Language selection

Search

Patent 3182543 Summary

Third-party information liability

Some of the information on this Web page has been provided by external sources. The Government of Canada is not responsible for the accuracy, reliability or currency of the information supplied by external sources. Users wishing to rely upon this information should consult directly with the source of the information. Content provided by external sources is not subject to official languages, privacy and accessibility requirements.

Claims and Abstract availability

Any discrepancies in the text and image of the Claims and Abstract are due to differing posting times. Text of the Claims and Abstract are posted:

  • At the time the application is open to public inspection;
  • At the time of issue of the patent (grant).
(12) Patent Application: (11) CA 3182543
(54) English Title: PROCESS FOR EXTRACTING CRUDE OIL FROM SUBSTRATES
(54) French Title: PROCEDE D'EXTRACTION DE PETROLE BRUT A PARTIR DE SUBSTRATS
Status: Report sent
Bibliographic Data
(51) International Patent Classification (IPC):
  • C10G 1/04 (2006.01)
  • C10G 1/00 (2006.01)
  • C10G 1/02 (2006.01)
(72) Inventors :
  • THAYER, IAN (United States of America)
  • AZBILL, KEITH (United States of America)
  • THOMPSON, PAUL (United States of America)
  • GAGO, RONALD (United States of America)
  • CLARK, DONALD (United States of America)
(73) Owners :
  • THAYER, IAN (United States of America)
  • AZBILL, KEITH (United States of America)
  • THOMPSON, PAUL (United States of America)
  • GAGO, RONALD (United States of America)
  • CLARK, DONALD (United States of America)
(71) Applicants :
  • THAYER, IAN (United States of America)
  • AZBILL, KEITH (United States of America)
  • THOMPSON, PAUL (United States of America)
  • GAGO, RONALD (United States of America)
  • CLARK, DONALD (United States of America)
(74) Agent: ATMAC PATENT SERVICES LTD.
(74) Associate agent:
(45) Issued:
(22) Filed Date: 2022-11-22
(41) Open to Public Inspection: 2023-02-08
Examination requested: 2022-11-22
Availability of licence: N/A
(25) Language of filing: English

Patent Cooperation Treaty (PCT): No

(30) Application Priority Data: None

Abstracts

English Abstract


A process allows the extraction of heavy hydrocarbon compounds from solid
substrates in an economical and efficient fashion. Materials containing heavy
hydrocarbons (i.e.
oil sands or roofing shingles) are broken up into an auger and then mixed with
light
hydrocarbons. Subsequently, the resulting slurry is shaken to separate fluids
from solids, and the
fluids are subjected to one or more filtering processes to remove waste
sediment. These filtering
processes may include a series of one or more of centrifuges and nozzle
purifier machines.
Filtered fluids are distilled to separate heavy hydrocarbons from light
hydrocarbons.
Simultaneously, the solids are heated to remove the remaining light
hydrocarbons as vapors.
Light hydrocarbons are cooled in a condenser and coalesced in a holding tank,
wherefrom they
may be recirculated into the process and used repeatedly. The now-isolated
heavy hydrocarbons
resulting from the distillation process may be removed as a purified product.


Claims

Note: Claims are shown in the official language in which they were submitted.


