + 1.050g K14 + 1.000g E8 + 1.050g K7 + 1.050g K2
2201 2.000g E2 + 2.100g K14 + 1.651g K16 + 2.000g E8 + 2.100g K9 + 2.100g K13
2202 2.000g E3 + 2.100g Kl4 + 2.000g E8 + 1.651g K16 + 2.100g K9 + 2.100g Kl
2203 0.200g E4 + 0.210g K14 + 0.200g E8 + 0.210g K9 + 1.651g K16 + 0.210g K11
2204 1.000g El + 1.050g K14 + 1.000g E8 + 1.050g K9 + 1.050g K24 + 1.651g K16
2205 1.000g E2 + 1.651g K16 + 1.050g K14 + 1.000g E8 + 1.050g K9 + 1.050g K2
2206 2.000g E3 + 2.100g K14 + 1.651g K16 + 2.000g E8 + 2.100g K13 + 2.100g Kl
2207 2.000g E4 + 2.100g K14 + 2.000g E8 + 1.651g K16 + 2.100g K22 + 2.100g K11
2208 1.000g E1 + 1.050g K14 + 1.000g E8 + 1.050g K22 + 1.651g K16 + 1.050g K24
2209 2.000g E2 + 2.100g K14 + 2.000g E8 + 2.100g K13 + 2.100g K2 + 1.651g K16
2210 2.000g E3 + 1.651g K16 + 2.100g K14 + 2.000g E8 + 2.l00g K1 + 2.100g K11
2211 0.200g E4 + 0.210g K14 + 1.651g K16 + 0.200g E8 + 0.210g K1 + 0.210g K24
2212 2.000g E1 + 2.100g K14 + 2.000g E8 + 1.651g K16 + 2.100g Kl + 2.100g K2
CA 02646867 2008-12-16
W245FQ/JC 121
2213 2.OOOg E2 + 2.100g K14 + 2.000g E8 + 2.100g K1 l+ 1.651g K16 + 2.100g K24
2214 0.200g E3 + 0.210g K14 + 0.200g E8 + 0.210g K11 + 0.210g K2 + 1.854g Kl6
2215 0.200g E4 + 1.854g K16 + 0.210g K14 + 0.200g E8 + 0.210g K24 + 0.210g K2
2216 0.250g El + 0.263g K14 + 1.854g K16 + 0.250g E6 + 0.263g K12
2217 1.250g E2 + 1.313g K14 + 1.250g E6 + 1.854g K16 + 1.313g K6
2218 1.250g E3 + 1.313g K14 + 1.250g E6 + 1.313g K7 + 1.854g K16
2219 2.500g E4 + 1.854g K16 + 2.625g K14 + 2.500g E6 + 2.625g K9
2220 1.250g E1 + 1.313g K14 + 1.854g K16 + 1.250g E6 + 1.313g K22
2221 1.250g E2 + 1.313g K14 + 1.250g E6 + 1.854g K16 + 1.313g K1
2222 1.250gE3+1.313gK14+1.250gE6+1.313gK11+1.854gK16
2223 1.250g E4 + 1.854g K16 + 1.313g K14 + 1.250g E6 + 1.313g K24
2224 2.500g El + 2.625g K14 + 1.854g K16 + 2.500g E6 + 2.625g K2
2225 2.000g E2 + 2.100g K14 + 2.000g E6 + 1.854g K16 + 2. l00g K12 + 2.100g K6
2226 1.000g E3 + 1.050g K14 + 1.000g E6 + 1.050g K12 + 1.854g K16 + 1.050g K7
2227 0.200g E4 + 0.210g K14 + 0.200g E6 + 0.210g K12 + 0.210g K9 + 1.854g K16
2228 1.000g El + 1.854g K16 + 1.050g K14 + 1.000g E6 + 1.050g K12 + 1.050g K13
2229 1.000g E2 + 1.050g K14 + 1.854g K16 + 1.000g E6 + 1.050g K12 + 1.050g K1
2230 1.000g E3 + 1.050g K14 + 1.000g E6 + 1.854g K16 + 1.050g K12 + 1.050g K11
2231 1.000g E4 + 1.050g K14 + 1.000g E6 + 1.050g K12 + 1.854g K16 + 1.050g K24
2232 2.000g El + 2.100g K14 + 2.000g E6 + 2.100g K12 + 2.100g K2 + 1.854g K16
2233 1.000g E2 + 1.854g K16 + 1.050g K14 + 1.000g E6 + 1.050g K6 + 1.050g K7
2234 2.000g E3 + 2.100g K14 + 1.854g K16 + 2.000g E6 + 2.100g K6 + 2.100g K9
2235 0.200g E4 + 0.210g K14 + 0.200g E6 + 1.854g K16 + 0.210g K6 + 0.210g K13
2236 0.200g El + 0.210g K14 + 0.200g E6 + 0.210g K6 + 1.854g K16 + 0.210g K1
2237 0.200g E2 + 0.210g K14 + 0.200g E6 + 0.210g K6 + 0.210g K11 + 1.854g K16
2238 0.200g E3 + 1.854g K16 + 0.210g K14 + 0.200g E6 + 0.210g K6 + 0.210g K24
2239 2.000g E4 + 2.100g K14 + 1.854g K16 + 2.000g E6 + 2.100g K6 + 2.100g K2
2240 1.000g E1 + 1.050g K14 + 1.000g E6 + 1.854g K16 + 1.050g K7 + 1.050g K9
2241 1.000g E2 + 1.050g K14 + 1.000g E6 + 1.050g K7 + 1.854g K16 + 1.050g K13
2242 0.200g E3 + 0.210g K14 + 0.200g E6 + 0.210g K8 + 0.210g K1 + 1.854g K16
2243 2.000g E4 + 1.854g K16 + 2.100g K14 + 2.000g E6 + 2.100g K7 + 2.100g K11
2244 0.200g E1 + 0.210g K14 + 1.854g K16 + 0.200g E6 + 0.210g K7 + 0.210g K24
CA 02646867 2008-12-16
W245FQ/JC 122
2245 0.200g E2 + 0.210g K14 + 0.200g E6 + 1.854g K16 + 0.210g K7 + 0.210g K2
2246 1.000g E3 + 1.050g K14 + 1.000g E6 + 1.050g K9 + 1.854g K16 + 1.050g K13
2247 2.000g E4 + 2.100g K14 + 2.000g E6 + 2.100g K9 + 2.100g Kl + 1.854g K16
2248 0.200g El + 1.854g K16 + 0.210g K14 + 0.200g E6 + 0.210g K9 + 0.210g K11
2249 1.000g E2 + 1.050g K14 + 1.854g K16 + 1.000g E6 + 1.050g K9 + 1.050g K24
2250 1.000g E3 + 1.050g K14 + 1.000g E6 + 1.854g K16 + 1.050g K9 + 1.050g K2
2251 2.000g E4 + 2.100g K14 + 2.000g E6 + 2.100g K13 + 1.854g K16 + 2.100g Kl
2252 0.200g E1 + 0.210g K14 + 0.200g E6 + 0.210g K13 + 0.210g K11 + 1.854g K16
2253 2.000g E2 + 1.854g K16 + 2.100g Kl4 + 2.000g E6 + 2.100g K13 + 2.100g K24
2254 0.200g E3 + 0.210g K14 + 1.854g K16 + 0.200g E6 + 0.210g K13 + 0.210g K2
2255 0.200g E4 + 0.210g K14 + 0.200g E6 + 1.854g K16 + 0.210g K1 + 0.210g K11
2256 0.200g E1 + 0.210g K14 + 0.200g E6 + 0.210g K1 + 1.854g K16 + 0.210g K24
2257 2.000g E2 + 2.100g K14 + 2.000g E6 + 2.100g Kl + 2.100g K2 + 1.854g K16
2258 2.000g E3 + 1.854g K16 + 2.100g K14 + 2.000g E6 + 2.100g K1 l+ 2.100g K24
2259 1.000g E4 + 1.050g K14 + 1.854g K16 + 1.000g E6 + 1.050g K11 + 1.050g K2
2260 0.200g El + 0.210g K14 + 0.200g E6 + 1.854g K16 + 0.210g K24 + 0.210g K2
2261 0.250g E2 + 0.263g K14 + 0.250g E5 + 0.263g K12 + 1.854g K16
2262 1.250g E3 + 1.854g K16 + 1.313g K14 + 1.250g E5 + 1.313g K6
2263 1.250g E4 + 1.313g K14 + 1.854g K16 + 1.250g E5 + 1.313g K7
2264 1.250g E1 + 1.313g K14 + 1.250g E5 + 1.854g K16 + 1.313g K9
2265 2.500g E2 + 2.625g K14 + 2.500g E5 + 2.625g K13 + 1.854g K16
2266 2.500g E3 + 1.854g K16 + 2.625g K14 + 2.500g E5 + 2.625g Kl
2267 1.250g E4 + 1.313g K14 + 1.854g K16 + 1.250g E5 + 1.313g K11
2268 0.250g El + 0.263g K14 + 0.250g E5 + 1.854g K16 + 0.263g K24
2269 2.500g E2 + 2.625g K14 + 2.500g E5 + 2.625g K2 + 1.854g K16
2270 2.000g E3 + 1.854g K16 + 2.100g K14 + 2.000g E5 + 2.100g K12 + 2.100g K6
2271 2.000g E4 + 2.100g K14 + 1.854g K16 + 2.000g E5 + 2.100g K12 + 2.100g K7
2272 1.000g E1 + 1.050g K14 + 1.000g E5 + 1.854g K16 + 1.050g K12 + 1.050g K9
2273 1.000g E2 + 1.050g K14 + 1.000g E5 + 1.050g K12 + 1.854g K16 + 1.050g K13
2274 0.200g E3 + 0.210g K14 + 0.200g E5 + 0.210g K12 + 0.210g K1 + 1.854g K16
2275 1.000g E4 + 1.854g K16 + 1.050g K14 + 1.000g E5 + 1.050g K12 + 1.050g Kl
1
2276 0.200g E1 + 0.210g K14 + 1.854g K16 + 0.200g E5 + 0.210g K12 + 0.210g K24
CA 02646867 2008-12-16
W245FQ/JC 123
2277 2.000g E2 + 2.100g K14 + 2.000g E5 + 1.854g K16 + 2.100g K12 + 2.100g K2
2278 1.000g E3 + 1.050g K14 + 1.000g E5 + 1.050g K6 + 1.854g K16 + 1.050g K7
2279 0.200g E4 + 0.210g K14 + 0.200g E5 + 0.210g K6 + 0.210g K9 + 1.854g K16
2280 2.000g El + 1.854g K16 + 2.100g K14 + 2.000g E5 + 2.100g K6 + 2.100g K13
2281 2.000g E2 + 2.100g K14 + 1.854g K16 + 2.000g E5 + 2.100g K6 + 2.100g Kl
2282 0.200g E3 + 0.210g K14 + 0.200g E5 + 1.854g K16 + 0.210g K6 + 0.210g K11
2283 2.000g E4 + 2.100g K14 + 2.000g E5 + 2.100g K6 + 1.854g K16 + 2.100g K24
2284 0.200g El + 0.210g K14 + 0.200g E5 + 0.210g K6 + 0.210g K2 + 1.854g K16
2285 1.000g E2 + 1.854g K16 + 1.050g K14 + 1.000g E5 + 1.050g K21 + 1.050g K9
2286 0.200g E3 + 0.210g K14 + 1.854g K16 + 0.200g E5 + 0.210g K7 + 0.210g K13
2287 1.000g E4 + 1.050g K14 + 1.000g E5 + 1.854g K16 + 1.050g K7 + 1.050g K1
2288 0.200g E1 + 0.210g K14 + 0.200g E5 + 0.210g K7 + 1.854g K16 + 0.210g K11
2289 1.000g E2 + 1.050g K14 + 1.000g E5 + 1.050g K7 + 1.050g K24 + 1.854g K16
2290 0.200g E3 + 1.854g K16 + 0.210g K14 + 0.200g E5 + 0.210g K7 + 0.210g K2
2291 2.000g E4 + 2.100g K14 + 1.854g K16 + 2.000g E5 + 2.100g K9 + 2.100g K13
2292 2.000g El + 2.100g K14 + 2.000g E5 + 1.854g K16 + 2.100g K9 + 2.100g K1
2293 2.000g E2 + 2.100g K14 + 2.000g E5 + 2.100g K9 + 1.854g K16 + 2.100g K11
2294 1.000g E3 + 1.050g K14 + 1.000g E5 + 1.050g K9 + 1.050g K24 + 1.854g K16
2295 0.200g E4 + 1.854g K16 + 0.210g K14 + 0.200g E5 + 0.210g K9 + 0.210g K2
2296 1.000g E1 + 1.050g K14 + 1.854g K16 + 1.000g E5 + 1.050g K13 + 1.050g K1
2297 0.200g E2 + 0.210g K14 + 0.200g E5 + 1.854g K16 + 0.210g K13 + 0.210g K11
2298 2.000g E3 + 2.100g K14 + 2.000g E5 + 2.100g K13 + 1.854g K16 + 2.100g K24
2299 2.000g E4 + 2.100g K14 + 2.000g E5 + 2.100g K22 + 2.100g K2 + 1.854g K16
2300 0.200g El + 1.854g K16 + 0.210g K14 + 0.200g E5 + 0.210g K1 + 0.210g K11
2301 1.000g E2 + 1.050g K14 + 0.057g K16 + 1.000g E5 + 1.050g K1 + 1.050g K24
2302 2.000g E3 + 2.100g K14 + 2.000g E5 + 0.057g K16 + 2.100g K1 + 2.100g K2
2303 2.000g E4 + 2.100g K14 + 2.000g E5 + 2.100g K11 + 0.057g K16 + 2.100g K24
2304 0.200g El + 0.210g K14 + 0.200g E5 + 0.210g K11 + 0.210g K2 + 0.057g K16
2305 1.000g E2 + 0.057g K16 + 1.050g K14 + 1.000g E5 + 1.050g K24 + 1.050g K2
2306 1.250g E3 + 1.313g K14 + 0.057g K16 + 1.250g E7 + 1.313g K12
2307 1.250g E4 + 1.313g K14 + 1.250g E7 + 0.057g K16 + 1.313g K6
2308 1.250g E1 + 1.313g K14 + 1.250g E7 + 1.313g K7 + 0.057g K16
CA 02646867 2008-12-16
W245FQ/JC 124
2309 1.250g E2 + 0.057g K16 + 1.313g K14 + 1.250g E7 + 1.313g K9
2310 0.250g E3 + 0.263g K14 + 0.057g K16 + 0.250g E7 + 0.263g K13
2311 1.250g E4 + 1.313g K14 + 1.250g E7 + 0.057g K16 + 1.313g K1
2312 0.250g El + 0.263g K14 + 0.250g E7 + 0.263g Kl 1+ 0.057g K16
2313 2.500g E2 + 0.057g K16 + 2.625g K14 + 2.500g E7 + 2.625g K24
2314 0.250g E3 + 0.263g K14 + 0.057g K16 + 0.250g E7 + 0.263g K2
2315 0.200g E4 + 0.210g K14 + 0.200g E7 + 0.057g K16 + 0.210g K12 + 0.210g K6
2316 2.000g E1 + 2.100g K14 + 2.000g E7 + 2.100g K12 + 0.057g K16 + 2.100g K7
2317 2.000g E2 + 2.100g K14 + 2.000g E7 + 2.100g K12 + 2.100g K9 + 0.057g K16
2318 0.200g E3 + 0.057g K16 + 0.210g K14 + 0.200g E7 + 0.210g K12 + 0.210g K13
2319 1.000g E4 + 1.050g K14 + 0.057g K16 + 1.000g E7 + 1.050g K12 + 1.050g Kl
2320 0.200g E1 + 0.210g K14 + 0.200g E7 + 0.057g K16 + 0.210g K12 + 0.210g K11
2321 2.000g E2 + 2.100g K14 + 2.000g E7 + 2.100g K12 + 0.057g K16 + 2.100g K24
2322 1.000g E3 + 1.050g K14 + 1.000g E7 + 1.050g K12 + l.050g K2 + 0.057g K16
2323 1.000g E4 + 0.057g K16 + 1.050g K14 + 1.000g E7 + 1.050g K6 + 1.050g K7
2324 0.200g E1 + 0.210g K14 + 0.057g K16 + 0.200g E7 + 0.210g K6 + 0.210g K9
2325 1.000g E2 + 1.050g K14 + 1.000g E7 + 0.057g K16 + 1.050g K6 + 1.050g K13
2326 2.000g E3 + 2.100g K14 + 2.000g E7 + 2.100g K6 + 0.057g K16 + 2.100g K1
2327 0.200g E4 + 0.210g K14 + 0.200g E7 + 0.210g K6 + 0.210g K11 + 0.057g K16
2328 0.200g El + 0.057g K16 + 0.210g K14 + 0.200g E7 + 0.210g K6 + 0.210g K24
2329 0.200g E2 + 0.210g K14 + 0.057g K16 + 0.200g E7 + 0.210g K6 + 0.210g K2
2330 0.200g E3 + 0.210g K14 + 0.200g E7 + 0.057g K16 + 0.210g K7 + 0.210g K9
2331 1.000g E4 + 1.050g K14 + 1.000g E7 + 1.050g K7 + 0.057g K16 + 1.050g K13
2332 2.000g El + 2.100g K14 + 2.000g E7 + 2.100g K7 + 2.100g K1 + 0.057g K16
2333 1.000g E2 + 0.057g K16 + 1.050g K14 + 1.000g E7 + 1.050g K7 + 1.050g K11
2334 0.200g E3 + 0.210g K14 + 0.057g K16 + 0.200g E7 + 0.210g K7 + 0.210g K24
2335 0.200g E4 + 0.210g K14 + 0.200g E7 + 0.057g K16 + 0.210g K7 + 0.210g K2
2336 2.000g El + 2.100g K14 + 2.000g E7 + 2.100g K9 + 0.057g K16 + 2.100g K13
2337 2.000g E2 + 2.100g K14 + 2.000g E7 + 2.100g K9 + 2.100g K1 + 0.057g K16
2338 0.200g E3 + 0.057g K16 + 0.210g K14 + 0.200g E7 + 0.2lOg K9 + 0.210g K11
2339 0.200g E4 + 0.210g K14 + 0.057g K16 + 0.200g E7 + 0.210g K9 + 0.210g K24
2340 0.200g El + 0.210g K14 + 0.200g E7 + 0.057g K16 + 0.210g K9 + 0.210g K2
CA 02646867 2008-12-16
W245FQ/JC 125
2341 2.000g E2 + 2.100g K14 + 2.000g E7 + 2.100g K13 + 0.057g K16 + 2.100g Kl
2342 1.000g E3 + 1.050g K14 + 1.000g E7 + 1.050g K13 + 1.050g K11 + 0.057g K16
2343 2.000g E4 + 0.057g K16 + 2.100g K14 + 2.000g E7 + 2.100g K22 + 2.100g K24
2344 1.000g El + 1.050g K14 + 0.057g K16 + 1.000g E7 + 1.050g K13 + 1.050g K2
2345 0.200g E2 + 0.210g K14 + 0.200g E7 + 0.057g K16 + 0.210g K1 + 0.210g K11
2346 0.200g E3 + 0.210g K14 + 0.200g E7 + 0.210g K1 + 0.057g K16 + 0.210g K24
2347 0.200g E4 + 0.210g K14 + 0.200g E7 + 0.210g K1 + 0.210g K2 + 0.057g K16
2348 0.200g El + 0.057g K16 + 0.210g K14 + 0.200g E7 + 0.210g K11 + 0.210g K24
2349 2.000g E2 + 2.100g K14 + 0.057g K16 + 2.000g E7 + 2.100g K11 + 2.100g K2
2350 0.200g E3 + 0.210g K14 + 0.200g E7 + 0.057g K16 + 0.210g K24 + 0.210g K2
2351 3.333g E4 + 3.500g K14 + 3.500g K12 + 0.057g K16
2352 1.250g E1 + 0.057g K16 + 1.313g K14 + 1.313g K12 + 1.313g K6
2353 0.250g E2 + 0.263g K14 + 0.057g K16 + 0.263g K12 + 0.263g K8
2354 2.500g E3 + 2.625g K14 + 2.625g K12 + 0.057g K16 + 2.625g K9
2355 2.500g E4 + 2.625g K14 + 2.625g K12 + 2.625g K13 + 0.057g K16
2356 0.250g El + 0.057g K16 + 0.263g K14 + 0.263g K12 + 0.263g K1
2357 1.250g E2 + 1.313g K14 + 0.057g K16 + 1.313g K12 + 1.313g K11
2358 1.250g E3 + 1.313g K14 + 1.313g K12 + 0.057g K16 + 1.313g K24
2359 2.500g E4 + 2.625g K14 + 2.625g K12 + 2.625g K2 + 0.057g K16
2360 0.200gE1 + 0.057g K16 + 0.210g K14 + 0.210g K12 + 0.210g K6 + 0.210g K7
2361 1.000g E2 + 1.050g K14 + 0.057g K16 + 1.050g K12 + 1.050g K6 + 1.050g K9
2362 1.000g E3 + 1.050g K14 + 1.050g K12 + 0.057g K16 + 1.050g K6 + 1.050g K13
2363 2.000g E4 + 2.100g K14 + 2.100g K12 + 2.100g K6 + 0.057g K16 + 2.100g K1
2364 1.000g El + 1.050g K14 + 1.050g K12 + 1.050g K6 + 1.050g K11 + 0.057g K16
2365 1.000g E2 + 0.057g K16 + 1.050g K14 + 1.050g K12 + 1.050g K6 + 1.050g K24
2366 2.000g E3 + 2.100g K14 + 0.057g K16 + 2. l00g K12 + 2.100g K6 + 2.100g K2
2367 2.000g E4 + 2.100g K14 + 2.l00g K12 + 0.057g K16 + 2.100g K7 + 2.100g K9
2368 1.000g El + 1.050g K14 + 1.050g K12 + 1.050g K7 + 0.057g K16 + 1.050g K13
2369 0.200g E2 + 0.210g K14 + 0.210g K12 + 0.210g K7 + 0.210g K1 + 0.057g K16
2370 0.200gE3+0.057gK16+0.210gK14+0.210gK12+0.210gK7+0.210gK11
2371 1.000g E4 + 1.050g K14 + 0.057g K16 + 1.050g K12 + 1.050g K21 + 1.050g
K24
2372 0.200gE1 + 0.210g K14 + 0.210g K12 + 0.057g K16 + 0.210g K7 + 0.210g K2
CA 02646867 2008-12-16
W245FQ/JC 126
2373 1 .000g E2 + 1.050g K14 + 1.050g K12 + l.050g K9 + 0.057g K16 + 1.050g
K13
2374 2.000g E3 + 2.100g K14 + 2.100g K12 + 2.100g K9 + 2.100g Kl + 0.057g K16
2375 2.000g E4 + 0.057g K16 + 2.100g K14 + 2.100g K12 + 2.100g K9 + 2.100g K11
2376 0.200g E1 + 0.210g K14 + 0.057g K16 + 0.210g K12 + 0.210g K9 + 0.210g K24
2377 0.200g E2 + 0.210g K14 + 0.210g K12 + 0.057g K16 + 0.210g K9 + 0.210g K2
2378 0.200g E3 + 0.210g K14 + 0.210g K12 + 0.210g K13 + 0.057g K16 + 0.210g K1
2379 1.000g E4 + 1.050g K14 + 1.050g K12 + 1.050g K13 + 1.050g K1 l+ 0.057g
K16
2380 2.000g El + 0.057g K16 + 2.100g K14 + 2.100g K12 + 2.100g K13 + 2.100g
K24
2381 1.000g E2 + 1.050g K14 + 0.057g K16 + 1.050g K12 + 1.050g K13 + 1.050g K2
2382 1.000g E3 + l.050g K14 + 1.050g K12 + 0.057g K16 + 1.050g K1 + 1.050g K11
2383 1.000g E4 + 1.050g K14 + 1.050g K12 + 1.050g KI + 0.057g K16 + 1.050g K24
2384 2.000gE1 +2.100gK14+2.100gK12+2.100gK1 + 2.100g K2 + 0.057g K16
2385 2.000gE2+0.057gK16+2.100gK14+2.100gK12+2.100gK11 +2.100gK24
2386 0.200g E3 + 0.210g K14 + 0.057g K16 + 0.210g K12 + 0.210g K11 + 0.210g K2
2387 1.000g E4 + 1.050g K14 + 1.050g K12 + 0.057g K16 + 1.050g K24 + 1.050g K2
2388 1.667g E1 + 1.750g K14 + 1.750g K6 + 0.057g K16 + O.O1Og K23
2389 2.500g E2 + 0.057g K16 + 2.625g K14 + 2.625g K6 + 2.625g K7
2390 2.500g E3 + 2.625g K14 + 0.057g K16 + 2.625g K6 + 2.625g K9
2391 0.250g E4 + 0.263g K14 + 0.263g K6 + 0.057g K16 + 0.263g K13
2392 0.250g El + 0.263g K14 + 0.263g K6 + 0.263g K1 + 0.260g K16
2393 2.500g E2 + 0.260g K16 + 2.625g K14 + 2.625g K6 + 2.625g K11
2394 2.500g E3 + 2.625g K14 + 0.260g K16 + 2.625g K6 + 2.625g K24
2395 2.500g E4 + 2.625g K14 + 2.625g K6 + 0.260g K16 + 2.625g K2
2396 2.000g E1 + 2.100g K14 + 2. l00g K6 + 2. l00g K7 + 0.260g K16 + 2.100g K9
2397 1.000g E2 + 1.050g K14 + 1.050g K6 + 1.050g K7 + 1.050g K13 + 0.260g K16
2398 1.000g E3 + 0.260g K16 + 1.050g K14 + 1.050g K6 + 1.050g K7 + 1.050g Kl
2399 0.200g E4 + 0.210g K14 + 0.260g K16 + 0.210g K6 + 0.210g K7 + 0.210g K11
2400 1.000g El + 1.050g K14 + 1.050g K6 + 0.260g K16 + 1.050g K7 + 1.050g K24
2401 2.000g E2 + 2. l00g K14 + 2. l00g K6 + 2. l00g K7 + 0.260g K16 + 2.100g
K2
2402 1.000g E3 + 1.050g K14 + 1.050g K6 + 1.050g K9 + 1.050g K13 + 0.260g K16
2403 2.000gE4+0.260gK16+2.100gK14+2.100gK6+2.100gK9+2.100gK1
2404 0.200gE1 +0.210gK14+0.260gK16+0.210gK6+0.210gK9+0.210gK11
CA 02646867 2008-12-16
W245FQ/JC 127
2405 0.200g E2 + 0.210g K14 + 0.210g K6 + 0.260g K16 + 0.210g K9 + 0.210g K24
2406 1.000g E3 + 1.050g K14 + l.050g K6 + 1.050g K9 + 0.260g K16 + 1.050g K2
2407 1.000g E4 + 1.050g K14 + 1.050g K6 + 1.050g K13 + 1.050g K1 + 0.260g K16
2408 2.000g El + 0.260g K16 + 2.100g K14 + 2.100g K6 + 2.100g K13 + 2.100g K11
2409 2.000g E2 + 2.100g K14 + 0.260g K16 + 2.100g K6 + 2.100g K13 + 2.100g K24
2410 1.000g E3 + 1.050g K14 + 1.050g K6 + 0.260g K16 + 1.050g K13 + 1.050g K2
2411 0.200gE4+0.210gK14+0.210gK6+0.210gK1 +0.260gK16+0.210gK11
2412 0.200gE1 +0.210gK14+0.210gK6+0.210gK1 + 0.210g K24 + 0.260g K16
2413 1.000g E2 + 0.260g K16 + 1.050g K14 + 1.050g K6 + 1.050g K1 + 1.050g K2
2414 0.200g E3 + 0.210g K14 + 0.260g K16 + 0.210g K6 + 0.210g K11 + 0.210g K24
2415 1.000g E4 + 1.050g K14 + 1.050g K6 + 0.260g K16 + 1.050g K11 + 1.050g K2
2416 1.000g El + 1.050g K14 + 1.050g K6 + 1.050g K24 + 0.260g K16 + 1.050g K2
2417 1.667g E2 + 1.750g K14 + 1.750g K7 + 0.260g K16
2418 1.250g E3 + 0.260g K16 + 1.313g K14 + 1.313g K7 + 1.313g K9
2419 0.250g E4 + 0.263g K14 + 0.260g K16 + 0.263g K7 + 0.263g K22
2420 1.250g E1 + 1.313g K14 + 1.313g K7 + 0.260g K16 + 1.313g K1
2421 0.250g E2 + 0.263g K14 + 0.263g K7 + 0.263g K11 + 0.260g K16
2422 0.250g E3 + 0.260g K16 + 0.263g K14 + 0.263g K7 + 0.263g K24
2423 2.500g E4 + 2.625g K14 + 0.260g K16 + 2.625g K7 + 2.625g K2
2424 2.000g E1 + 2.100g K14 + 2.100g K8 + 0.260g K16 + 2.100g K9 + 2.100g K13
2425 2.000g E2 + 2.100g K14 + 2.100g K7 + 2.100g K9 + 0.260g K16 + 2.100g K1
2426 0.200g E3 + 0.210g K14 + 0.210g K7 + 0.210g K9 + 0.210g K11 + 0.260g K16