WHAT IS CLAIMED IS:
1. An extraction process for separating crude oil from substrates
comprising:
masticating a solid substrate in one or more feed-augers, the solid substrate
containing
heavy hydrocarbons, the heavy hydrocarbons having an API of less than 21;
passing the solid substrate into a mixing chamber;
adding light hydrocarbons to the mixing chamber, the light hydrocarbons having
an API of
more than 45, such that the light hydrocarbons, the heavy hydrocarbons, and
solid
particulates together form a slurry;
purging the mixing chamber of oxygen by injecting nitrogen into the mixing
chamber;
passing the slurry through one or more shakers to separate the slurry into
solids and fluids;
passing the solids through one or more heated-augers to vaporize and remove
the remaining
light hydrocarbons;
passing the fluids through one or more of a centrifuge and a nozzle purifier
to remove solid
particulates from the fluids;
passing the fluids into a distillation stage;
applying heat to the distillation stage to vaporize the light hydrocarbons;
removing the light hydrocarbons from the one or more heated-augers and the
distillation
stage to a condenser;
condensing the light hydrocarbons to a liquid state;
reinjecting the light hydrocarbons into the mixing chamber;
removing the heavy hydrocarbons from the distillation stage as a purified
product having
less than one percent of solid particulates.
2. The extraction process of claim 1 with the additional step of
discarding the solids remaining in the one or more heated-augers after the
heavy
hydrocarbons have been removed from the distillation stage.
7

Description

Note: Descriptions are shown in the official language in which they were submitted.


THA0000CADOO
PROCESS FOR EXTRACTING CRUDE OIL FROM SUBSTRATES
BACKGROUND OF THE INVENTION
Technical Field
[0001] The present invention relates generally to the field of
hydrocarbon processing and
more specifically relates to extraction of crude oils.
Related Art
[0002] The following includes information that may be useful in
understanding the present
disclosure. It is not an admission that any of the information provided herein
is prior art nor
material to the presently described or claimed inventions, nor that any
publication or document
that is specifically or implicitly referenced is prior art.
[0003] Hydrocarbon compounds form the vast majority of fuel energy
sources in modern
industry. Accordingly, processing a wide variety of hydrocarbon types into
purities suitable for
combustion is a critical technology. However, the economic viability of such
processing varies by
hydrocarbon. In particular, a distinction is made between "light" hydrocarbons
(typically defined
as having API gravity over 200) and "heavy" hydrocarbons (having API gravity
less than 20 ).
Generally, "light" hydrocarbons are more valuable and are also easier to
process and transport
due to their flow characteristics. "Heavy" hydrocarbons (i.e. crude oil)
present problems in
processing and transportation since they do not flow easily. Since heavy
hydrocarbons are also
worth less, purifying heavy hydrocarbons is disincentivized in the industry.
If heavy
hydrocarbons can be purified, they can be subjected to cracking processes to
convert the long-
chain hydrocarbon molecules into more useful forms, generally by use of
catalysts. However, it is
the purification of heavy hydrocarbons prior to reaching this stage which is
of particular
difficulty.
[0004] This disincentivization of purifying heavy hydrocarbons is
problematic for two
primary reasons. First, this leaves an untapped source of profit, especially
when light
hydrocarbons and heavy hydrocarbons are harvested together in the same
extraction process.
1
Date Recue/Date Received 2022-11-22

THA0000CADOO
Second, heavy hydrocarbons can be a detriment to the environment when left as
waste product.
Examples may include naturally or artificially occurring oil-saturated soils,
asphalt roof shingles,
aqueous oil spills, and bitumen from degrading or deconstructed roadways.
Accordingly, there is
seen a need to develop a practical and economically viable process for
purifying crude oil out of
.. solid substrates.
[0005] Various attempts have been made to solve problems found in the
oil processing art.
Among these are found in U.S. Patent Nos. 3,415,738, 1,908,616, and 8,790,509.
This prior art is
representative of processes for purifying heavy hydrocarbons.
[0006] None of the above inventions and patents, taken either singly or
in combination, is
seen to describe the invention as claimed. Thus, a need exists for a reliable
process for extracting
crude oil from substrates, and to avoid the above-mentioned problems.
SUMMARY OF THE INVENTION
[0007] In view of the foregoing disadvantages inherent in the known
hydrocarbon processing
art, the present disclosure provides a novel process for extracting crude oil
from substrates. The
general purpose of the present disclosure, which will be described
subsequently in greater detail,
is to provide a process for extracting crude oil from substrates.
[0008] The process allows the extraction of heavy hydrocarbon compounds
from solid
substrates in an economical and efficient fashion. Materials containing heavy
hydrocarbons (i.e.
oil sands or roofing shingles) are broken up into an auger and then mixed with
light
hydrocarbons. Subsequently, the resulting slurry is shaken to separate fluids
from solids, and the
fluids are subjected to one or more filtering processes to remove waste
sediment. These filtering
processes may include a series of one or more of centrifuges and nozzle
purifier machines.
Filtered fluids are distilled to separate heavy hydrocarbons from light
hydrocarbons.
Simultaneously, the solids are heated to remove the remaining light
hydrocarbons as vapors.
Light hydrocarbons are cooled in a condenser and coalesced in a holding tank,
wherefrom they
may be recirculated into the process and used repeatedly. The now-isolated
heavy hydrocarbons
resulting from the distillation process may be removed as a purified product.
2
Date Recue/Date Received 2022-11-22