2427 2.000g E4 + 0.260g K16 + 2.100g K14 + 2.100g K7 + 2.100g K9 + 2.100g K24
2428 2.000g El + 2.100g K14 + 0.260g K16 + 2.100g K7 + 2.100g K9 + 2.100g K2
2429 1.000g E2 + 1.050g K14 + 1.050g K21 + 0.260g K16 + 1.050g K13 + 1.050g K1
2430 1.000g E3 + 1.050g K14 + 1.050g K7 + 1.050g K13 + 0.260g K16 + 1.050g K11
2431 1.000g E4 + 1.050g K14 + 1.050g K7 + 1.050g K13 + 1.050g K24 + 0.260g K16
2432 2.000g E1 + 0.260g K16 + 2.100g K14 + 2.100g K7 + 2.100g K13 + 2.100g K2
2433 0.200g E2 + 0.210g K14 + 0.260g K16 + 0.210g K7 + 0.210g K1 + 0.210g K11
2434 1.000g E3 + 1.050g K14 + 1.050g K7 + 0.260g K16 + 1.050g K1 + 1.050g K24
2435 0.200g E4 + 0.210g K14 + 0.210g K7 + 0.2lOg K18 + 0.260g K16 + 0.210g K2
2436 1.000g E1 + 1.050g K14 + 1.050g K7 + 1.050g Kl 1+ 1.050g K24 + 0.260g K16
CA 02646867 2008-12-16
W245FQ/JC 128
2437 2.000g E2 + 0.260g K16 + 2.100g K14 + 2.100g K7 + 2.100g K11 + 2.100g K2
2438 1.000g E3 + 1.050g K14 + 0.260g K16 + 1.050g K7 + 1.050g K24 + 1.050g K2
2439 3.333g E4 + 3.500g K14 + 3.500g K9 + 0.260g K16
2440 0.250g El + 0.260g K16 + 0.263g K14 + 0.263g K9 + 0.263g K13
2441 1.250gE2+ 1.313gK14+0.260gK16+ 1.313gK9+ 1.313gK1
2442 0.250g E3 + 0.263g K14 + 0.263g K9 + 0.260g K16 + 0.263g Kl 1
2443 1.250g E4 + 1.313g K14 + 1.313g K9 + 1.313g K24 + 0.260g K16
2444 2.500g El + 0.260g K16 + 2.625g K14 + 2.625g K9 + 2.625g K2
2445 2.000g E2 + 2.100g K14 + 0.260g K16 + 2.100g K9 + 2.100g K13 + 2.100g K1
2446 2.000g E3 + 2.100g K14 + 2.100g K9 + 0.260g K16 + 2.100g K13 + 2.100g K11
2447 0.200g E4 + 0.210g K14 + 0.210g K9 + 0.210g K13 + 0.260g K16 + 0.210g K24
2448 2.000g El + 2.100g K14 + 2.100g K9 + 2.100g K13 + 2.100g K2 + 0.260g K16
2449 0.200g E2 + 0.260g K16 + 0.210g K14 + 0.210g K9 + 0.210g K1 + 0.210g K11
2450 2.000g E3 + 2.100g K14 + 0.260g K16 + 2.100g K9 + 2.100g K1 + 2.100g K24
2451 2.000g E4 + 2.100g K14 + 2.100g K9 + 0.260g K16 + 2.100g Kl + 2.100g K2
2452 2.000g E1 + 2.100g K14 + 2.100g K9 + 2.100g K11 + 0.260g K16 + 2.100g K24
2453 1.000g E2 + 1.050g K14 + 1.050g K9 + 1.050g K11 + 1.050g K2 + 0.260g K16
2454 1.000g E3 + 0.260g K16 + 1.050g K14 + 1.050g K9 + 1.050g K24 + 1.050g K2
2455 1.667g E4 + 1.750g K14 + 0.260g K16 + 1.750g K13
2456 2.500g El + 2.625g K14 + 2.625g K13 + 0.260g K16 + 2.625g K1
2457 2.500g E2 + 2.625g K14 + 2.625g K13 + 2.625g K11 + 0.260g K16
2458 2.500g E3 + 0.260g K16 + 2.625g K14 + 2.625g K13 + 2.625g K24
2459 1.250g E4 + 1.313g K14 + 0.260g K16 + 1.313g K13 + 1.313g K2
2460 1.000g El + 1.050g K14 + 1.050g K13 + 0.260g K16 + 1.050g Kl + 1.050g K11
2461 0.200g E2 + 0.210g K14 + 0.210g K13 + 0.210g K1 + 0.260g K16 + 0.210g K24
2462 1.000g E3 + 1.050g K14 + 1.050g K13 + 1.050g K1 + 1.050g K2 + 0.260g K16
2463 1.000g E4 + 0.260g K16 + 1.050g K14 + 1.050g K13 + 1.050g K11 + 1.050g
K24
2464 2.000g E1 + 2.100g K14 + 0.260g K16 + 2.100g K13 + 2.100g K11 + 2.100g K2
2465 2.000g E2 + 2.100g K14 + 2.100g K13 + 0.260g K16 + 2.100g K24 + 2.100g K2
2466 3.333g E3 + 3.500g K14 + 3.500g K1 + 0.260g K16
2467 0.250g E4 + 0.260g K16 + 0.263g K14 + 0.263g Kl + 0.263g Kl 1
2468 2.500g El + 2.625g K14 + 0.260g K16 + 2.625g K1 + 2.625g K24
CA 02646867 2008-12-16
W245FQ/JC 129
2469 2.500g E2 + 2.625g K14 + 2.625g K1 + 0.260g K16 + 2.625g K2
2470 1.000g E3 + 1.050g K14 + 1.050g K1 + 1.050g K11 + 0.260g K16 + 1.050g K24
2471 1.000g E4 + 1.050g K14 + 1.050g K1 + 1.050g K11 + 1.050g K2 + 0.260g K16
2472 2.000g El + 0.260g K16 + 2.100g K14 + 0.100g K18 + 2.100g K24 + 2.100g K2
2473 0.333g E2 + 0.350g K14 + 0.260g K16 + 0.350g K11
2474 2.500g E3 + 2.625g K14 + 2.625g Kl 1+ 0.260g K16 + 2.625g K24
2475 0.250g E4 + 0.263g K14 + 0.263g Kl 1+ 0.263g K2 + 0.260g K16
2476 2.000g E1 + 0.260g K16 + 2.l00g K14 + 2. l00g K11 + 2.100g K24 + 2.l00g
K2
2477 5.000g E1 + 5.250g K14 + 0.260g K16 + O.OlOg Dl
2478 3.333g E3 + 0.260g K16 + 3.500g K14 + 3.500g K24
2479 3.333g E4 + 3.500g K14 + 0.260g K16 + 3.500g K2
2480 2.500g El + 2.625g K14 + 2.625g K24 + 0.260g K16 + 2.625g K2
2481 0.250g E2 + 0.263g K24 + 0.250g E8 + 0.263g K12 + 0.260g K16
2482 2.500g E3 + 0.260g K16 + 2.625g K24 + 2.500g E8 + 2.625g K6
2483 2.500g E4 + 2.625g K24 + 0.462g K16 + 2.500g E8 + 2.625g K7
2484 1.250g El + 1.313g K24 + 1.250g E8 + 0.462g K16 + 1.313g K4 + 1.313g K9
2485 2.500g E2 + 2.625g K24 + 2.500g E8 + 2.625g K13 + 0.462g K16
2486 1.250g E3 + 0.462g K16 + 1.313g K24 + 1.250g E8 + 1.313g K1
2487 1.250g E4 + 1.313g K24 + 0.462g K16 + 1.250g E8 + 1.313g K11
2488 1.250g El + 1.313g K24 + 1.250g E8 + 0.462g K16 + 1.313g K14
2489 2.500g E2 + 2.625g K24 + 2.500g E8 + 1.625g K2 + 1.313g K4 + 0.462g K16
2490 0.200g E3 + 0.462g K16 + 0.210g K24 + 0.200g E8 + 0.210g K12 + 0.210g K6
2491 1.000g E4 + 1.050g K24 + 0.462g K16 + 1.000g E8 + 1.050g K12 + 1.050g K7
2492 2.000g El + 2.100g K24 + 2.000g E8 + 0.462g K16 + 2.100g K12 + 2.100g K9
2493 2.000g E2 + 2.100g K24 + 2.000g E8 + 2.100g K12 + 0.462g K16 + 2.100g K13
2494 0.200g E3 + 0.210g K24 + 0.200g E8 + 0.210g K12 + 0.210g K1 + 0.462g K16
2495 2.000g E4 + 0.462g 1(16 + 2.100g K24 + 2.000g E8 + 2.100g 1(12 + 2.100g
Kl 1
2496 0.200g E1 + 0.210g K24 + 0.462g K16 + 0.200g E8 + 0.210g K12 + 0.210g K14
2497 0.200g E2 + 0.210g K24 + 0.200g E8 + 0.462g K16 + 0.210g K12 + 0.210g K2
2498 1.000g E3 + 1.050g K24 + 1.000g E8 + 1.050g K6 + 0.462g K16 + 1.050g K7
2499 0.200g E4 + 0.210g K24 + 0.200g E8 + 0.210g K6 + 0.210g K9 + 0.462g K16
2500 1.000g El + 0.462g K16 + 1.050g K24 + 1.000g E8 + 1.050g K6 + 1.050g K13
CA 02646867 2008-12-16
W245FQ/JC 130
2501 0.200g E2 + 0.210g K24 + 0.462g K16 + 0.200g E8 + 0.210g K6 + 0.210g K1
2502 1.000g E3 + 1.050g K24 + 1.000g E8 + 0.462g K16 + 1.050g K6 + 1.050g K11
2503 0.200g E4 + 0.210g K24 + 0.200g E8 + 0.210g K6 + 0.462g K16 + 0.210g K14
2504 0.200g El + 0.210g K24 + 0.200g E8 + 0.210g K6 + 0.210g K2 + 0.462g K16
2505 1.000g E2 + 0.462g K16 + 1.050g K24 + 1.000g E8 + 1.050g K7 + 1.050g K9
2506 0.200g E3 + 0.210g K24 + 0.462g K16 + 0.200g E8 + 0.210g K7 + 0.210g K22
2507 0.200g E4 + 0.210g K24 + 0.200g E8 + 0.462g K16 + 0.210g K7 + 0.210g K1
2508 0.200g El + 0.210g K24 + 0.200g E8 + 0.210g K7 + 0.462g K16 + 0.210g K11
2509 0.200g E2 + 0.210g K24 + 0.200g E8 + 0.210g K8 + 0.210g K14 + 0.462g K16
2510 1.000g E3 + 0.462g K16 + 1.050g K24 + 1.000g E8 + 1.050g K7 + 1.050g K2
2511 2.000g E4 + 2.100g K24 + 0.462g K16 + 2.000g E8 + 2.100g K9 + 2.100g K13
2512 1.000g El + 1.050g K24 + 1.000g E8 + 0.462g K16 + 1.050g K9 + 1.050g Kl
2513 0.200g E2 + 0.210g K24 + 0.200g E8 + 0.210g K9 + 0.462g K16 + 0.210g K11
2514 2.000g E3 + 2.100g K24 + 2.000g E8 + 2.100g K9 + 2.100g K14 + 0.462g K16
2515 2.000g E4 + 0.462g K16 + 2.100g K24 + 2.000g E8 + 2.100g K9 + 2.100g K2
2516 1.000g El + 1.050g K24 + 0.462g K16 + 1.000g E8 + 1.050g K13 + 1.050g K1
2517 0.200g E2 + 0.210g K24 + 0.200g E8 + 0.462g K16 + 0.210g K13 + 0.210g K11
2518 1.000g E3 + 1.050g K24 + 1.000g E8 + 1.050g K13 + 0.462g K16 + 1.050g K14
2519 2.000g E4 + 2.100g K24 + 2.000g E8 + 2.100g K13 + 2. l00g K2 + 0.462g K16
2520 0.200g El + 0.462g K16 + 0.210g K24 + 0.200g E8 + 0.210g K1 + 0.210g K11
2521 2.000g E2 + 2.100g K24 + 0.462g K16 + 2.000g E8 + 2.100g K1 + 2.100g K14
2522 2.000g E3 + 2.100g K24 + 2.000g E8 + 0.462g K16 + 2.100g K1 + 2.100g K2
2523 0.200g E4 + 0.210g K24 + 0.200g E8 + 0.210g Kl 1+ 0.462g K16 + 0.210g K14
2524 2.000g El + 2.100g K24 + 2.000g E8 + 2.100g 1(11 + 2.100g K2 + 0.462g K16
2525 2.000g E2 + 0.462g K16 + 2.100g K24 + 2.000g E8 + 2.100g K14 + 2.100g K2
2526 1.250g E3 + 1.313g K24 + 0.462g K16 + 1.250g E6 + 1.313g K12
2527 1.250g E4 + 1.313g K24 + 1.250g E6 + 0.462g K16 + 1.313g K6
2528 0.250g El + 0.263g K24 + 0.250g E6 + 0.263g K7 + 0.462g K16
2529 1.250g E2 + 0.462g K16 + 1.313g K24 + 1.250g E6 + 1.313g K9
2530 0.250g E3 + 0.263g K24 + 0.462g K16 + 0.250g E6 + 0.263g K13
2531 2.500g E4 + 2.625g K24 + 2.500g E6 + 0.462g K16 + 2.625g K1
2532 2.500g El + 2.625g K24 + 2.500g E6 + 2.625g K11 + 0.462g K16
CA 02646867 2008-12-16
W245FQ/JC 131
2533 2.500g E2 + 0.462g K16 + 2.625g K24 + 2.500g E6 + 2.625g K14
2534 1.250g E3 + 1.313g K24 + 0.462g K16 + 1.250g E6 + 1.313g K2
2535 0.200g E4 + 0.210g K24 + 0.200g E6 + 0.462g K16 + 0.210g K12 + 0.210g K6
2536 0.200g El + 0.210g K24 + 0.200g E6 + 0.210g 1(12 + 0.462g K16 + 0.210g K7
2537 1.000g E2 + 1.050g K24 + 1.000g E6 + 1.050g K12 + 1.050g K9 + 0.462g K16
2538 2.000g E3 + 0.462g K16 + 2.100g K24 + 2.000g E6 + 2.100g K12 + 2.100g K13
2539 2.000g E4 + 2.100g K24 + 0.462g K16 + 2.000g E6 + 2.100g K12 + 2.1 OOg K
1
2540 2.000g El + 2.100g K24 + 2.000g E6 + 0.462g K16 + 2.100g K12 + 2.100g Kl
1
2541 0.200g E2 + 0.210g K24 + 0.200g E6 + 0.210g K12 + 0.462g K16 + 0.210g K14
2542 0.200g E3 + 0.210g K24 + 0.200g E6 + 0.210g K12 + 0.210g K2 + 0.462g K16
2543 2.000g E4 + 0.462g K 16 + 2. l 00g K24 + 2.000g E6 + 2. l 00g K6 + 2.100g
K21
2544 1.000g El + 1.050g K24 + 0.462g K16 + 1.000g E6 + 1.050g K6 + 1.050g K9
2545 0.200g E2 + 0.210g K24 + 0.200g E6 + 0.462g K16 + 0.210g K6 + 0.210g K13
2546 2.000g E3 + 2.100g K24 + 2.000g E6 + 2.100g K6 + 0.462g K16 + 2.100g 1(1
2547 2.000g E4 + 2.100g K24 + 2.000g E6 + 2.100g K6 + 2.100g K11 + 0.462g K16
2548 2.000g E1 + 0.462g K16 + 2.100g K24 + 2.000g E6 + 2.100g K6 + 2.100g K14
2549 0.200g E2 + 0.210g K24 + 0.462g K16 + 0.200g E6 + 0.210g K6 + 0.210g K2
2550 2.000g E3 + 2.100g K24 + 2.000g E6 + 0.462g K16 + 2.100g K7 + 2.100g K9
2551 1.000g E4 + 1.050g K24 + 1.000g E6 + 1.050g K7 + 0.462g K16 + 1.050g K13
2552 2.000g El + 2.100g K24 + 2.000g E6 + 2.100g K7 + 2.100g K1 + 0.462g K16
2553 2.000g E2 + 0.462g K16 + 2.100g K24 + 2.000g E6 + 2.100g K7 + 2.100g Kl 1
2554 0.200g E3 + 0.210g K24 + 0.462g K16 + 0.200g E6 + 0.210g K7 + 0.210g K14
2555 2.000g E4 + 2.100g K24 + 2.000g E6 + 0.462g K16 + 2.100g K7 + 2.100g K2
2556 1.000g El + 1.050g K24 + 1.000g E6 + 1.050g K9 + 0.462g K16 + 1.050g K13
2557 1.000g E2 + 1.050g K24 + 1.000g E6 + 1.050g K9 + 1.050g Kl + 0.462g K16
2558 1.000g E3 + 0.462g K16 + 1.050g K24 + 1.000g E6 + 1.050g K9 + 1.050g K11
2559 0.200g E4 + 0.210g K24 + 0.462g K16 + 0.200g E6 + 0.210g K9 + 0.210g K14
2560 1.000g El + 1.050g K24 + 1.000g E6 + 0.462g K16 + 1.050g K9 + 1.050g K2
2561 0.200g E2 + 0.210g K24 + 0.200g E6 + 0.210g K13 + 0.462g K16 + 0.210g K1
2562 0.200g E3 + 0.210g K24 + 0.200g E6 + 0.210g K22 + 0.210g K11 + 0.462g K16
2563 1.000g E4 + 0.462g K16 + 1.050g K24 + 1.000g E6 + 1.050g K13 + 1.050g K14
2564 2.000g El + 2.100g K24 + 0.462g K16 + 2.000g E6 + 2.100g K13 + 2.100g K2
CA 02646867 2008-12-16
W245FQ/JC 132
2565 1.000g E2 + 1.050g K24 + 1.000g E6 + 0.462g K16 + 1.050g Kl + 1.050g K11
2566 2.000g E3 + 2.100g K24 + 2.000g E6 + 2.100g K1 + 0.462g K16 + 2.100g K14
2567 2.000g E4 + 2.100g K24 + 2.000g E6 + 2.100g K1 + 2.100g K2 + 0.462g K16
2568 1.000g E1 + 0.462g K16 + 1.050g K24 + 1.000g E6 + 1.050g K11 + 1.050g K14
2569 0.200g E2 + 0.210g K24 + 0.462g K16 + 0.200g E6 + 0.210g K11 + 0.210g K2
2570 1.000g E3 + 1.050g K24 + 1.000g E6 + 0.462g K16 + 1.050g K14 + 1.050g K2
2571 2.500g E4 + 2.625g K24 + 2.500g E5 + 2.625g K12 + 0.462g K16
2572 0.250g E1 + 0.462g K16 + 0.263g K24 + 0.250g E5 + 0.263g K6
2573 0.250g E2 + 0.263g K24 + 0.462g K16 + 0.250g E5 + 0.263g K7
2574 1.250g E3 + 1.313g K24 + 1.250g E5 + 1.665g K16 + 1.313g K9
2575 2.500g E4 + 2.625g K24 + 2.500g E5 + 2.625g K13 + 1.665g K16
2576 2.500g E1 + 1.665g K16 + 2.625g K24 + 2.500g E5 + 2.625g K1
2577 2.500g E2 + 2.625g K24 + 1.665g K16 + 2.500g E5 + 2.625g K11
2578 1.250g E3 + 1.313g K24 + 1.250g E5 + 1.665g K16 + 1.313g K14
2579 1.250g E4 + 1.313g K24 + 1.250g E5 + 1.313g K2 + 1.665g K16
2580 1.000g El + 1.665g K16 + 1.050g K24 + 1.000g E5 + 1.050g K12 + 1.050g K6
2581 0.200g E2 + 0.210g K24 + 1.665g K16 + 0.200g E5 + 0.210g K12 + 0.210g K7
2582 1.000g E3 + 1.050g K24 + 1.000g E5 + 1.665g K16 + 1.050g K12 + 1.050g K9
2583 0.200g E4 + 0.210g K24 + 0.200g E5 + 0.210g K12 + 1.665g K16 + 0.210g K13
2584 0.200g El + 0.210g K24 + 0.200g E5 + 0.210g K12 + 0.210g K1 + 1.665g K16
2585 1.000g E2 + 1.665g K16 + 1.050g K24 + 1.000g E5 + 1.050g K12 + 1.050g K11
2586 0.200g E3 + 0.210g K24 + 1.665g K16 + 0.200g E5 + 0.210g K12 + 0.210g K14
2587 1.000g E4 + 1.050g K24 + 1.000g E5 + 1.665g K16 + 1.050g K12 + 1.050g K2
2588 0.200g El + 0.210g K24 + 0.200g E5 + 0.210g K6 + 1.665g K16 + 0.210g K7
2589 2.000g E2 + 2.100g K24 + 2.000g E5 + 2.100g K6 + 2.100g K9 + 1.665g K16
2590 0.200g E3 + 1.665g K16 + 0.210g K24 + 0.200g E5 + 0.210g K6 + 0.210g K13
2591 1.000g E4 + 1.050g K24 + 1.665g K16 + 1.000g E5 + 1.050g K6 + 1.050g KI
2592 2.000g E1 + 2.100g K24 + 2.000g E5 + 1.665g K16 + 2.100g K6 + 2.100g Kl 1
2593 0.200g E2 + 0.210g K24 + 0.200g E5 + 0.210g K6 + 1.665g K16 + 0.210g K14
2594 2.000g E3 + 2.100g K24 + 2.000g E5 + 2.100g K6 + 2.100g K2 + 1.665g K16
2595 2.000g E4 + 1.665g K16 + 2.100g K24 + 2.000g E5 + 2.100g K7 + 2.100g K9
2596 1.000g El + 1.050g K24 + 1.665g K16 + 1.000g E5 + 1.050g K7 + 1.050g K13
CA 02646867 2008-12-16
W245FQ/JC 133
2597 0.200g E2 + 0.210g K24 + 0.200g E5 + 1.665g K16 + 0.210g K7 + 0.210g K1
2598 1.000g E3 + 1.050g K24 + 1.000g E5 + 1.050g K7 + 1.665g K16 + 1.050g Kl 1
2599 1.000g E4 + 1.050g K24 + 1.000g E5 + 1.050g K7 + 1.050g K14 + 1.665g K16
2600 1.000g E1 + 1.665g K16 + 1.050g K24 + 1.000g E5 + 1.050g K7 + 1.050g K2
2601 1.000g E2 + 1.050g K24 + 1.665g K16 + 1.000g E5 + 1.050g K9 + 1.050g K13
2602 0.200g E3 + 0.210g K24 + 0.200g E5 + 1.665g K16 + 0.210g K9 + 0.210g K1
2603 0.200g E4 + 0.210g K24 + 0.200g E5 + 0.210g K9 + 1.665g K16 + 0.210g K11
2604 1.000g El + 1.050g K24 + 1.000g E5 + 1.050g K9 + 1.050g K14 + 1.665g K16
2605 0.200g E2 + 1.665g K16 + 0.210g K24 + 0.200g E5 + 0.210g K9 + 0.210g K2
2606 1.000g E3 + 1.050g K24 + 1.665g K16 + 1.000g E5 + 1.050g K13 + 1.050g K1
2607 0.200g E4 + 0.210g K24 + 0.200g E5 + 1.665g K16 + 0.210g K13 + 0.210g K11
2608 1.000g El + 1.050g K24 + 1.000g E5 + 1.050g K13 + 1.665g K16 + 1.050g K14
2609 2.000g E2 + 2.100g K24 + 2.000g E5 + 2.100g K13 + 2.100g K2 + 1.665g K16
2610 1.000g E3 + 1.665g K16 + 1.050g K24 + 1.000g E5 + 1.050g K1 + 1.050g K11
2611 2.000g E4 + 2.100g K24 + 1.665g K16 + 2.000g E5 + 2.100g K1 + 2.100g K14
2612 1.000g E1 + 1.050g K24 + 1.000g E5 + 1.665g K16 + 1.050g K1 + 1.050g K2
2613 2.000g E2 + 2.100g K24 + 2.000g E5 + 2.100g K11 + 1.665g K16 + 2.100g K14
2614 2.000g E3 + 2.100g K24 + 2.000g E5 + 2.100g K11 + 2.100g K2 + 1.665g K16
2615 2.000g E4 + 1.665g K16 + 2.100g K24 + 2.000g E5 + 2.100g K14 + 2.100g K2
2616 1.250g E1 + 1.313g K24 + 1.665g K16 + 1.250g E7 + 1.313g K12
2617 0.250g E2 + 0.263g K24 + 0.250g E7 + 1.665g K16 + 0.263g K6
2618 0.250g E3 + 0.263g K24 + 0.250g E7 + 0.263g K7 + 1.665g K16
2619 1.250g E4 + 1.665g K16 + 1.313g K24 + 1.250g E7 + 1.313g K9
2620 2.500g El + 2.625g K24 + 1.665g K16 + 2.500g E7 + 2.625g K13
2621 2.500g E2 + 2.625g K24 + 2.500g E7 + 1.665g K16 + 2.625g 1(1
2622 2.500g E3 + 2.625g K24 + 2.500g E7 + 2.625g K11 + 1.665g K16
2623 0.250g E4 + 1.665g K16 + 0.263g K24 + 0.250g E7 + 0.263g K14
2624 2.500g El + 2.625g K24 + 1.665g K16 + 2.500g E7 + 2.625g K2
2625 2.000g E2 + 2.100g K24 + 2.000g E7 + 1.665g K16 + 2.100g K12 + 2.100g K6
2626 1.000g E3 + 1.050g K24 + 1.000g E7 + 1.050g K12 + 1.665g K16 + 1.050g K7
2627 2.000g E4 + 2.100g K24 + 2.000g E7 + 2.100g K12 + 2.100g K9 + 1.665g K16
2628 1.000g E1 + 1.665g K16 + 1.050g K24 + 1.000g E7 + 1.050g K12 + 1.050g
K1.3
CA 02646867 2008-12-16
W245FQ/JC 134
2629 0.200g E2 + 0.210g K24 + 1.665g K16 + 0.200g E7 + 0.210g K12 + 0.210g K1
2630 1.000g E3 + 1.050g K24 + 1.000g E7 + 1.665g K16 + 1.050g K12 + 1.050g K11
2631 0.200g E4 + 0.210g K24 + 0.200g E7 + 0.210g K12 + 1.665g K16 + 0.210g K14
2632 0.200g E1 + 0.210g K24 + 0.200g E7 + 0.210g K12 + 0.210g K2 + 1.665g K16
2633 0.200g E2 + 1.665g K16 + 0.210g K24 + 0.200g E7 + 0.210g K6 + 0.210g K8
2634 1.000g E3 + 1.050g K24 + 1.665g K16 + 1.000g E7 + 1.050g K6 + 1.050g K9
2635 1.000g E4 + 1.050g K24 + 1.000g E7 + 1.665g K16 + 1.050g K6 + 1.050g K13
2636 0.200g E1 + 0.210g K24 + 0.200g E7 + 0.210g K6 + 1.665g K16 + 0.210g K1
2637 0.200g E2 + 0.210g K24 + 0.200g E7 + 0.210g K6 + 0.210g K11 + 1.665g K16
2638 1.000g E3 + 1.665g K16 + 1.050g K24 + 1.000g E7 + 1.050g K6 + 1.050g K14
2639 1.000g E4 + 1.050g K24 + 1.665g K16 + 1.000g E7 + 1.050g K6 + 1.050g K2
2640 2.000g El + 2.100g K24 + 2.000g E7 + 1.665g K16 + 2.100g K7 + 2.100g K9
2641 1.000g E2 + 1.050g K24 + 1.000g E7 + l.050g K7 + 1.665g K16 + 1.050g K13
2642 2.000g E3 + 2.100g K24 + 2.000g E7 + 2.100g K21 + 2.100g Kl + 1.665g K16
2643 1.000g E4 + 1.665g K16 + 1.050g K24 + 1.000g E7 + 1.050g K7 + 1.050g K11
2644 2.000g E1 + 2.100g K24 + 1.665g K16 + 2.000g E7 + 2.100g K7 + 2.100g K14
2645 2.000g E2 + 2.100g K24 + 2.000g E7 + 1.665g K16 + 2.100g K7 + 2.100g K2
2646 0.200g E3 + 0.210g K24 + 0.200g E7 + 0.210g K9 + 1.665g K16 + 0.210g K13
2647 0.200g E4 + 0.210g K24 + 0.200g E7 + 0.210g K9 + 0.210g K1 + 1.665g K16
2648 1.000g El + 1.665g K16 + 1.050g K24 + 1.000g E7 + 1.050g K9 + 1.050g K11
2649 0.200g E2 + 0.210g K24 + 1.665g K16 + 0.200g E7 + 0.210g K9 + 0.210g K14
2650 1.000g E3 + 1.050g K24 + 1.000g E7 + 1.665g K16 + 1.050g K9 + 1.050g K2
2651 0.200g E4 + 0.210g K24 + 0.200g E7 + 0.210g K13 + 1.665g K16 + 0.210g K1
2652 2.000g El + 2.100g K24 + 2.000g E7 + 2.100g K13 + 2.100g K11 + 1.665g K16