THA0000CADOO
[0009] For purposes of summarizing the invention, certain aspects,
advantages, and novel
features of the invention have been described herein. It is to be understood
that not necessarily all
such advantages may be achieved in accordance with any one particular
embodiment of the
invention. Thus, the invention may be embodied or carried out in a manner that
achieves or
optimizes one advantage or group of advantages as taught herein without
necessarily achieving
other advantages as may be taught or suggested herein. The features of the
invention which are
believed to be novel are particularly pointed out and distinctly claimed in
the concluding portion
of the specification. These and other features, aspects, and advantages of the
present invention
will become better understood with reference to the following drawings and
detailed description.
BRIEF DESCRIPTION OF THE DRAWINGS
[0010] The figures which accompany the written portion of this
specification illustrate
embodiments and methods of use for the present disclosure, a process for
extracting crude oil
from substrates, constructed and operative according to the teachings of the
present disclosure.
[0011] FIG. 1 is a flow chart illustrating a process for extracting
crude oil from substrates.
[0012] FIG. 2 is chart illustrating the process for extracting crude oil
from substrates and the
interaction of auxiliary systems according to an embodiment of the present
invention.
[0013] The various embodiments of the present invention will hereinafter
be described in
conjunction with the appended drawings, wherein like designations denote like
elements.
DETAILED DESCRIPTION
[0014] As discussed above, embodiments of the present disclosure relate to
a hydrocarbon
separation process and more particularly to a process for extracting crude oil
from substrates as
used to improve the efficiency of harvesting heavy hydrocarbons.
[0015] Generally, the process may be divided into a number of distinct
steps. FIG. 1 shows
an extraction process according to an embodiment of the present disclosure.
3
Date Recue/Date Received 2022-11-22

THA0000CADOO
[0016] Step 1 (101): Initial contaminated hydrocarbons (the object of
the process) are added
to an auger (specifically, a feed-auger). The auger may be used to break up
the material feed. In
some instances, more solid material (such as bitumen or roofing shingles) may
require more
aggressive deconstruction. The auger further acts as a barrier for vapors
during this process.
Augers may be slightly heated in some embodiments; however, heating is not a
primary process
at this stage.
[0017] Step 2 (102): The contaminated hydrocarbons are added to a mixing
tank. Light
hydrocarbons are added to the mixing tank via injection nozzles. The lights
serve to increase API
and flowability, and also act as a solvent to remove heavy oil from the solid
substrate. Nitrogen
purge occurs to displace oxygen in the tank. (Nitrogen may be generated from
atmosphere in
auxiliary process.) Additionally, a vacuum may pull evaporate fumes into a
vapor recovery
system. Slight warming may occur to improve flow characteristics.
[0018] Step 3 (103): This slurry (of contaminated hydrocarbons and added
lights) pass
through shakers to remove waste particulates. Resolution of the shakers may
range from 50 to
300 mesh API as desired for a particular process application by the end user.
Separated fluids
pass down into shakers to be passed to the decanter centrifuge. Waste solids
still containing some
hydrocarbons pass over shakers and directly into the distillation chamber.
Repeated nitrogen
purging.
[0019] Step 4 (104) (optional): Fluids passes through centrifuge to
further remove waste
particulates. Recommended minimum centrifugal force is 2500 G's. Preferably,
this is a decanter
type centrifuge.
[0020] Step 5 (105) (optional) Nozzle machine further removes waste
particulates from the
fluids. This step will generally be used if the contaminate content
(contaminants being basic
solids and water, or BS&W) is still over one percent of total mass. In some
embodiments, a
holding tank may be placed between steps 4 and 5 where this ratio can be
determined for quality
control.
[0021] Step 6: (106) Fluids from holding tank following the centrifuge
and the nozzle
machine enter distillation system. Meanwhile, solids from the shakers are
heating in augers.
4
Date Recue/Date Received 2022-11-22