2653 1.000g E2 + 1.665g K16 + 1.050g K24 + 1.000g E7 + 1.050g K13 + 1.050g K14
2654 0.200g E3 + 0.210g K24 + 1.665g K16 + 0.200g E7 + 0.210g K13 + 0.210g K2
2655 1.000g E4 + 1.050g K24 + 1.000g E7 + 1.665g K16 + 1.050g K1 + 1.050g K11
2656 2.000g El + 2.100g K24 + 2.000g E7 + 2.100g K1 + 1.665g K16 + 2.100g K14
2657 2.000g E2 + 2.100g K24 + 2.000g E7 + 2.100g Kl + 2.100g K2 + 1.665g K16
2658 2.000g E3 + 1.665g K16 + 2.100g K24 + 2.000g E7 + 2.100g K11 + 2.100g K14
2659 0.200g E4 + 0.210g K24 + 1.665g K16 + 0.200g E7 + 0.210g K11 + 0.210g K2
2660 0.200g El + 0.210g K24 + 0.200g E7 + 1.665g K16 + 0.210g K14 + 0.210g K2
CA 02646867 2008-12-16
W245FQ/JC 135
2661 1.667g E2 + 1.750g K24 + 1.750g K12 + 1.665g K16
2662 0.250g E3 + 1.665g K16 + 0.263g K24 + 0.263g K12 + 0.263g K6
2663 2.500g E4 + 2.625g K24 + 1.665g K16 + 2.625g K12 + 2.625g K7
2664 1.250g E1 + 1.313g K24 + 1.313g K12 + 1.888g K16 + 1.313g K9
2665 0.250g E2 + 0.263g K24 + 0.263g K12 + 0.263g K13 + 1.888g K16
2666 2.500g E3 + 1.888g K16 + 2.625g K24 + 2.625g K12 + 2.625g K1
2667 2.500g E4 + 2.625g K24 + 1.888g K16 + 2.625g K12 + 2.625g K11
2668 2.500g El + 2.625g K24 + 2.625g K12 + 1.888g K16 + 2.625g K14
2669 0.250g E2 + 0.263g K24 + 0.263g K12 + 0.263g K2 + 1.888g K16
2670 2.000g E3 + 1.888g K16 + 2. l00g K24 + 2. l00g K12 + 2.100g K6 + 2.100g
K7
2671 2.000g E4 + 2.100g K24 + 1.888g K16 + 2. l00g K12 + 2.100g K6 + 2.100g K9
2672 1.000g E1 + 1.050g K24 + 1.050g K12 + 1.888g K16 + 1.050g K6 + 1.050g K13
2673 1.000g E2 + 1.050g K24 + 1.050g K12 + 1.050g K6 + 1.888g K16 + 1.050g Kl
2674 2.000g E3 + 2.100g K24 + 2.100g K12 + 2.100g K6 + 2.100g K11 + 1.888g K16
2675 1.000g E4 + 1.888g K16 + 1.050g K24 + 1.050g K12 + 1.050g K6 + 1.050g K14
2676 0.200g E1 + 0.210g K24 + 1.888g K16 + 0.210g K12 + 0.210g K6 + 0.210g K2
2677 1.000g E2 + 1.050g K24 + 1.050g K12 + 1.888g K16 + 1.050g K7 + 1.050g K9
2678 2.000g E3 + 2.100g K24 + 2.100g K12 + 2.100g K7 + 1.888g K16 + 2.100g K13
2679 2.000g E4 + 2.100g K24 + 2.100g K12 + 2.100g K7 + 2.100g K1 + 1.888g K16
2680 0.200g E1 + 1.888g K16 + 0.210g K24 + 0.210g K12 + 0.210g K7 + 0.210g K11
2681 0.200g E2 + 0.210g K24 + 1.888g K16 + 0.210g K12 + 0.210g K7 + 0.210g K14
2682 2.000g E3 + 2.100g K24 + 2.100g K12 + 1.888g K16 + 2.100g K7 + 2.100g K2
2683 0.200g E4 + 0.210g K24 + 0.210g K12 + 0.210g K9 + 1.888g K16 + 0.210g K13
2684 1.000g E1 + 1.050g K24 + 1.050g K12 + 1.050g K9 + 1.050g K1 + 1.888g K16
2685 0.200g E2 + 1.888g K16 + 0.210g K24 + 0.210g K12 + 0.210g K9 + 0.210g K11
2686 1.000g E3 + 1.050g K24 + 1.888g K16 + 1.050g K12 + 1.050g K9 + 1.050g K14
2687 1.000g E4 + 1.050g K24 + 1.050g K12 + 1.888g K16 + 1.050g K9 + 1.050g K2
2688 1.000g El + 1.050g K24 + 1.050g K12 + 1.050g K13 + 1.888g K16 + 1.050g K1
2689 2.000g E2 + 2.100g K24 + 2.100g K12 + 2.100g K13 + 2.100g K11 + 1.888g
K16
2690 0.200g E3 + 1.888g K16 + 0.210g K24 + 0.210g K12 + 0.210g K13 + 0.210g
K14
2691 1.000g E4 + 1.050g K24 + 1.888g K16 + 1.050g K12 + 1.050g K13 + 1.050g K2
2692 2.000g E1 + 2.100g K24 + 2.100g K12 + 1.888g K16 + 2.100g K1 + 2.100g Kl
1
CA 02646867 2008-12-16
W245FQ/JC 136
2693 0.200gE2+0.210gK24+0.210gK12+0.210gK1 + 1.888g K16 + 0.210g K14
2694 0.200g E3 + 0.210g K24 + 0.210g K12 + 0.210g Kl + 0.210g K2 + 1.888g K16
2695 1.000g E4 + 1.888g K16 + 1.050g K24 + 1.050g K12 + 1.050g K11 + 1.050g
K14
2696 1.000g El + 1.050g K24 + 1.888g K16 + 1.050g K12 + 1.050g Kl 1+ 1.050g K2
2697 2.000g E2 + 2.100g K24 + 2.l00g K12 + 1.888g K16 + 2.100g K14 + 2.l00g K2
2698 1.667g E3 + 1.750g K24 + 1.750g K6 + 1.888g K16
2699 0.250g E4 + 1.888g K16 + 0.263g K24 + 0.263g K6 + 0.263g K7
2700 2.500g El + 2.625g K24 + 1.888g K16 + 2.625g K6 + 2.625g K9
2701 1.250g E2 + 1.313g K24 + 1.313g K6 + 1.888g K16 + 1.313g K13
2702 1.250g E3 + 1.313g K24 + 1.313g K6 + 1.313g K1 + 1.888g K16
2703 1.250g E4 + 1.888g K16 + 1.313g K24 + 1.313g K6 + 1.313g K11
2704 1.250g E1 + 1.313g K24 + 1.888g K16 + 1.313g K6 + 1.313g K14
2705 1.250g E2 + 1.313g K24 + 1.313g K6 + 1.888g K16 + 1.313g K2
2706 1.000g E3 + 1.050g K24 + 1.050g K6 + 1.050g K7 + 1.888g K16 + 1.050g K9
2707 1.000g E4 + 1.050g K24 + 1.050g K6 + 1.050g K7 + 1.050g K13 + 1.888g K16
2708 2.000g E1 + 1.888g K16 + 2.100g K24 + 2.100g K6 + 2.100g K7 + 2.100g K1
2709 2.000g E2 + 2.100g K24 + 1.888g K16 + 2.100g K6 + 2.100g K7 + 2.100g K11
2710 1.000g E3 + 1.050g K24 + 1.050g K6 + 1.888g K16 + 1.050g K7 + 1.050g K14
2711 1.000g E4 + 1.050g K24 + 1.050g K6 + 1.050g K7 + 1.888g K16 + 1.050g K2
2712 1.000g E1 + 1.050g K24 + 1.050g K6 + 1.050g K9 + 1.050g K13 + 1.888g K16
2713 1.000g E2 + 1.888g K16 + 1.050g K24 + 1.050g K6 + 1.050g K9 + 1.050g Ki
2714 0.200g E3 + 0.210g K24 + 1.888g K16 + 0.210g K6 + 0.210g K9 + 0.210g K11
2715 0.200g E4 + 0.210g K24 + 0.210g K6 + 1.888g K16 + 0.210g K9 + 0.210g K14
2716 0.200g E1 + 0.210g K24 + 0.210g K6 + 0.210g K9 + 1.888g K16 + 0.210g K2
2717 2.000g E2 + 2.100g K24 + 2.100g K6 + 2.100g K13 + 2.100g K1 + 1.888g K16
2718 1.000g E3 + 1.888g K16 + 1.050g K24 + 1.050g K6 + 1.050g K13 + 1.050g Kl
1
2719 0.200g E4 + 0.210g K24 + 1.888g K16 + 0.210g K6 + 0.210g K13 + 0.210g K14
2720 0.200g E1 + 0.210g K24 + 0.210g K6 + 1.888g K16 + 0.210g K13 + 0.210g K2
2721 0.200g E2 + 0.210g K24 + 0.210g K6 + 0.210g K1 + 1.888g K16 + 0.210g K11
2722 0.200g E3 + 0.210g K24 + 0.210g K6 + 0.210g K1 + 0.210g K14 + 1.888g K16
2723 2.000g E4 + 1.888g K16 + 2.100g K24 + 2.100g K6 + 2.100g K1 + 2.100g K2
2724 1.000g E1 + 1.050g K24 + 1.888g K16 + 1.050g K6 + 1.050g Kl 1+ 1.050g K14
CA 02646867 2008-12-16
W245FQ/JC 137
2725 1.000g E2 + 1.050g K24 + 1.050g K6 + 1.888g K16 + 1.050g K11 + 1.050g K2
2726 2.000g E3 + 2.100g K24 + 2.100g K6 + 2.100g K14 + 1.888g K16 + 2.100g K2
2727 1.667g E4 + 1.750g K24 + 1.750g K8 + 1.888g K16
2728 1.250gE1+1.888gK16+1.313gK24+1.313gK7+1.313gK9
2729 0.250g E2 + 0.263g K24 + 1.888g K16 + 0.263g K21 + 0.263g K13
2730 1.250g E3 + 1.313g K24 + 1.313g K7 + 1.888g K16 + 1.313g K1
2731 2.500g E4 + 2.625g K24 + 2.625g K7 + 2.625g K11 + 1.888g K16
2732 0.250g El + 1.888g K16 + 0.263g K24 + 0.263g K7 + 0.263g K14
2733 2.500g E2 + 2.625g K24 + 1.888g K16 + 2.625g K7 + 2.625g K2
2734 2.000g E3 + 2.100g K24 + 2.100g K7 + 1.888g K16 + 2.100g K9 + 2.100g K13
2735 0.200g E4 + 0.210g K24 + 0.210g K7 + 0.210g K9 + 1.888g K16 + 0.210g K1
2736 2.000g E1 + 2.100g K24 + 2.100g K7 + 2.100g K9 + 2.100g K11 + 1.888g K16
2737 1.000g E2 + 1.888g K16 + 1.050g K24 + 1.050g K7 + 1.050g K9 + 1.050g K14
2738 0.200g E3 + 0.210g K24 + 1.888g K16 + 0.210g K7 + 0.210g K9 + 0.210g K2
2739 1.000g E4 + 1.050g K24 + 1.050g K7 + 1.888g K16 + 1.050g K13 + 1.050g Kl
2740 1.000g E1 + 1.050g K24 + 1.050g K7 + 1.050g K13 + 1.888g K16 + 1.050g K11
2741 0.200g E2 + 0.210g K24 + 0.210g K7 + 0.210g K13 + 0.210g K14 + 1.888g K16
2742 0.200g E3 + 1.888g K16 + 0.210g K24 + 0.210g K7 + 0.210g K13 + 0.210g K2
2743 2.000g E4 + 2.l00g K24 + 1.888g K16 + 2.100g K7 + 2.100g K1 + 2.l00g Kl 1
2744 1.000g E1 + 1.050g K24 + 1.050g K7 + 1.888g K16 + 1.050g K1 + 1.050g K14
2745 1.000g E2 + 1.050g K24 + 1.050g K7 + 1.050g K1 + 1.888g K16 + 1.050g K2
2746 2.000g E3 + 2.100g K24 + 2.100g K7 + 2.100g K11 + 2.100g K14 + 1.888g K16
2747 1.000g E4 + 1.888g K16 + 1.050g K24 + 1.050g K7 + 1.050g K11 + 1.050g K2
2748 2.000g E1 + 2.100g K24 + 1.888g K16 + 2.100g K7 + 2.100g K14 + 2.100g K2
2749 1.667g E2 + 1.750g K24 + 1.750g K9 + 1.888g K16
2750 0.250g E3 + 1.888g K16 + 0.263g K24 + 0.263g K9 + 0.263g K13
2751 1.250g E4 + 1.313g K24 + 1.888g K16 + 1.313g K9 + 1.313g K1
2752 1.250g E1 + 1.313g K24 + 1.313g K9 + 1.888g K16 + 1.313g K11
2753 2.500g E2 + 2.625g K24 + 2.625g K9 + 2.625g K14 + 1.888g K16
2754 0.250g E3 + 1.888g K16 + 0.263g K24 + 0.263g K9 + 0.263g K2
2755 0.200g E4 + 0.210g K24 + 0.09lg K16 + 0.210g K9 + 0.210g K13 + 0.2lOg K1
2756 0.200g El + 0.210g K24 + 0.210g K9 + 0.091g K16 + 0.210g K13 + 0.210g K11
CA 02646867 2008-12-16
W245FQ/JC 138
2757 0.200g E2 + 0.210g K24 + 0.210g K9 + 0.210g K13 + 0.091 g K16 + 0.210g K
14
2758 2.000g E3 + 2.100g K24 + 2. l 00g K9 + 2. l 00g K 13 + 2.1 OOg K2 + 0.091
g K 16
2759 0.200gE4+0.091gK16+0.210gK24+0.210gK9+0.210gK1+0.210gK11
2760 0.200gE1 +0.210gK24+0.091gK16+0.210gK9+0.210gK1 +0.210gK14
2761 0.200gE2+0.210gK24+0.210gK9+0.091gK16+0.210gK1 +0.210gK2
2762 0.200g E3 + 0.210g K24 + 0.210g K9 + 0.210g K11 + 0.091g K16 + 0.210g K14
2763 2.000g E4 + 2.100g K24 + 2.l00g K9 + 2. l00g K11 + 2.l00g K2 + 0.091g K16
2764 1.000g E1 + 0.091g K16 + 1.050g K24 + 1.050g K9 + 1.050g K14 + 1.050g K2
2765 3.333g E2 + 3.500g K24 + 0.091g K16 + 3.500g K13
2766 0.250g E3 + 0.263g K24 + 0.263g K13 + 0.091g K16 + 0.263g K1
2767 0.250g E4 + 0.263g K24 + 0.263g K13 + 0.263g Kl 1+ 0.091g K16
2768 0.250g El + 0.091g K16 + 0.263g K24 + 0.263g K13 + 0.263g K14
2769 0.250g E2 + 0.263g K24 + 0.091g K16 + 0.263g K13 + 0.263g K2
2770 2.000g E3 + 2.100g K24 + 2.100g K13 + 0.091g K16 + 2.100g K1 + 2.100g K11
2771 0.200g E4 + 0.210g K24 + 0.210g K13 + 0.210g K1 + 0.091g K16 + 0.210g K14
2772 1.000g El + 1.050g K24 + 1.050g K13 + 1.050g K1 + l.050g K2 + 0.091g K16
2773 0.200g E2 + 0.091g K16 + 0.210g K24 + 0.210g K13 + 0.210g K11 + 0.210g
K14
2774 0.200g E3 + 0.210g K24 + 0.091g K16 + 0.210g K13 + 0.210g K11 + 0.210g K2
2775 2.000g E4 + 2.100g K24 + 2.100g K13 + 0.091g K16 + 2.100g K14 + 2.100g K2
2776 0.333g El + 0.350g K24 + 0.350g KI + 0.091g K16
2777 1.250g E2 + 0.091g K16 + 1.313g K24 + 1.313g K1 + 1.313g K11
2778 2.500g E3 + 2.625g K24 + 0.091g K16 + 2.625g Kl + 2.625g K14
2779 1.250g E4 + 1.313g K24 + 1.313g K1 + 0.091g K16 + 1.313g K2
2780 0.200gE1 +0.210gK24+0.210gK1 +0.210gK11 +0.091gK16+0.210gK14
2781 1.000g E2 + 1.050g K24 + 1.050g K1 + 1.050g K11 + 1.050g K2 + 0.091g K16
2782 0.200g E3 + 0.091 g K16 + 0.210g K24 + 0.210g Kl + 0.210g K14 + 0.210g K2
2783 1.667g E4 + 1.750g K24 + 0.091g K16 + 1.750g K11
2784 2.500g El + 2.625g K24 + 2.625g K11 + 0.091g K16 + 2.625g K14
2785 0.250g E2 + 0.263g K24 + 0.263g K11 + 0.263g K2 + 0.091g K16
2786 0.200g E3 + 0.091g K16 + 0.210g K24 + 0.210g K11 + 0.210g K14 + 0.210g K2
2787 0.3339 E4 + 0.350g K24 + 0.091g K16 + 0.350g K14
2788 0.250g El + 0.263g K24 + 0.263g K14 + 0.091g K16 + 0.263g K2
CA 02646867 2008-12-16
W245FQ/JC 139
2789 5.000g E1 + 5.250g K24 + 0.091g K16 + 0.210g K23
2790 3.333g E3 + 0.091g K16 + 3.500g K24 + 3.500g K2
2791 2.500g E4 + 2.625g K2 + 0.091g K16 + 2.500g E8 + 2.625g K12
2792 0.250g El + 0.263g K2 + 0.250g E8 + 0.091g K16 + 0.263g K6
2793 0.250g E2 + 0.263g K2 + 0.250g E8 + 0.263g K8 + 0.091g K16
2794 0.250g E3 + 0.091g K16 + 0.263g K2 + 0.250g E8 + 0.263g K9
2795 1.250g E4 + 1.313g K2 + 0.091g K16 + 1.250g E8 + 1.313g K13
2796 2.500g El + 2.625g K2 + 2.500g E8 + 0.091g K16 + 2.625g K1
2797 0.250g E2 + 0.263g K2 + 0.250g E8 + 0.263g K11 + 0.091g K16
2798 1.250g E3 + 0.091g K16 + 1.313g K2 + 1.250g E8 + 1.313g K14
2799 0.250g E4 + 0.263g K2 + 0.091g K16 + 0.250g E8 + 0.263g K24
2800 0.200g El + 0.210g K2 + 0.200g E8 + 0.091g K16 + 0.210g K12 + 0.210g K6
2801 2.000g E2 + 2.100g K2 + 2.000g E8 + 2.100g K12 + 0.091g K16 + 2.100g K21
2802 1.000g E3 + 1.050g K2 + 1.000g E8 + 1.050g K12 + 1.050g K9 + 0.091g K16
2803 1.000g E4 + 0.091g K16 + 1.050g K2 + 1.000g E8 + 1.050g K12 + 1.050g K13
2804 0.200g El + 0.210g K2 + 0.091g K16 + 0.200g E8 + 0.210g K12 + 0.210g K1
2805 0.200gE2+0.210gK2+0.200gE8+0.091gK16+0.210gK12+0.210gK11
2806 1.000g E3 + 1.050g K2 + 1.000g E8 + 1.050g K12 + 0.091g K16 + 1.050g K14
2807 1.000g E4 + 1.050g K2 + 1.000g E8 + 1.050g K12 + 1.050g K24 + 0.091g K16
2808 1.000g El + 0.091g K16 + 1.050g K2 + 1.000g E8 + 1.050g K6 + 1.050g K7
2809 0.200g E2 + 0.210g K2 + 0.091g K16 + 0.200g E8 + 0.210g K6 + 0.210g K9
2810 0.200gE3+0.210gK2+0.200gE8+0.091gK16+0.210gK6+0.210gK13
2811 0.200gE4+0.210gK2+0.200gE8+0.210gK6+0.091gK16+0.210gK1
2812 0.200gE1 +0.210gK2+0.200gE8+0.210gK6+0.210gK11 +0.091gK16
2813 2.000g E2 + 0.091g K16 + 2.100g K2 + 2.000g E8 + 2.100g K6 + 2.100g K14
2814 2.000g E3 + 2.100g K2 + 0.091 g K16 + 2.000g E8 + 2.100g K6 + 2.100g K24
2815 2.000g E4 + 2.100g K2 + 2.000g E8 + 0.091 g K 16 + 2. l 00g K7 + 2. l 00g
K9
2816 1.000g E1 + 1.050g K2 + 1.000g E8 + 1.050g K7 + 0.091g K16 + 1.050g K13
2817 2.000g E2 + 2.100g K2 + 2.000g E8 + 2.100g K7 + 2.100g K1 + 0.091g K16
2818 1.000g E3 + 0.091g K16 + 1.050g K2 + 1.000g E8 + 1.050g K7 + 1.050g Kl 1
2819 1.000g E4 + 1.050g K2 + 0.09lg K16 + 1.000g E8 + 1.050g K7 + 1.050g K14
2820 1.000g E1 + 1.050g K2 + 1.000g E8 + 0.091g K16 + 1.050g K7 + 1.050g K24
CA 02646867 2008-12-16
W245FQ/JC 140
2821 2.000g E2 + 2.100g K2 + 2.000g E8 + 2.100g K9 + 0.091g K16 + 2.100g K13
2822 0.200g E3 + 0.210g K2 + 0.200g E8 + 0.210g K9 + 0.210g Kl + 0.091g K16
2823 2.000g E4 + 0.091g K16 + 2.100g K2 + 2.000g E8 + 2.100g K9 + 2.100g K11
2824 2.000g El + 2.100g K2 + 0.091g K16 + 2.000g E8 + 2.100g K9 + 2.100g K14
2825 0.200g E2 + 0.210g K2 + 0.200g E8 + 0.091g K16 + 0.210g K9 + 0.210g K24
2826 2.000g E3 + 2.100g K2 + 2.000g E8 + 2.100g K13 + 0.091g K16 + 2.100g K1
2827 2.000g E4 + 2.100g K2 + 2.000g E8 + 2.100g K13 + 2.100g K11 + 0.091g K16
2828 1.000g E1 + 0.091g K16 + 1.050g K2 + 1.000g E8 + 1.050g K13 + 1.050g K14
2829 0.200g E2 + 0.210g K2 + 0.091g K16 + 0.200g E8 + 0.210g K13 + 0.210g K24
2830 2.000g E3 + 2.100g K2 + 2.000g E8 + 0.091g K16 + 2.100g K1 + 2.100g K11
2831 1.000g E4 + 1.050g K2 + 1.000g E8 + 1.050g Kl + 0.091g K16 + 1.050g K14
2832 0.200g El + 0.210g K2 + 0.200g E8 + 0.210g K1 + 0.210g K24 + 0.091g K16
2833 1.000g E2 + 0.091g K16 + 1.050g K2 + 1.000g E8 + 1.050g K11 + 1.050g K14
2834 1.000g E3 + 1.050g K2 + 0.091g K16 + 1.000g E8 + 1.050g K11 + 1.050g K24
2835 1.000g E4 + 1.050g K2 + 1.000g E8 + 0.091g K16 + 1.050g K14 + 1.050g K24
2836 1.250g E1 + 1.313g K2 + 1.250g E6 + 1.313g K12 + 0.091g K16
2837 0.250g E2 + 0.091g K16 + 0.263g K2 + 0.250g E6 + 0.263g K6
2838 0.250g E3 + 0.263g K2 + 0.091g K16 + 0.250g E6 + 0.263g K7
2839 2.500g E4 + 2.625g K2 + 2.500g E6 + 0.091g K16 + 2.625g K9
2840 1.250gE1+1.313gK2+1.250gE6+1.313gK13+0.091gK16
2841 0.250g E2 + 0.091g K16 + 0.263g K2 + 0.250g E6 + 0.263g K1
2842 2.500g E3 + 2.625g K2 + 0.294g K16 + 2.500g E6 + 2.625g K11
2843 2.500g E4 + 2.625g K2 + 2.500g E6 + 0.294g K16 + 2.625g K14
2844 1.250g E8 + 0.613g K12 + 0.250g K25 + 0.113g K24 + 0.294g K16
2845 1.000g E2 + 0.294g K16 + 1.050g K2 + 1.000g E6 + 1.050g K12 + 1.050g K6
2846 0.200g E3 + 0.210g K2 + 0.294g K16 + 0.200g E6 + 0.210g K12 + 0.210g K7
2847 1.000g E4 + 1.050g K2 + 1.000g E6 + 0.294g K16 + 1.050g K12 + 1.050g K9
2848 0.200g E1 + 0.210g K2 + 0.200g E6 + 0.210g K12 + 0.294g K16 + 0.210g K22
2849 0.200g E2 + 0.210g K2 + 0.200g E6 + 0.210g K12 + 0.210g K1 + 0.294g K16
2850 1.000g E3 + 0.294g K16 + 1.050g K2 + 1.000g E6 + 1.050g K12 + 1.050g K11
2851 1.000g E4 + 1.050g K2 + 0.294g K16 + 1.000g E6 + 1.050g K12 + 1.050g K14
2852 1.000g E1 + 1.050g K2 + 1.000g E6 + 0.294g K16 + 1.050g K12 + 1.050g K24
CA 02646867 2008-12-16
W245FQ/JC 141
2853 0.200g E2 + 0.210g K2 + 0.200g E6 + 0.210g K6 + 0.294g K16 + 0.210g K7
2854 2.000g E3 + 2.100g K2 + 2.000g E6 + 2.100g K6 + 2.100g K9 + 0.294g K16
2855 1 .000g E4 + 0.294g K16 + 1.050g K2 + 1.000g E6 + 1.050g K6 + 1.050g K13
2856 0.200g E1 + 0.21Og K2 + 0.294g K16 + 0.200g E6 + 0.210g K6 + 0.210g K1
2857 0.200g E2 + 0.210g K2 + 0.200g E6 + 0.294g K16 + 0.210g K6 + 0.210g K11
2858 2.000g E3 + 2.100g K2 + 2.000g E6 + 2.100g K6 + 0.294g K16 + 2.100g K14
2859 1.000g E4 + 1.050g K2 + 1.000g E6 + 1.050g K6 + 1.050g K24 + 0.294g K16
2860 1.000g El + 0.294g K16 + 1.050g K2 + 1.000g E6 + 1.050g K7 + 1.050g K9
2861 1.000g E2 + 1.050g K2 + 0.294g K16 + 1.000g E6 + 1.050g K7 + 1.050g K13
2862 0.200g E3 + 0.210g K2 + 0.200g E6 + 0.294g K16 + 0.210g K7 + 0.210g K1
2863 2.000g E4 + 2.100g K2 + 2.000g E6 + 2.100g K7 + 0.294g K16 + 2.100g K11
2864 0.200g E1 + 0.210g K2 + 0.200g E6 + 0.210g K7 + 0.210g K14 + 0.294g K16
2865 2.000g E2 + 0.294g K16 + 2.100g K2 + 2.000g E6 + 2.100g K7 + 2.100g K24
2866 1.000g E3 + 1.050g K2 + 0.294g K16 + 1.000g E6 + 1.050g K9 + 1.050g K13
2867 2.000g E4 + 2.100g K2 + 2.000g E6 + 0.294g K16 + 2.100g K9 + 2.100g K1
2868 1.000g E1 + 1.050g K2 + 1.000g E6 + 1.050g K9 + 0.294g K16 + 1.050g K11
2869 2.000g E2 + 2.l00g K2 + 2.000g E6 + 2.l00g K9 + 2.l00g K14 + 0.294g K16
2870 2.000g E3 + 0.294g K16 + 2. l00g K2 + 2.000g E6 + 2. l00g K9 + 2. l00g
K24
2871 0.200g E4 + 0.210g K2 + 0.294g K16 + 0.200g E6 + 0.210g K13 + 0.210g K1
2872 2.000g E1 + 2.100g K2 + 2.000g E6 + 0.294g K16 + 2.100g K13 + 2.100g Kl 1
2873 0.200g E2 + 0.210g K2 + 0.200g E6 + 0.210g K13 + 0.294g K16 + 0.210g K14
2874 0.200g E3 + 0.21Og K2 + 0.200g E6 + 0.210g K13 + 0.210g K24 + 0.294g K16
2875 1.000g E4 + 0.294g K16 + 1.050g K2 + 1.000g E6 + 1.050g K1 + 1.050g Kl 1
2876 0.200g El + 0.210g K2 + 0.294g K16 + 0.200g E6 + 0.210g K1 + 0.210g K14
2877 0.200g E2 + 0.210g K2 + 0.200g E6 + 0.294g K16 + 0.210g K1 + 0.210g K24
2878 2.000g E3 + 2.100g K2 + 2.000g E6 + 2.100g K11 + 0.294g K16 + 2.100g K14
2879 1.000g E4 + 1.050g K2 + 1.000g E6 + 1.050g K11 + 1.050g K24 + 0.294g K16
2880 1.000g El + 0.294g K16 + 1.050g K2 + 1.000g E6 + 1.050g K14 + 1.050g K24
2881 1.250g E2 + 1.313g K2 + 0.294g K16 + 1.250g E5 + 1.313g K12
2882 0.250g E3 + 0.263g K2 + 0.250g E5 + 0.294g K16 + 0.263g K6
2883 2.500g E4 + 2.625g K2 + 2.500g E5 + 2.625g K7 + 0.294g K16