THA0000CADOO
Heating is critical at this stage to remove light hydrocarbons as vapors.
Heating in one
embodiment may be approximately 500 to 650 degrees Fahrenheit. Nitrogen may be
applied to
purge oxygen. Solids are discarded following this step.
[0022] Step 7: (107) Light hydrocarbons are removed from the heated
augers and cooled in a
condenser. Condenser may use a glycol chiller or a fin fan cooler. Lights are
also collected from
the distillation column. The now re-liquified lights may be recirculated into
Step 2 with a new
batch of raw product to participate in the refining process repeatedly. In
order to continually
provide light hydrocarbons to an automated process, a storage tank collects
and stores re-liquified
lights between the condenser and the mixer in Step 2. Examples of light
hydrocarbons able to be
removed and condensed in this way include natural gas condensate and naphtha,
and generally
any hydrocarbon in the range of 45 to 65 API.
[0023] Step 8: (108) The isolates, the now purified heavy hydrocarbons
(i.e. crude oil, etc.),
may be removed from the distillation column as product.
[0024] FIG. 2 is a flowchart illustrating the extraction process of FIG.
1, according to an
embodiment of the present disclosure. This figure illustrates a process flow
including auxiliary
processes. As before, the process begins when substrates to be purified enter
augers 201.
Masticated substrates enter mixing chamber 202, where light hydrocarbons are
added and a
nitrogen purge occurs. As illustrated, it is here that nitrogen is injected
from nitrogen generator
301. Nitrogen generator may harvest nitrogen directly from the atmosphere,
such as via fractional
distillation or any other practical method. Nitrogen purging may also occur in
shakers 203 and
heater augers 207. From mixing chamber 202, the slurry of substrate and light
hydrocarbons
passes into shakers 203. Here, fluids pass down through the shakers and move
on to centrifuge
204, storage tank 205, and nozzle machine 206, reaching secondary tank 210 in
a decontaminated
form. Hydrocarbons pass from tank 210 into distillation column 211, separating
light
hydrocarbons which can be vaporized from heavy hydrocarbons. In some
embodiments, some of
these steps (generally either 206, or 204-206) may be skipped if such
extensive purification is not
necessary. Meanwhile, the solids pass from shakers 203 into heated augers 207.
Preferably,
heated augers move material for a minimum of 40 feet. Heated augers 207
separate vaporized
hydrocarbons from the solids. Heat is applied (preferably to a climax of
between 500- and 650-
5
Date Recue/Date Received 2022-11-22