2884 0.250g El + 0.294g K16 + 0.263g K2 + 0.250g E5 + 0.263g K9
CA 02646867 2008-12-16
W245FQ/JC 142
2885 1.250g E2 + 1.313g K2 + 0.294g K16 + 1.250g E5 + 1.313g K13
2886 2.500g E3 + 2.625g K2 + 2.500g E5 + 0.294g K16 + 2.625g K1
2887 1.250g E4 + 1.313g K2 + 1.250g E5 + 1.313g K11 + 0.294g K16
2888 1.250g El + 0.294g K16 + 1.313g K2 + 1.250g E5 + 1.313g K14
2889 1.250g E2 + 1.313g K2 + 0.294g K16 + 1.250g E5 + 1.313g K24
2890 1.000g E3 + 1.050g K2 + 1.000g E5 + 0.294g K16 + 1.050g K12 + 1.050g K6
2891 0.200g E4 + 0.210g K2 + 0.200g E5 + 0.210g K12 + 0.294g K16 + 0.210g K7
2892 0.200g E1 + 0.210g K2 + 0.200g E5 + 0.210g K12 + 0.210g K9 + 0.294g K16
2893 2.000g E2 + 0.294g K16 + 2.100g K2 + 2.000g E5 + 2.100g K12 + 2.100g K13
2894 2.000g E3 + 2.100g K2 + 0.294g K16 + 2.000g E5 + 2.100g K12 + 2.100g K1
2895 1.000g E4 + 1.050g K2 + 1.000g E5 + 0.294g K16 + 1.050g K12 + 1.050g K11
2896 1.000g El + 1.050g K2 + 1.000g E5 + 1.050g K12 + 0.294g K16 + 1.050g K14
2897 0.200g E2 + 0.210g K2 + 0.200g E5 + 0.210g K12 + 0.210g K24 + 0.294g K16
2898 1.000g E3 + 0.294g K16 + 1.050g K2 + 1.000g E5 + 1.050g K6 + 1.050g K7
2899 0.200g E4 + 0.210g K2 + 0.294g K16 + 0.200g E5 + 0.210g K6 + 0.210g K9
2900 1.000g El + 1.050g K2 + 1.000g E5 + 0.294g K16 + 1.050g K6 + 1.050g K22
2901 0.200g E2 + 0.2lOg K2 + 0.200g E5 + 0.210g K6 + 0.294g K16 + 0.210g K1
2902 1.000g E3 + 1.050g K2 + 1.000g E5 + 1.050g K6 + 1.050g K11 + 0.294g K16
2903 2.000g E4 + 0.294g K16 + 2.100g K2 + 2.000g E5 + 2.100g K6 + 2.100g K14
2904 2.000g El + 2.100g K2 + 0.294g K16 + 2.000g E5 + 2.100g K6 + 2.100g K24
2905 0.200g E2 + 0.210g K2 + 0.200g E5 + 0.294g K16 + 0.210g K7 + 0.210g K9
2906 2.000g E3 + 2.100g K2 + 2.000g E5 + 2.100g K21 + 0.294g K16 + 2.100g K13
2907 1.000g E4 + 1.050g K2 + 1.000g E5 + 1.050g K8 + 1.050g K1 + 0.294g K16
2908 2.000g El + 0.294g K16 + 2.100g K2 + 2.000g E5 + 2.100g K7 + 2.100g K11
2909 2.000g E2 + 2.100g K2 + 0.294g K16 + 2.000g E5 + 2.100g K7 + 2.100g K14
2910 0.200g E3 + 0.210g K2 + 0.200g E5 + 0.294g K16 + 0.210g K7 + 0.210g K24
2911 0.200g E4 + 0.210g K2 + 0.200g E5 + 0.210g K9 + 0.294g K16 + 0.210g K13
2912 1.000g El + 1.050g K2 + 1.000g E5 + 1.050g K9 + 1.050g K1 + 0.294g K16
2913 1.000g E2 + 0.294g K16 + 1.050g K2 + 1.000g E5 + 1.050g K9 + 1.050g K11
2914 2.000g E3 + 2.100g K2 + 0.294g K16 + 2.000g E5 + 2.100g K9 + 2.100g K14
2915 0.200g E4 + 0.210g K2 + 0.200g E5 + 0.294g K16 + 0.210g K9 + 0.210g K24
2916 2.000g El + 2.100g K2 + 2.000g E5 + 2.100g K13 + 0.294g K16 + 2.100g Kl
CA 02646867 2008-12-16
W245FQ/JC 143
2917 2.000gE2+2.100gK2+2.000gE5+2.100gK13+2.100gK11 +0.294gK16
2918 2.000g E3 + 0.294g K16 + 2.100g K2 + 2.000g E5 + 2.100g K13 + 2.100g K14
2919 2.000g E4 + 2.100g K2 + 0.294g K16 + 2.000g E5 + 2.100g K13 + 2.100g K24
2920 1.000g El + 1.050g K2 + 1.000g E5 + 0.294g K16 + 1.050g K1 + 1.050g K11
2921 2.000gE2+2.100gK2+2.000gE5+2.100gK1+0.294gK16+2.100gK14
2922 2.000g E3 + 2.100g K2 + 2.000g E5 + 2.100g K1 + 2.100g K24 + 0.294g K16
2923 0.200g E4 + 0.294g K16 + 0.210g K2 + 0.200g E5 + 0.210g K11 + 0.210g K14
2924 1.000g El + 1.050g K2 + 0.294g K16 + 1.000g E5 + 1.050g K11 + 1.050g K24
2925 0.200g E2 + 0.210g K2 + 0.200g E5 + 0.294g K16 + 0.210g K14 + 0.210g K24
2926 1.250g E3 + 1.313g K2 + 1.250g E7 + 1.313g K12 + 0.294g K16
2927 0.250g E4 + 0.294g K16 + 0.263g K2 + 0.250g E7 + 0.263g K6
2928 0.250g E1 + 0.263g K2 + 0.294g K16 + 0.250g E7 + 0.263g K7
2929 2.500g E2 + 2.625g K2 + 2.500g E7 + 0.294g K16 + 2.625g K9
2930 2.500g E3 + 2.625g K2 + 2.500g E7 + 2.625g K13 + 0.294g K16
2931 1.250g E4 + 0.294g K16 + 1.313g K2 + 1.250g E7 + 1.313g K1
2932 1.250g E1 + 1.313g K2 + 0.497g K16 + 1.250g E7 + 1.313g K11
2933 1.250g E2 + 1.313g K2 + 1.250g E7 + 0.497g K16 + 1.313g K14
2934 0.250g E3 + 0.263g K2 + 0.250g E7 + 0.263g K24 + 0.497g K16
2935 2.000g E4 + 0.497g K16 + 2.100g K2 + 2.000g E7 + 2.100g K12 + 2.100g K6
2936 0.200g El + 0.210g K2 + 0.497g K16 + 0.200g E7 + 0.210g K12 + 0.210g K7
2937 1.000g E2 + 1.050g K2 + 1.000g E7 + 0.497g K16 + 1.050g K12 + 1.050g K9
2938 0.200g E3 + 0.210g K2 + 0.200g E7 + 0.210g K12 + 0.497g K16 + 0.210g K13
2939 2.000g E4 + 2.100g K2 + 2.000g E7 + 2.100g K12 + 2.100g K1 + 0.497g K16
2940 2.000g E1 + 0.497g K16 + 2.100g K2 + 2.000g E7 + 2.100g K12 + 2.100g K11
2941 2.000g E2 + 2.100g K2 + 0.497g K16 + 2.000g E7 + 2.100g K12 + 2.100g K14
2942 1.000g E3 + 1.050g K2 + 1.000g E7 + 0.497g K16 + 1.050g K12 + 1.050g K24
2943 2.000g E4 + 2.100g K2 + 2.000g E7 + 2.100g K6 + 0.497g K16 + 2.100g K7
2944 2.000g E1 + 2.100g K2 + 2.000g E7 + 2.100g K6 + 2.100g K9 + 0.497g K16
2945 1.000g E2 + 0.497g K16 + 1.050g K2 + 1.000g E7 + 1.050g K6 + 1.050g K13
2946 1.000g E3 + 1.050g K2 + 0.497g K16 + 1.000g E7 + 1.050g K6 + 1.050g K1
2947 1.000g E4 + 1.050g K2 + 1.000g E7 + 0.497g K16 + 1.050g K6 + 1.050g K11
2948 2.000g El + 2.100g K2 + 2.000g E7 + 2.100g K6 + 0.497g K16 + 2.100g K14
CA 02646867 2008-12-16
W245FQ/JC 144
2949 0.200g E2 + 0.210g K2 + 0.200g E7 + 0.210g K6 + 0.210g K24 + 0.497g K16
2950 1.000g E3 + 0.497g K16 + 1.050g K2 + 1.000g E7 + 1.050g K7 + 1.050g K9
2951 2.000g E4 + 2.100g K2 + 0.497g K16 + 2.000g E7 + 2.100g K7 + 2.100g K13
2952 0.200g E1 + 0.210g K2 + 0.200g E7 + 0.497g K16 + 0.210g K7 + 0.210g K1
2953 1.000g E2 + 1.050g K2 + 1.000g E7 + 1.050g K7 + 0.497g K16 + 1.050g K11
2954 0.200g E3 + 0.210g K2 + 0.200g E7 + 0.210g K7 + 0.210g K14 + 0.497g K16
2955 2.000g E4 + 0.497g K16 + 2.100g K2 + 2.000g E7 + 2.100g K7 + 2.100g K24
2956 0.200g El + 0.210g K2 + 0.497g K16 + 0.200g E7 + 0.210g K9 + 0.210g K13
2957 0.200g E2 + 0.210g K2 + 0.200g E7 + 0.497g K16 + 0.210g K9 + 0.210g K1
2958 1.000g E3 + 1.050g K2 + 1.000g E7 + 1.050g K9 + 0.497g K16 + 1.050g Kl 1
2959 0.200g E4 + 0.210g K2 + 0.200g E7 + 0.210g K9 + 0.210g K14 + 0.497g K16
2960 1.000g El + 0.497g K16 + 1.050g K2 + 1.000g E7 + 1.050g K9 + 1.050g K24
2961 2.000g E2 + 2.100g K2 + 0.497g K16 + 2.000g E7 + 2.100g K13 + 2.100g K1
2962 2.000g E3 + 2.100g K2 + 2.000g E7 + 0.497g K16 + 2.100g K13 + 2.100g K11
2963 2.000g E4 + 2.100g K2 + 2.000g E7 + 2.100g K13 + 0.497g K16 + 2.100g K14
2964 1.000g El + 1.050g K2 + 1.000g E7 + 1.050g K13 + 1.050g K24 + 0.497g K16
2965 2.000g E2 + 0.497g K16 + 2.100g K2 + 2.000g E7 + 2. lOOg Kl + 2.100g K11
2966 1.000g E3 + 1.050g K2 + 0.497g K16 + 1.000g E7 + 1.050g K1 + 1.050g K14
2967 2.000g E4 + 2.100g K2 + 2.000g E7 + 0.497g K16 + 2.100g K1 + 2.100g K24
2968 0.200g E1 + 0.210g K2 + 0.200g E7 + 0.210g K11 + 0.497g K16 + 0.210g K14
2969 1.000g E2 + 1.050g K2 + 1.000g E7 + 1.050g K11 + 1.050g K24 + 0.497g K16
2970 2.000g E3 + 0.497g K16 + 2.l00g K2 + 2.000g E7 + 2.l00g K14 + 2.100g K24
2971 3.333g E4 + 3.500g K2 + 0.497g K16 + 3.500g K12
2972 2.500g El + 2.625g K2 + 2.625g K12 + 0.497g K16 + 2.625g K6
2973 0.250g E2 + 0.263g K2 + 0.263g K12 + 0.263g K7 + 0.497g K16
2974 0.250g E3 + 0.497g K16 + 0.263g K2 + 0.263g K12 + 0.263g K9
2975 2.500g E4 + 2.625g K2 + 0.497g K16 + 2.625g K12 + 2.625g K13
2976 2.500g El + 2.625g K2 + 2.625g K12 + 0.497g K16 + 2.625g K1
2977 1.250g E2 + 1.313g K2 + 1.313g K12 + 1.313g K11 + 0.497g K16
2978 2.500g E3 + 0.497g K16 + 2.625g K2 + 2.625g K12 + 2.625g K14
2979 1.250gE4+ 1.313g K2 + 0.497g K16 + 1.313gK12+ 1.313gK24
2980 1.000g El + 1.050g K2 + 1.050g K12 + 0.497g K16 + 1.050g K6 + 1.050g K7
CA 02646867 2008-12-16
W245FQ/JC 145
2981 2.000g E2 + 2.100g K2 + 2.100g K12 + 2.100g K6 + 0.497g K16 + 2.100g K9
2982 2.000g E3 + 2.100g K2 + 2.100g K12 + 2.100g K6 + 2.100g K13 + 0.497g K16
2983 2.000g E4 + 0.497g K16 + 2.100g K2 + 2.100g K12 + 2.100g K6 + 2.100g K1
2984 1.000g E1 + 1.050g K2 + 0.497g K16 + 1.050g K12 + 1.050g K6 + 1.050g Kl 1
2985 1.000g E2 + 1.050g K2 + 1.050g K12 + 0.497g K16 + 1.050g K6 + 1.050g K14
2986 0.200gE3+0.210gK2+0.210gK12+0.210gK6+0.497gK16+0.210gK24
2987 2.000g E4 + 2.100g K2 + 2.100g K12 + 2.100g K7 + 2.100g K9 + 0.497g K16
2988 0.200g E1 + 0.497g K16 + 0.210g K2 + 0.210g K12 + 0.210g K7 + 0.210g K13
2989 0.200gE2+0.210gK2+0.497gK16+0.210gK12+0.210gK7+0.210gK1
2990 0.200g E3 + 0.210g K2 + 0.210g K12 + 0.497g K16 + 0.210g K7 + 0.210g K11
2991 2.000g E4 + 2.100g K2 + 2.100g K12 + 2.100g K7 + 0.497g K16 + 2.100g K14
2992 0.200gE1 + 0.210g K2 + 0.210g K12 + 0.210g K21 + 0.210g K24 + 0.497g K16
2993 2.000g E2 + 0.497g K16 + 2.100g K2 + 2.100g K12 + 2.100g K9 + 2.100g K13
2994 1.000g E3 + 1.050g K2 + 0.497g K16 + 1.050g K12 + 1.050g K9 + 1.050g K1
2995 2.000g E4 + 2.100g K2 + 2.100g K12 + 0.497g K16 + 2.100g K9 + 2.100g K11
2996 0.200gE1 + 0.210g K2 + 0.210g K12 + 0.210g K9 + 0.497g K16 + 0.210g K14
2997 2.000g E2 + 2.100g K2 + 2.100g K12 + 2.100g K9 + 2.100g K24 + 0.497g K16
2998 1.000g E3 + 0.497g K16 + 1.050g K2 + 1.050g K12 + 1.050g K13 + 1.050g K1
2999 0.200g E4 + 0.210g K2 + 0.497g K16 + 0.210g K12 + 0.210g K13 + 0.210g K11
3000 1.000g El + 1.050g K2 + 1.050g K12 + 0.497g K16 + 1.050g K13 + 1.050g K14
3001 2.000g E2 + 2.100g K2 + 2.100g K12 + 2.100g K13 + 0.497g K16 + 2.100g K24
3002 0.200g E3 + 0.210g K2 + 0.210g K12 + 0.210g K1 + 0.210g K11 + 0.497g K16
3003 1.000g E4 + 0.497g K16 + 1.050g K2 + 1.050g K12 + 1.050g K1 + 1.050g K14
3004 0.200g E1 + 0.210g K2 + 0.497g K16 + 0.210g K12 + 0.210g K1 + 0.210g K24
3005 2.000g E2 + 2.100g K2 + 2.100g K12 + 0.497g K16 + 2.100g K11 + 2.100g K14
3006 1.000g E3 + 1.050g K2 + 1.050g K12 + 1.050g K11 + 0.497g K16 + 1.050g K24
3007 1.000g E4 + 1.050g K2 + 1.050g K12 + 1.050g K14 + 1.050g K24 + 0.497g K16
3008 1.667g El + 0.497g K16 + 1.750g K2 + 1.750g K6
3009 1.250g E2 + 1.313g K2 + 0.497g K16 + 1.313g K6 + 1.313g K7
3010 2.500g E3 + 2.625g K2 + 2.625g K6 + 0.497g K16 + 2.625g K9
3011 0.250g E4 + 0.263g K2 + 0.263g K6 + 0.263g K13 + 0.497g K16
3012 0.250g El + 0.497g K16 + 0.263g K2 + 0.263g K6 + 0.263g Kl
CA 02646867 2008-12-16
W245FQ/JC 146
3013 2.500g E2 + 2.625g K2 + 0.497g K16 + 2.625g K6 + 2.625g K11
3014 0.250g E3 + 0.263g K2 + 0.263g K6 + 0.497g K16 + 0.263g K14
3015 1.250g E4 + 1.313g K2 + 1.313g K6 + 1.313g K24 + 0.497g K16
3016 0.200g E1 + 0.497g K16 + 0.210g K2 + 0.210g K6 + 0.210g K8 + 0.210g K9
3017 0.200g E2 + 0.210g K2 + 0.497g K16 + 0.210g K6 + 0.210g K7 + 0.210g K13
3018 2.000g E3 + 2.100g K2 + 2.100g K6 + 0.497g K16 + 2.100g K7 + 2.100g Kl
3019 2.000g E4 + 2.100g K2 + 2.100g K6 + 2.100g K7 + 0.497g K16 + 2.100g Kl 1
3020 1.000g El + 1.050g K2 + 1.050g K6 + 1.050g K7 + 1.050g K14 + 0.497g K16
3021 2.000g E2 + 0.497g K16 + 2.100g K2 + 2.100g K6 + 2.100g K7 + 2.100g K24
3022 2.000g E3 + 2.100g K2 + 0.497g K16 + 2.100g K6 + 2.100g K9 + 2.100g K13
3023 0.200g E4 + 0.210g K2 + 0.210g K6 + 0.497g K16 + 0.210g K9 + 0.210g K1
3024 2.000g E1 + 2.100g K2 + 2.100g K6 + 2.100g K9 + 0.497g K16 + 2.100g K11
3025 0.200g E2 + 0.210g K2 + 0.210g K6 + 0.210g K9 + 0.210g K14 + 0.497g K16
3026 0.200g E3 + 0.497g K16 + 0.210g K2 + 0.210g K6 + 0.210g K9 + 0.210g K24
3027 1.000g E4 + 1.050g K2 + 0.497g K16 + 1.050g K6 + 1.050g K13 + 1.050g K1
3028 2.000g E1 + 2.100g K2 + 2.100g K6 + 0.497g K16 + 2.100g K13 + 2.100g K11
3029 1.000g E2 + 1.050g K2 + 1.050g K6 + 1.050g K13 + 0.497g K16 + 1.050g K14
3030 2.000g E3 + 2.100g K2 + 2.100g K6 + 2.100g K13 + 2.100g K24 + 0.497g K16
3031 0.200gE4+0.497gK16+0.210gK2+0.210gK6+0.210gK1 +0.210gK11
3032 0.200g E1 + 0.210g K2 + 0.497g K16 + 0.210g K6 + 0.210g K1 + 0.210g K14
3033 1.000g E2 + 1.050g K2 + 1.050g K6 + 0.497g K16 + 1.050g K1 + 1.050g K24
3034 1.000g E3 + 1.050g K2 + 1.050g K6 + 1.050g K11 + 0.497g K16 + 1.050g K14
3035 0.200g E4 + 0.210g K2 + 0.210g K6 + 0.210g K11 + 0.210g K24 + 0.497g K16
3036 1.000g El + 0.497g K16 + 1.050g K2 + 1.050g K6 + 1.050g K14 + 1.050g K24
3037 1.667g E2 + 1.750g K2 + 0.497g K16 + 1.750g K7
3038 0.250g E3 + 0.263g K2 + 0.263g K7 + 0.497g K16 + 0.263g K9
3039 1.250g E4 + 1.313g K2 + 1.313g K7 + 1.313g K13 + 0.497g K16
3040 2.500g El + 0.497g K16 + 2.625g K2 + 2.625g K7 + 2.625g K1
3041 2.500g E2 + 2.625g K2 + 0.497g K16 + 2.625g K7 + 2.625g Kl 1
3042 1.250g E3 + 1.313g K2 + 1.313g K7 + 0.497g K16 + 1.313g K14
3043 0.250g E4 + 0.263g K2 + 0.263g K7 + 0.263g K24 + 0.497g K16
3044 2.000g El + 0.497g K16 + 2.100g K2 + 2.100g K7 + 2.100g K9 + 2.100g K13
CA 02646867 2008-12-16
W245FQ/JC 147
3045 1.000g E2 + 1.050g K2 + 0.497g K16 + 1.050g K7 + 1.050g K9 + 1.050g Kl
3046 1.000g E3 + 1.050g K2 + 1.050g K7 + 0.497g K16 + 1.050g K9 + 1.050g K11
3047 2.000g E4 + 2.100g K2 + 2.100g K7 + 2.100g K9 + 0.497g K16 + 2.100g K14
3048 0.200g E 1+ 0.210g K2 + 0.210g K7 + 0.210g K9 + 0.210g K24 + 0.497g K 16
3049 1.000g E2 + 0.497g K16 + 1.050g K2 + 1.050g K7 + 1.050g K13 + 1.050g K1
3050 2.000g E3 + 2.100g K2 + 0.497g K16 + 2.100g K21 + 2.100g K13 + 2.100g K11
3051 0.200g E4 + 0.210g K2 + 0.210g K7 + 0.497g K16 + 0.210g K13 + 0.210g K14
3052 1.000g El + 1.050g K2 + 1.050g K7 + 1.050g K13 + 0.497g K16 + 1.050g K24
3053 0.200g E2 + 0.210g K2 + 0.210g K8 + 0.210g K1 + 0.210g K11 + 0.497g K16
3054 2.000g E3 + 0.497g K16 + 2.l00g K2 + 2.l00g K7 + 2.l00g K1 + 2.l00g K14
3055 2.000g E4 + 2.100g K2 + 0.497g K16 + 2.100g K7 + 2.100g K1 + 2.100g K24
3056 1.000g E1 + 1.050g K2 + 1.050g K7 + 0.497g K16 + 1.050g K11 + 1.050g K14
3057 1.000g E2 + 1.050g K2 + 1.050g K7 + 1.050g K11 + 0.497g K16 + 1.050g K24
3058 0.200g E3 + 0.210g K2 + 0.210g K7 + 0.210g K14 + 0.210g K24 + 0.497g K16
3059 0.333g E4 + 0.497g K16 + 0.350g K2 + 0.350g K9
3060 0.250g El + 0.263g K2 + 0.497g K16 + 0.263g K9 + 0.263g K13
3061 0.250g E2 + 0.263g K2 + 0.263g K9 + 0.497g K16 + 0.263g K1
3062 0.250g E3 + 0.263g K2 + 0.263g K9 + 0.263g K11 + 0.497g K16
3063 2.500g E4 + 0.497g K16 + 2.625g K2 + 2.625g K9 + 2.625g K14
3064 1.250g E1 + 1.313g K2 + 0.497g K16 + 1.313g K9 + 1.313g K24
3065 0.200g E2 + 0.210g K2 + 0.210g K9 + 0.497g K16 + 0.210g K13 + 0.210g K1
3066 1.000g E3 + 1.050g K2 + 1.050g K9 + 1.050g K13 + 1.700g K16 + 1.050g Ki 1
3067 0.200g E4 + 0.210g K2 + 0.210g K9 + 0.210g K13 + 0.210g K14 + 1.700g K16
3068 0.200g E1 + 1.700g K16 + 0.210g K2 + 0.210g K9 + 0.210g K13 + 0.210g K24
3069 0.200g E2 + 0.210g K2 + 1.700g K16 + 0.210g K9 + 0.210g Kl + 0.210g K11
3070 0.200g E3 + 0.210g K2 + 0.210g K9 + 1.700g K16 + 0.210g K1 + 0.210g K14
3071 2.000g E4 + 2.100g K2 + 2.100g K9 + 2.100g K1 + 1.700g K16 + 2.100g K24
3072 1.000g E1 + 1.050g K2 + 1.050g K9 + 1.050g K11 + 1.050g K14 + 1.700g K16
3073 1.000g E2 + 1.700g K16 + 1.050g K2 + 1.050g K9 + 1.050g K11 + 1.050g K24
3074 0.200g E3 + 0.210g K2 + 1.700g K16 + 0.210g K9 + 0.210g K14 + 0.210g K24
3075 1.333g E8 + 0.020g K2 + 0.050g K25 + 1.700g K16
3076 2.500g El + 1.700g K16 + 2.625g K2 + 2.625g K13 + 2.625g K1
CA 02646867 2008-12-16
W245FQ/JC 148
3077 0.250g E2 + 0.263g K2 + 1.700g K16 + 0.263g K13 + 0.263g K11
3078 1.250g E3 + 1.313g K2 + 1.313g K13 + 1.700g K16 + 1.313g K14
3079 1.250g E4 + 1.313g K2 + 1.313g K13 + 1.313g K24 + 1.700g K16
3080 1.000g E1 + 1.700g K16 + 1.050g K2 + 1.050g K13 + 1.050g K1 + 1.050g K11
3081 2.000g E2 + 2.100g K2 + 1.700g K16 + 2.100g K13 + 2.100g K1 + 2.100g K14
3082 0.200g E3 + 0.210g K2 + 0.210g K13 + 1.700g K16 + 0.210g Kl + 0.210g K24
3083 1.000g E4 + 1.050g K2 + 1.050g K13 + 1.050g K11 + 1.700g K16 + 1.050g K14
3084 0.200g E1 + 0.210g K2 + 0.210g K13 + 0.210g K11 + 0.210g K24 + 1.700g K16
3085 0.200g E2 + 1.700g K16 + 0.210g K2 + 0.210g K13 + 0.210g K14 + 0.210g K24
3086 3.333g E3 + 3.500g K2 + 1.700g K16 + 3.500g K1
3087 0.250g E4 + 0.263g K2 + 0.263g K1 + 1.700g K16 + 0.263g K11
3088 1.250gE1+1.313gK2+1.313gK1+1.313gK14+1.700gK16
3089 1.250g E2 + 1.700g K16 + 1.313g K2 + 1.313g K1 + 1.313g K24
3090 1.000g E3 + 1.050g K2 + 1.700g K16 + 1.050g K1 + 1.050g K11 + 1.050g K14
3091 1.000g E4 + 1.050g K2 + 1.050g K1 + 1.700g K16 + 1.050g K11 + 1.050g K24
3092 2.000g E1 + 2.100g K2 + 2.100g K1 + 2.100g K14 + 1.700g K16 + 2.100g K24
3093 0.333g E2 + 0.350g K2 + 0.350g Kl 1+ 1.700g K16
3094 1.250g E3 + 1.700g K16 + 1.313g K2 + 1.313g K11 + 1.313g K14
3095 1.250g E4 + 1.313g K2 + 1.700g K16 + 1.313g K11 + 1.313g K24
3096 2.000g El + 2.100g K2 + 2.l00g K11 + 1.700g K16 + 2.l00g K14 + 2.100g K24
3097 1.667g E2 + 1.750g K2 + 1.750g K14 + 1.700g K16
3098 0.250g E3 + 1.700g K16 + 0.263g K2 + 0.263g K14 + 0.263g K24
3099 1.667g E4 + 1.750g K2 + 1.700g K16 + 1.750g K24
3100 0.300g E1 + 0.100g E2 + 0.100g K8 + 0.100g K12 + 0.100g K13 + 0.100g Kl4
+
0.700g K16 + 0.200g J1
The large number of examples shown is based on the enormous flexibility for
the formulator due
to the sheer unlimited ability to use 3-amino-2,6-dimethylphenol in the
context of keratin fiber
coloring compositions. Many more compositions similar to those exemplified are
possible by
modification of compounds (dyes or additives) and their amount in the
composition as such. All
these are obvious alterations for the skilled person from those exemplified
and are not included
for the sake of conciseness.
CA 02646867 2008-12-16
W245FQ/JC 149
Unless stated otherwise, all of the percentages given in the present
application are percentages by
weight.
The dimensions and values disclosed herein are not to be understood as being
strictly limited to
the exact numerical values recited. Instead, unless otherwise specified, each
such dimension is
intended to mean both the recited value and a functionally equivalent range
surrounding that
value. For example, a dimension disclosed as "40 mm" is intended to mean
"about 40 mm".