THA0000CADOO
degrees Fahrenheit) to remove light hydrocarbons as vapors. From here, vapors
enter condenser
208, where condensation occurs to return the light hydrocarbons to a liquid
form. Light
hydrocarbons from distillation column 211 also collect in condenser 208.
Vacuum 212 provides
the force to draw light hydrocarbon vapors into condenser 208. These
condensates may be stored
in a holding chamber feeding mixing chamber 202. Purified heavy hydrocarbons
may be
removed from distillation stage 211 as a final product and collected in
holding tank 213.
Concurrently, oil heater 302 may operated in a closed circuit, with passages
in contact with
augers 201 and distillation stage 207 for heating purposes.
[0025]
Some auxiliary systems may be implemented. Firstly, an oil heater may heat
a process
oil to 650 degrees Fahrenheit and circulate oil in contact with the augers and
distillation system to
heat these components of the system process. A vacuum pump may operate to pull
vapors from
both the augers and shaker enclosure to add these to the condenser (in
addition to those removed
from the distillation stage). Lastly, a nitrogen generator may produce purge
gas to use in the
augers.
[0026]
The exact specifications, materials used, and method of use of the process for
extracting crude oil from substrates may vary upon manufacturing. Additional
steps may be
implemented where necessary for varying input products, output goals,
environmental factors,
etc.
[0027]
The embodiments of the invention described herein are exemplary and
numerous
modifications, variations and rearrangements can be readily envisioned to
achieve substantially
equivalent results, all of which are intended to be embraced within the spirit
and scope of the
invention. Further, the purpose of the foregoing abstract is to enable the
U.S. Patent and
Trademark Office and the public generally, and especially the scientist,
engineers and
practitioners in the art who are not familiar with patent or legal terms or
phraseology, to
determine quickly from a cursory inspection the nature and essence of the
technical disclosure of
the application.
6
Date Recue/Date Received 2022-11-22

Representative Drawing
A single figure which represents the drawing illustrating the invention.
Administrative Status

For a clearer understanding of the status of the application/patent presented on this page, the site Disclaimer , as well as the definitions for Patent , Administrative Status , Maintenance Fee  and Payment History  should be consulted.

Administrative Status

Title Date
Forecasted Issue Date Unavailable
(22) Filed 2022-11-22
Examination Requested 2022-11-22
(41) Open to Public Inspection 2023-02-08

Abandonment History

There is no abandonment history.

Maintenance Fee


 Upcoming maintenance fee amounts

Description Date Amount
Next Payment if standard fee 2024-11-22 $125.00
Next Payment if small entity fee 2024-11-22 $50.00

Note : If the full payment has not been received on or before the date indicated, a further fee may be required which may be one of the following

  • the reinstatement fee;
  • the late payment fee; or
  • additional fee to reverse deemed expiry.

Patent fees are adjusted on the 1st of January every year. The amounts above are the current amounts if received by December 31 of the current year.
Please refer to the CIPO Patent Fees web page to see all current fee amounts.

Payment History

Fee Type Anniversary Year Due Date Amount Paid Paid Date
Application Fee 2022-11-22 $203.59 2022-11-22
Request for Examination 2026-11-23 $408.00 2022-11-22
Owners on Record

Note: Records showing the ownership history in alphabetical order.

Current Owners on Record
THAYER, IAN
AZBILL, KEITH
THOMPSON, PAUL
GAGO, RONALD
CLARK, DONALD
Past Owners on Record
None
Past Owners that do not appear in the "Owners on Record" listing will appear in other documentation within the application.
Documents

To view selected files, please enter reCAPTCHA code :



To view images, click a link in the Document Description column. To download the documents, select one or more checkboxes in the first column and then click the "Download Selected in PDF format (Zip Archive)" or the "Download Selected as Single PDF" button.

List of published and non-published patent-specific documents on the CPD .

If you have any difficulty accessing content, you can call the Client Service Centre at 1-866-997-1936 or send them an e-mail at CIPO Client Service Centre.


Document
Description 
Date
(yyyy-mm-dd) 
Number of pages   Size of Image (KB) 
New Application 2022-11-22 10 336
Abstract 2022-11-22 1 26
Claims 2022-11-22 1 39
Description 2022-11-22 6 319
Drawings 2022-11-22 2 37
Examiner Requisition 2024-04-16 3 138
Representative Drawing 2023-08-14 1 11
Cover Page 2023-08-14 2 50